CYCLOPHOSPHAMIDE

CYCLOPHOSPHAMIDE
CASRN: 50-18-0
http://toxnet.nlm.nih.gov/cgi-bin/sis/search/f?./temp/~AAA2IaWOB:3

Human Health Effects:

Evidence for Carcinogenicity:

Classification of carcinogenicity: 1) evidence in humans: sufficient; 2) evidence in animals: sufficient. Overall summary evaluation of carcinogenic risk to humans is Group 1: The agent is carcinogenic to humans. /From table/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. S7 61 (1987)]**PEER REVIEWED**

The Carcinogen Assessment Group in EPA's Research and Development Office has evaluated cyclophosphamide for carcinogenicity. According to their analysis, the weight of evidence for cyclophosphamide is group C, which is based on inadequate evidence in humans and limited evidence in animals. As a group C chemical, cyclophosphamide is considered a possible human carcinogen.
[USEPA; Methodology for Evaluating Potential Carcinogenicity in Support of Reportable Quantity Adjustments Pursuant to Cercla Section 102 (1986) OHEA-C-073]**PEER REVIEWED**

Human Toxicity Excerpts:

LIMB REDUCTION DEFECTS HAVE BEEN OBSERVED IN TWO CASES OF INFANTS EXPOSED TO CYCLOPHOSPHAMIDE IN UTERO. ONE MOTHER RECEIVED 100 MG/DAY DURING HER ENTIRE PREGNANCY: HER INFANT HAD NO BIG TOES OR THEIR RESPECTIVE METATARSALS AND PHALANGES; THE LEFT FIFTH FINGER HAD A HYPOPLASTIC MIDPHALANGE; THE INFANT ALSO HAD A PROMINENT PALATAL GROOVE. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 180 (1981)]**PEER REVIEWED**

Paternal use of cyclophosphamide prior to conception has been associated with cardiac & limb abnormalities in an infant.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide crosses the placenta. Use in humans has resulted in both normal & malformed (missing fingers &/or toes, cardiac anomalies, hernias) newborns; risk seems to be less in the second & third trimesters. Low birth weight is also a risk with exposure of the fetus to antineoplastics. First trimester: It is usually recommended that use of antineoplastics, especially combination chemotherapy, be avoided whenever possible, especially during the first trimester. Although information is limited because of the relatively few instances of antineoplastic admin during pregnancy, the mutagenic, teratogenic, & carcinogenic potential of these medications must be considered. Other hazards to the fetus include adverse reactions seen in adults.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

... A treated mother gave birth to a 1900 g infant with multiple anomalies including 4 toes on each foot, flattening of the nasal bridge & a hypoplastic 5th finger. The clinical picture was compatible with fetal injury occurring during an intensive course of iv therapy (1,800 mg) given at about the 77th to 82nd day of gestation.
[Shepard, T.H. Catalog of Teratogenic Agents. 5th ed. Baltimore, MD: The Johns Hopkins University Press, 1986. 159]**PEER REVIEWED**

Patients who receive high dose of cyclophosphamide over prolonged periods may develop interstitial pulmonary fibrosis, which can be fatal. In some cases, discontinuance of the drug and administration of corticosteriods has failed to reverse this syndrome.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Cardiotoxicity, which is uncommon at usual dosages, has been reported in patients receiving high doses of cyclophosphamide (120 (i.e., 60 mg/kg daily) to 270 mg/kg over a period of a few days), generally as part of an intensive, multiple-drug antineoplastic regimen or in conjunction with transplantation procedures. Potentially fatal cardiotoxicity also has occurred when cyclophosphamide (given concomitantly with mesna /2-mercaptoethane sulfonic acid sodium salt/ and followed with autologous bone marrow transplant) was administered inadvertently in a dosage of 4 g/sq m daily for 4 doses rather than in a total dose of 4 g/sq m administered over 4 days in equally divided doses of 1 g/sq m daily as part of a phase I protocol. Deaths have occurred from diffuse hemorrhagic myocardial necrosis and from a syndrome of acute myopericarditis when cyclophosphamide was used in high doses alone or in combination regimens; severe, sometimes fatal congestive heart failure has occurred rarely within a few days after the first dose of cyclophosphamide in such cases. Hemopericardium secondary to hemorrhagic myocarditis and myocardial necrosis, and pericarditis without evidence of hemopericardium, also has been reported.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Sister chromatid exchanges (SCE) and lymphocyte subsets of children with acute lymphoblastic leukemia (ALL) were investigated during chemotherapy. The treatment followed protocol ALL-BFM-90. Children with ALL at the time of diagnosis showed statistically significant higher SCE frequencies (4.9 + or - 0.77) than healthy controls (3.6 + or - 0.93; P = 0.002). The in vivo effects of cyclophosphamide (CP) resulted in a dramatic increase of the SCE frequency (20.5 + or - 3.76). This increased SCE level of lymphocytes might reflect an instability of DNA or a deficiency of DNA repair. One could suggest that lymphocytes of children with ALL might have a higher susceptibility to harmful influences; and this could be a co-factor towards the development of the malignant disease. However, immediately 1 wk after the admin of CP, the SCE rate decreased. This decline of SCE frequency correlated with a severe reduction of the absolute number of T lymphocytes. The observed reduction of SCE frequency may be due to a loss of T lymphocytes, or SCE became repaired during 1 week.
[Mertens R et al; Leukemia 9 (3): 501-5 (1995)]**PEER REVIEWED**

In the present study a cancer risk assessment of occupational exposure to cyclophosphamide (CP), a genotoxic carcinogenic antineoplastic agent, was carried out following two approaches based on (1) data from an animal study and (2) data on primary and secondary tumors in CP-treated patients. Data on the urinary excretion of CP in health care workers were used to estimate the uptake of CP, which ranged from 3.6 to 18 ug/day. Based on data from an animal study, cancer risks were calculated for a health care worker with a body weight of 70 kg and a working period of 40 yr, 200 days/yr (linear extrapolation). The life-time risks (70 yr) of urinary bladder cancer in men and leukemias in men and women were found to be nearly the same and ranged from 95 to 600 per million. Based on the patient studies, cancer risks were calculated by multiplication of the 10-yr cumulative incidence per gram of CP in patients by the estimated mean total uptake in health care workers over 10 yr, 200 days/yr. The risk of leukemias in women over 10 yr ranged from 17 to 100 per million using the secondary tumor data (linear extrapolation). Comparable results were obtained for the risk of urinary bladder tumors and leukemias in men and women when primary tumor data were used. Thus, on an annual basis, cancer risks obtained from both the animal and the patient study were nearly the same and ranged from about 1.4 to 10 per million. In The Netherlands it is proposed that, for workers, a cancer risk per cmpd of one extra cancer case/million/year should be striven for ("target risk") and that no risk higher than 100/million/year ("prohibitory risk") should be tolerated.
[Sessink PH et al; Int Arch Occup Environ Health 67 (5): 317-23 (1995)]**PEER REVIEWED**

Cyclophosphamide ... commonly cause a severe hemorrhagic cystitis in acute overdose. Nausea and vomiting occur acutely due to destruction of the intestinal epithelium. Myelosuppression with resultant leukopenia, anemia, and variable thrombocytopenia has been reported. Leukocyte counts fall within 1 week after therapeutic treatment; platelets decline soon afterward. Maximum depression occurs in 2-3 weeks, followed by quick recovery. Hair and hearing loss with tinnitus have been reported.
[Ford MD, Delaney KA, Ling LJ, Erickson T; Clinical Toxicology. W.B. Saunders Company., Philadelphia, PA. 2001 455]**PEER REVIEWED**

Alkylating agents are cytotoxic and kill rapidly dividing neoplastic and normal cells and have drastic effects on cells of the immune system. ... In cancer patients, a high CY dose (1000 mg/sq m intravenously (iv)) results in 30 and 40% reduction of B and T cells, respectively, after 7 days ... . A low CY dose (300 mg/sq m iv), on the contrary, had no effect on the number of B and T cells. /Alkylating agents/
[Foye, W.O. (ed.). Cancer Chemotherapeutic Agents. ACS Professional Reference Book. Washington, D.C.: American Chemical Society, 1995. 468]**PEER REVIEWED**

A newborn exposed in utero to cyclophosphamide during the 1st trimester presented with multiple anomalies. the mother, who was being treated for a severe exacerbation of systemic lupus erythematosus, received 2 IV doses of 200 mg each between 15 & 46 days' gestation. Except for prednisone, 20 mg/day, no other medication was given during the pregnancy. The 3150 g female infant was delivered at 39 wk gestational age with multiple abnormalities, including dysmorphic facies, multiple eye defects including bilateral blepharophimosis with left microphthalmos, abnormally shaped. low-set ears, cleft palate, bilaterally absent thumbs, & dystrophic nails. Borderline microcephaly, hypotonia, & possible developmental delay were observed at 10 months of age.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 234]**PEER REVIEWED**

Cyclophosphamide is one of the most common causes of chemotherapy-induced menstrual difficulties & azoospermia. Permanent secondary amenorrhea with evidence of primary ovarian damage has been observed after long-term (20 months) use of cyclophosphamide. In contrast, successful pregnancies have been reported following high-dose therapy. Moreover, azoospermia appears to be reversible when the drug is stopped.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 234]**PEER REVIEWED**

Cyclophosphamide-induced chromosomal abnormalities are also of doubtful clinical significance but have been described in some patients after use of the drug. A study published in 1974 reported chromosome abnormalities in patients treated with cyclophosphamide for rheumatoid arthritis & scleroderma. In contrast, chromosome studies were normal in a mother & infant treated during the 2nd & 3rd trimesters in another report. In another case, a 34 yr old woman with acute lymphoblastic leukemia was treated with multiple antineoplastic agents form 22 wk gestation until delivery of a healthy female infant 18 wk later. Cyclophosphamide was admin 3 times between the 26th & 30th wks of gestation. Chromosome analysis of the newborn revealed a normal karyotype (46,XX) but with gaps & a ring chromosome. The clinical significance of these finding sin unknown, but since these abnormalities may persist for several years, the potential existed for an increased risk of cancer as well as for a risk of genetic damage in the next generation.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 235]**PEER REVIEWED**

A study published in 1985 examined 30 men to determine the effect of cyclophosphamide on male hormone levels & spermatogenesis. The men had been treated at a mean age of 9.4 yr for a mean duration of 280 days. The mean age of the men at the time of the study was 22 yrs with a mean interval form end of treatment to evaluation of 12.8 yrs. Four of the men were azoospermic, 9 were oligospermic, & 17 were normospermic. Compared to normal controls, however, the 17 men classified as normospermic had lower ejaculate volumes (3.1 vs. 3.3 ml), lower sperm density (54.5*10^6 vs. 79*10^6/ml), decreased sperm motility (42% vs. 61%, p<0.05), & less normal sperm forms (61% vs. 70%, p<0.05). concns of testosterone, dehydroepiandrosterone sulfate, & prolactin were not significantly different between patients & controls. One oligospermic man (sperm density 12*10^6/ml) had fathered a child.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 236]**PEER REVIEWED**

A 1979 report involved a case of an 18 yr old woman with Burkitt lymphoma diagnosed in the 26th wk of gestation. She was treated with a 7 day course of cyclophosphamide, 10 mg/kg/day IV, as a single daily dose (total dose 3.5 g). Six weeks after the last chemotherapy dose, she delivered a normal, 2160 g male infant. Analysis of the newborn's blood counts was not conducted. The tumor recurred in the postpartum period, & treatment with cyclophosphamide, 6 mg/kg/day IV, was started 20 days after delivery. Although she was advised not to nurse her infant, she continued to do so until her sudden death after the third dose of cyclophosphamide. Blood counts were conducted on both the mother & the infant during therapy. Immediately prior to the first dose, the infant's leukocyte & platelet counts were 4,800/cu mm (abnormally low for age) & 270,000/cu mm, respectively. After the third maternal dose, the infant's counts were 3,200/cu mm & 47,000/cu mm, respectively. Both counts were interpreted by the investigator as signs of cyclophosphamide-induced toxicity. It was concluded that breast feeding should be stopped during therapy with the agent.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 237]**PEER REVIEWED**

Chemotherapy induced pulmonary toxicity: Cyclophosphamide. Histopathology: endothelial swelling, pneumocyte dysplasia, lymphocyte infiltration; fibrosis. Clinical features: Does not appear to be schedule- or does-related & may occur after discontinuation. Clinical presentation: progressive dyspnea, fever, dry cough, tachypnea, fine rales, decr diffusing capacity & restrictive ventilatory defect, bilateral interstitial infiltrates. Treatment/Outcome: Clinical recovery reported in about 50% of patients within 1-8 wk if therapy stopped. Some of these patients received steroid therapy; however, others have died despite steroid therapy. Occasionally, therapy has been restated without recurrence. /from table/
[Young, L.Y., M.A. Koda-Kimble (eds.). Applied Therapeutics. The Clinical Use of Drugs. 6th ed. Vancouver, WA., Applied Therapeutics, Inc. 1995.,p. 91-24]**PEER REVIEWED**

Two patients received four times the lethal dose of cyclophosphamide: one died & the other has residual cardiac damage.
[Ellenhorn, M.J., S. Schonwald, G. Ordog, J. Wasserberger. Ellenhorn's Medical Toxicology: Diagnosis and Treatment of Human Poisoning. 2nd ed. Baltimore, MD: Williams and Wilkins, 1997. 1345]**PEER REVIEWED**

In order to develop a method for detecting metabolism-mediated embryotoxicity, differentiating embryonic stem (ES) cells were exposed to the well-known proteratogen, cyclophosphamide (CPA). CPA was tested in a scientifically validated embryonic stem-cell test (EST), and in the newly developed reporter-gene assay for developmental cardiotoxicity. Both assays gave false-negative results. Because no metabolic competence (cytochrome P450 activity) was found in the ES cells under the selected culture conditions, a simple biotransformation system was combined with the reporter-gene assay. As the metabolic pathway of CPA is well characterised, the genetically engineered mammalian cell line V79, transfected with CYP2B1 cDNA, was selected as a biotransformation system. CYP2B1 is responsible for transforming CPA into teratogenically active metabolites. The supernatants of genetically engineered V79 cells were analysed in the reporter-gene assay for developmental cardiotoxicity. In preliminary experiments, the combined system was able to detect the embryotoxic potential of the proteratogen, CPA.
[Bremer S, et al; Altern Lab Anim 30 (1): 77-85 (2002)]**PEER REVIEWED**

A 3 hr exposure time, in both the absence & presence of metabolic activation, was used for the in vitro Comet assay. ...The Comet assay & the chromosomal aberration tests was found to be satisfactory on a qualitative basis, although positive results in the Comet assay were always at higher doses than in the cytogenetic test.
[Giannotti E, et al; Mutagenesis 17 (2): 163-70. 2002.]**PEER REVIEWED**

These studies enable the pattern of emesis and nausea for 3 days following high-dose cyclophosphamide to be described and give some insight into the mechanisms of emesis which may be operating. Nausea and vomiting induced by cyclophosphamide-based chemotherapy has long latency of onset (8-13 hr) and continues for at least 3 days. These findings are of particular importance as many of these patients receive chemotherapy as outpatients and emphasize the need for appropriate anti-emetic prophylaxis for patients at home. Ondansetron was extremely effective over this time in the control of emesis and nausea. These results suggest that high-dose cyclophosphamide-induced emesis over days 1-3 is largely mediated via 5-hydroxytryptamine (5-HT) and 5-HT3 receptors.
[Beck TM; Anticancer Dugs 6 (2): 237-42 (1995)]**PEER REVIEWED**

Skin, Eye and Respiratory Irritations:

A powerful skin irritant.
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 973]**PEER REVIEWED**

Drug Warnings:

Appropriate caution is advised when the drug is considered for use in ... /nonneoplastic/ conditions, not only because of its acute toxic effects but also because of its high potential for inducing sterility, teratogenic effects, & leukemia. ... Administration of the drug should be interrupted at the first indication of dysuria or hematuria. The syndrome of inappropriate secretion of antidiuretic hormone (ADH) has been observed in patients receiving cyclophosphamide, usually at doses higher than 50 mg/kg. It is important to be aware of the possibility of water intoxication, since these patients are usually vigorously hydrated.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

POTENTIAL ADVERSE EFFECTS ON FETUS: Various fetal malformations, especially skeletal defects and dysmorphic features, but other chemotherapeutic agents given concurrently. POTENTIAL SIDE EFFECTS ON BREAST-FED INFANT: Transient neutropenia from cyclophosphamide with prednisone and vincristine. Potential mutagenicity, carcinogenicity, adverse effects on fetus. FDA Category: D (D = There is evidence of human fetal risk, but the potential benefits from use in pregnant women may be acceptable despite the potential risks (e.g., if the drug is needed in a life-threatening situation or for a serious disease for which safer drugs cannot be used or are ineffective.)) /from Table II/
[Stockton DL and Paller AS; J Am Acad Dermatol 23 (1):87-103 (1990)]**PEER REVIEWED**

Drugs that are Contraindicated during Breast-Feeding: Cyclophosphamide: Possible immune suppression; unknown effect on growth or association with carcinogenesis; neutropenia. /from Table 1./
[Report of the American Academy of Pediatrics Committee on Drugs in Pediatrics 93 (1): 138 (1994)]**PEER REVIEWED**

THE DRUG IS MOST TOXIC TO THE HUMAN FETUS DURING 1ST 3 MO & CONGENITAL ABNORMALITIES HAVE BEEN DETECTED AFTER IV INJECTION OF LARGE DOSES TO PREGNANT WOMEN DURING THIS PERIOD OF PREGNANCY. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 146 (1975)]**PEER REVIEWED**

For routine clinical use, ample fluid intake is recommended.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1396]**PEER REVIEWED**

Cyclophosphamide is distributed into breast milk. Breast-feeding is not recommended during chemotherapy because of the risks to the infant (adverse effects, mutagenicity, carcinogenicity).
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Prepubescent girls treated with cyclophosphamide usually develop secondary sexual characteristics normally, have regular menses, and subsequently conceive; however, ovarian fibrosis and apparent complete loss of germ cells after prolonged treatment in late prepubescence have been reported. Prepubescent boys treated with cyclophosphamide develop secondary sexual characteristics normally, but may have oligospermia or azoospermia, increased gonadotropin secretion, and some degree of testicular atrophy; azoospermia may be reversible, although possibly not for several years after the end of cyclophosphamide therapy.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Although appropriate studies on the relationship of age to the effects of cyclophosphamide have not been performed in the geriatric population, geriatrics-specific problems are not expected to limit the usefulness of this medication in the elderly. However, elderly patients are more likely to have age-related renal function impairment, which may require caution in patients receiving cyclophosphamide.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

The bone marrow depressant effects of cyclophosphamide may result in an increased incidence of microbial infection, delayed healing, and gingival bleeding. Dental work, whenever possible should be completed prior to initiation of therapy or deferred until blood counts have returned to normal. Patients should be instructed in proper oral hygiene during treatment, including caution in use of regular tooth brushes, dental floss, and toothpicks. Cyclophosphamide may also rarely cause stomatitis associated with considerable discomfort.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Because normal defense mechanisms may be suppressed by cyclophosphamide therapy, concurrent use with a live virus vaccine may potentiate the replication of the vaccine virus, may increase the side/adverse effects of the vaccine virus, and/or may decrease the patient's antibody response to the vaccine; immunization of these patients should be undertaken only with extreme caution after careful review of the patient's hematologic status and only with the knowledge and consent of the physician managing the cyclophosphamide therapy. The interval between discontinuation of medication that cause immunosuppression and restoration of the patient's ability to respond to the vaccine depends on the intensity and type of immunosuppression-causing medications used, the underlying disease, and other factors; estimates vary from 3 months to 1 year. Patients with leukemia in remission should not receive live virus vaccine until at least 3 months after their last chemotherapy. In addition, immunization with oral polio-virus vaccine should be postponed in persons in close contact with the patient, especially family members.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Anorexia, nausea, and vomiting occur commonly with cyclophosphamide, especially at high doses; some clinicians reported that these effects respond to treatment with antiemetics. Occasionally, diarrhea, hemorrhagic colitis, mucosal irritation, and oral ulceration have been reported. Rarely, aphthous stomatitis, enterocolitis, and hepatotoxicity as evidenced by jaundice and hepatic dysfunction have occurred.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Alopecia occurs frequently in patients who receive cyclophosphamide and patients should be forewarned of this possibility. In usual doses, about 33% of patients who receive the drug experience alopecia, generally beginning about 3 weeks after initiation of therapy; the condition is usually reversible but new hair may be a different color or texture. Transverse ridging, retarded growth, and/or pigmentation of fingernails may occur, as well as skin pigmentation. Nonspecific dermatitis has also been reported.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Other reported adverse effects of cyclophosphamide include headache, dizziness, and myxedema. Faintness, facial flushing, diaphoresis, and oropharyngeal sensation have occurred following IV administration of cyclophosphamide, have been reported. The drug may interfere with normal wound healing.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements).,p. 960-1]**PEER REVIEWED**

Some patients who have received cyclophosphamide alone, as part of a combination regimen, or as adjunctive therapy have developed secondary malignancies, most frequently urinary bladder, myeloproliferative, & lymphoproliferative malignancies. Although a causal relationship has not been definitely established, the possibility of development of a secondary malignancy should be considered in weighing the possible benefit from the drug against the potential risk. Secondary malignancies have occurred most frequently in patients who have been treated with cyclophosphamide for primary myeloproliferative & lymphoproliferative malignancies & primary nonmalignant diseases in which immune processes are believed to be involved. Secondary urinary bladder malignancies generally have occurred in patients who previously developed hemorrhagic cystitis. In some cases, the secondary malignancy was not detected until several years after discontinuance of cyclophosphamide therapy. Long-term follow-up of women who received cyclophosphamide-containing adjuvant chemotherapy regimens for the treatment of early breast cancer indicates that the incidence of other solid tumors & secondary leukemia in these women is not substantially greater than that in the general population.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 961]**PEER REVIEWED**

CAREFUL EVALUATION OF BONE MARROW FUNCTION IS IMPERATIVE AND PROLONGED THERAPY IS GUIDED BY KEEPING THE TOTAL LEUKOCYTE COUNT BETWEEN 2500 AND 4000 CELLS PER CUBIC MILLIMETER OF BLOOD OR BY OBTAINING THE DESIRED RESPONSE OF THE TUMOR.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1218]**PEER REVIEWED**

Potentially fatal cardiotoxicity also has occurred when cyclophosphamide (given concomitantly with mesna /2-mercaptoethane sulfonic acid sodium salt/ and followed with autologous bone marrow transplant) was administered inadvertently in a dosage of 4 g/sq m daily for 4 doses rather than in a total dose of 4 g/sq m administered over 4 days in equally divided doses of 1 g/sq m daily as part of a phase I protocol.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

One of the major and dose limiting adverse effects of cyclophosphamide is hematologic toxicity, which is usually reversible after discontinuance of the drug. Hematopoietic adverse effects include leukopenia, thrombocytopenia, hypothrombinemia, and anemia. Leukopenia is considered to be an expected effect of cyclophosphamide therapy and may be severe. Leukopenia nadirs generally occur at 8-15 days following a single dose of cyclophosphamide and recovery usually occurs within 17-28 days. Thrombocytopenia is reportedly less common, with nadirs occurring 10-15 days after administration of the drug. Anemia, particularly after large doses or prolonged therapy, and rarely hypoprothrombinemia have been reported. Rarely, cyclophosphamide has been reported to produce positive direct antiglobulin (Coombs') test results and hemolytic anemia.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

In children treated with cyclophosphamide a transient blurring of vision has been reported in 5 out of 59, coming on in minutes after intravenous injection in two and within 24 hours in the other three. The duration of blurring ranged from one hour to two weeks, but vision returned to normal in all.
[Grant, W.M. Toxicology of the Eye. 3rd ed. Springfield, IL: Charles C. Thomas Publisher, 1986. 299]**PEER REVIEWED**

Cyclophosphamide can cause sterility in people of either sex. It can damage the germinal cells in prepubertal, pubertal and adult males, and causes premature ovarian failure in females.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 180 (1981)]**PEER REVIEWED**

... To analyse the treatment-related complications of busulphan and cyclophosphamide (BU-CY) as the conditioning regimen for allogeneic peripheral blood stem cell transplantation (allo-PBSCT). ... The clinical data of 40 leukemia patients undergoing allo-PBSCT between June 1997 and May 1999 in our BMT center were retrospectively analysed. ... Recovery of neutrophil and platelet was achieved at a median of day +13 (9 similar 28) and day +12 (7 similar 60) respectively. Acute GVHD occurred in 17 of 40 patients (42.5%) with grade II-IV in 10 patients (25%). Chronic GVHD developed in 21 out of 30 evaluable patients (70%). Mild to severe mucositis occurred in 30 patients (75%), and 4 of them had severe esophagitis with bleeding. Haemorrhagic cystitis developed in 8/40 (20%) patients, the median time of its onset was day +100 (+7 to +165). Six of 40 patients (15%) developed interstitial pneumonia (IP), 5 of them were due to cytomegalovirus infection, and the remaining one due to pneumocystis carinii infection. No hepatic veno-occlusive disease was observed and no seizure occurred. During the median follow-up of 480 (300 similar 1000) days, 4 (10%) patients relapsed and 8 (20%) patients died of the transplant-related complications. The 3 year leukemia-free survival rate was 70%. ... BU (domestic busulfan)-CY regimen is relatively easy to administer and well tolerated, with low extramedullary toxicities.
[Zhu K, et al; Zhonghua Xue Ye Xue Za Zhi 21 (8): 403-405. 2000.]**PEER REVIEWED**

... We now described five patients receiving monthly cycles of iv CP /cyclophosphamide/ whose allergic reactions included clinical features of type I hypersensitivity but were atypical in their markedly delayed onset (i.e., 8 to 16 hr in patients 1 to 4 and 10 days in patient 5) ... The objective was to investigate these late-developing clinical reactions by skin testing with CP and two of its major metabolites ... The five patients and a control group receiving iv CP uneventfully were studied by the same skin test protocol ... The four individual in the control group were unreactive to CP or its metabolites. All five patients with late-onset allergic reactions had positive immediate skin test results to CP metabolites but not to CP itself. We propose that the allergic reactions in patients 1 to 4 were mediated, wholly or in major part, by IgE antibodies reactive with allergens derived from time-dependent drug metabolites.
[Popescu NA et al; J Allergy Clin Immunol 97 (1 Pt 1): 26-33 (1996)]**PEER REVIEWED**

Sterile hemorrhagic cystitis has been reported to occur in up to 20% of patients (especially children) on long-term cyclophosphamide therapy. The effect, which rarely can be severe and even fatal, is attributed to chemical irritation by active metabolites of cyclophosphamide that accumulate in concentrated urine. Hematuria usually resolves spontaneously within a few days after discontinuance of cyclophosphamide therapy but may persist for several months. Fibrosis of the bladder (sometimes extensive), with or without cystitis, also has occurred, but less frequently. Atypical epithelial cells may be found in the urinary sediment. These adverse effects appear to be related to the dosage and duration of cyclophosphamide therapy. Nephrotoxicity, including hemorrhagic ureteritis and renal tubular necrosis, has been reported; such lesions reportedly resolve in most instances following discontinuance of cyclophosphamide therapy.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

THERE HAVE BEEN AT LEAST 30 CASE REPORTS OF MALIGNANCY IN PATIENTS TREATED WITH CYCLOPHOSPHAMIDE FOR NONMALIGNANT DISORDERS, MAINLY RHEUMATOID ARTHRITIS AND CHRONIC GLOMERULONEPHRITIS. THESE INCLUDED 17 ACUTE NONLYMPHOCYTIC LEUKEMIAS, ONE CHRONIC NONLYMPHOCYTIC LEUKEMIA, ONE ACUTE LYMPHOCYTIC LEUKEMIA, ONE CHRONIC LYMPHOCYTIC LEUKEMIA, TWO BLADDER CANCERS, ONE SQUAMOUS CELL CANCER OF THE SKIN, THREE RETICULUM CELL SARCOMAS, ONE HODGKIN'S DISEASE, ONE MELANOMA, TWO CEREBRAL GLIOMAS, ONE CERVICAL CANCER AND ONE PLEURAL SARCOMA. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 182 (1981)]**PEER REVIEWED**

Gonadal suppression, resulting in amenorrhea or azoospermia, may occur in patients taking antineoplastic therapy, especially with the alkylating agents. In general, these effects appear to be related to dose & length of therapy & may be irreversible. Prediction of the degree of testicular or ovarian function impairment is complicated by the common use of combinations of several antineoplastics, which makes it difficult to assess the effects of individual agents. However, there have been numerous reports of gonadal suppression with use of cyclophosphamide, which seems to depend on dose, duration, & state of gonadal function at the time of therapy, sterility may be irreversible in some patients.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 1102]**PEER REVIEWED**

THERE WAS INCR IN NUMBER OF CHROMOSOMAL ABERRATIONS IN THE PERIPHERAL BLOOD LYMPHOCYTES OF CHILDREN TREATED WITH CYCLOPHOSPHAMIDE (3-5 MG/DAY FOR 6-8 MONTHS) FOR NONMALIGNANT CONDITIONS & OF PATIENTS WITH RHEUMATOID ARTHRITIS FOLLOWING CYCLOPHOSPHAMIDE TREATMENT. SIMILAR INCR WERE OBSERVED IN LYMPHOCYTES OF WOMEN WITH RECURRENT OVARIAN OR UTERAL CARCINOMA 3 OR 24 HR AFTER AN IV ADMIN OF 2.0 G & IN THE BONE MARROW & LYMPH NODE CELLS OF PATIENTS WITH LYMPHOGRANULOMATOSIS 24-72 HR AFTER SINGLE DOSE OF 400 MG CYCLOPHOSPHAMIDE. INCR LEVELS OF SISTER CHROMATID EXCHANGE IN PERIPHERAL BLOOD LYMPHOCYTES HAVE BEEN OBSERVED IN PATIENTS TREATED WITH CYCLOPHOSPHAMIDE. THESE HAVE INCLUDED PATIENTS WITH MALIGNANT LYMPHOMA & NEPHROTIC SYNDROME, A PATIENT WITH RETICULOSARCOMA, 3 PATIENTS WITH UNSPECIFIED MALIGNANT TUMORS & 1 PATIENT WITH ACUTE GLOMERULONEPHRITIS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 181 (1981)]**PEER REVIEWED**

LEUKOPENIA IS INEVITABLE SIDE EFFECT & IS USED AS INDEX OF DOSAGE ... HYPOPROTHROMBINEMIA ... .
[Osol, A. (ed.). Remington's Pharmaceutical Sciences. 16th ed. Easton, Pennsylvania: Mack Publishing Co., 1980. 1088]**PEER REVIEWED**

Nausea & vomiting, myelosuppression with platelet sparing, & alopecia are common to virtually all regimens using cyclophosphamide. Mucosal ulcerations &, less frequently, interstitial pulmonary fibrosis also may result from cyclophosphamide treatment. Extravasation of the drug into subcutaneous tissues does not produce local reactions, & thrombophlebitis does not complicate iv admin. The occurrence of sterile hemorrhagic cystitis has been reported in 5%-10% of patients. As noted above, this has been attributed to chemical irritation produced by acrolein. Its incidence is significantly reduced by coadministration of mesna. For routine clinical use, ample fluid intake is recommended. Admin of the drug should be interrupted at the first indication of dysuria or hematuria. The syndrome of inappropriate secretion of antidiuretic hormone (ADH) has been observed in patients receiving cyclophosphamide, usually at doses higher then 50 mg/kg. It is important to be aware of the possibility of water intoxication, since these patients usually are vigorously hydrated.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

Medical Surveillance:

PRECAUTIONS FOR "CARCINOGENS": Whenever medical surveillance is indicated, in particular when exposure to a carcinogen has occurred, ad hoc decisions should be taken concerning ... /cytogenetic and/or other/ tests that might become useful or mandatory. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 23]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ There is no method available for routine monitoring of personnel for evidence of hazardous drug exposure. Tests for the presence of mutagens or chromosomal damage are not drug specific and are of value only in controlled studies. Chemical analysis of urine for the presence of hazardous drugs at the sensitivity level needed to detect occupational exposure is limited to a few drugs and is not yet commercially available. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 759]**PEER REVIEWED**

Probable Routes of Human Exposure:

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The danger to health-care personnel from handling a hazardous drug stems from a combination of its inherent toxicity and the extent to which workers are exposed to the drug in the course of carrying out their duties. This exposure may be through inadvertent ingestion of the drug on foodstuffs (eg, workers' lunches), inhalation of drug dusts or droplets or direct skin contact. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 752]**PEER REVIEWED**

NIOSH (NOES Survey 1981-1983) has statistically estimated that 30,026 workers (20,745 of these are female) are potentially exposed to cyclophosphamide in the US(1). Occupational exposure to cyclophosphamide may occur through inhalation and dermal contact with this compound at workplaces where cyclophosphamide is produced or used(SRC). Workers involved in formulating and dispensing the drug may be exposed through dermal contact (with the dry powder or solutions), or inhalation of dust(SRC). Direct human exposure occurs through ingestion of the drug (when dispensed in tablet form) and through injection (when administered intravenously)(2).
[(1) NIOSH; National Occupational Exposure Survey (NOES) (1983) (2) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Lyon, France: World Health Org, Inter Agency Res Cancer 26: 165-202 (1981)]**PEER REVIEWED**

Air monitoring conducted in a West German manufacturing facility in April 1984 found cyclophosphamide levels ranging from 0.1 to 810 ug/cu m(1). Air concentrations of 2-480 ug/cu m were detected in a production area of a plant involved weighing cyclophosphamide and formulating it into tablets(1). No detectable levels (detection limit of 0.05 ug/cu m) were found in air samples (taken from flow hoods) from a hospital dispensing and administering cyclophosphamide; however, filter media from the flow hoods contained measurable quantities suggesting that some exposure can occur(1). Concentrations of cyclophosphamide in personal air samplers from a manufacturing facility ranged from less than the detection limit to 97.0 ug/cu m, and in a laminar-flow hood, the concentrations ranged from 0-60 ng/cu m(2).
[(1) Pyy, L et al; Am Ind Hyd Assoc J 49: 314-317 (1988) (2) Sorsa, M et al; Mutat Res 204: 465-79 (1988)]**PEER REVIEWED**

Body Burden:

In a cross-sectional study, the urine of 20 hospital workers occupationally exposed to cyclophosphamide and 21 unexposed controls was monitored for excretion of cyclophosphamide. During the week in which samples were collected, most of the workers handled cyclophosphamide fewer than 5 times and the amount handled each time ranged from 100-1000 mg (mean +/- 350 mg). All workers claimed to have taken regular safety precautions, ie, at least wearing gloves during handling. The drug was identified in 5 cases (range: 0.7-2.5 ug excreted/24 hr urine). A clear relationship between cyclophosphamide handling and urinary detection was shown. 4 of 5 persons with detectable urinary cyclophosphamide had handled cyclophosphamide 10 times or more during the week.
[Evelo CTA et al; Int Arch Occup Environ Health 58: 151-5 (1986)]**PEER REVIEWED**

Cyclophosphamide (along with ifosfamide) was detected in the urine of 8 pharmacy technicians and nurses (along with ifosfamide) at amounts ranging from <0.001-0.5 ug(1). 21 nurses and pharmacy personnel in a Munich, Germany hospital were monitored for compound exposure; on days when 3,900 mg/l cyclophosphamide was mixed, 12 of 31 urine samples tested positive with concentrations ranging from 3.5 to 38 ug/24 hr urine(2).
[(1) Sessink, PJM et al; Int Arch Occup Environ Health 64: 105-112 (1992) (2) Ensslin AS et al; Occup Environ Med 51: 229-33 (1994)]**PEER REVIEWED**

Antidote and Emergency Treatment:

Basic treatment: Establish a patent airway. Suction if necessary. Watch for signs of respiratory insufficiency and assist ventilations if needed. Administer oxygen by nonrebreather mask at 10 to 15 L/min. Monitor for pulmonary edema and treat if necessary ... . Monitor for shock and treat if necessary ... . Anticipate seizures and treat if necessary ... . For eye contamination, flush eyes immediately with water. Irrigate each eye continuously with normal saline during transport ... . Do not use emetics. For ingestion, rinse mouth and administer 5 ml/kg up to 200 ml of water for dilution if the patient can swallow, has a strong gag reflex, and does not drool ... . Cover skin burns with dry sterile dressings after decontamination ... . /Poison A and B/
[Bronstein, A.C., P.L. Currance; Emergency Care for Hazardous Materials Exposure. 2nd ed. St. Louis, MO. Mosby Lifeline. 1994. 139]**PEER REVIEWED**

Advanced treatment: Consider orotracheal or nasotracheal intubation for airway control in the patient who is unconscious, has severe pulmonary edema, or is in respiratory arrest. Positive pressure ventilation techniques with a bag valve mask device may be beneficial. Monitor cardiac rhythm and treat arrhythmias as necessary ... . Start an IV with D5W /SRP: "To keep open", minimal flow rate/. Use lactated Ringer's if signs of hypovolemia are present. Watch for signs of fluid overload. Consider drug therapy for pulmonary edema ... . For hypotension with signs of hypovolemia, administer fluid cautiously. Watch for signs of fluid overload ... . Treat seizures with diazepam (Valium) ... . Use proparacaine hydrochloride to assist eye irrigation ... . /Poison A and B/
[Bronstein, A.C., P.L. Currance; Emergency Care for Hazardous Materials Exposure. 2nd ed. St. Louis, MO. Mosby Lifeline. 1994. 139]**PEER REVIEWED**

Animal Toxicity Studies:

Evidence for Carcinogenicity:

Classification of carcinogenicity: 1) evidence in humans: sufficient; 2) evidence in animals: sufficient. Overall summary evaluation of carcinogenic risk to humans is Group 1: The agent is carcinogenic to humans. /From table/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. S7 61 (1987)]**PEER REVIEWED**

The Carcinogen Assessment Group in EPA's Research and Development Office has evaluated cyclophosphamide for carcinogenicity. According to their analysis, the weight of evidence for cyclophosphamide is group C, which is based on inadequate evidence in humans and limited evidence in animals. As a group C chemical, cyclophosphamide is considered a possible human carcinogen.
[USEPA; Methodology for Evaluating Potential Carcinogenicity in Support of Reportable Quantity Adjustments Pursuant to Cercla Section 102 (1986) OHEA-C-073]**PEER REVIEWED**

Non-Human Toxicity Excerpts:

TWO GROUPS OF 10 MALE AND 10 FEMALE, 4 TO 24 WEEK OLD NZB/NZW HYBRID MICE /WHICH DEVELOPED AUTOIMMUNE COMPLEX NEPHRITIS/ WERE GIVEN DAILY SC INJECTIONS OF 1 MG/KG BODY WT OR 8 MG/KG BODY WT CYCLOPHOSPHAMIDE IN 0.1 ML SALINE FOR UP TO 93 WK; 20 MALES AND 20 FEMALES WERE INJECTED WITH SALINE ALONE AND SERVED AS CONTROLS. FIFTY PERCENT OF MALE CONTROLS HAD DIED BY THE 31ST WK OF THE STUDY, COMPARED WITH 41 AND 60 WK FOR THOSE GIVEN THE LOW AND HIGH DOSE LEVELS. FIFTY PERCENT OF MALE CONTROLS HAD DIED BY 57 WK, COMPARED WITH 71 AND 80 WK FOR THE TREATED ANIMALS. TUMORS WERE OBSERVED IN TREATED MALES AFTER 60 WK OF TREATMENT AND IN FEMALES AFTER 40 WEEKS. EIGHT MALES & 9 FEMALES GIVEN THE HIGHEST DOSE LEVEL DEVELOPED NEOPLASMS, INCL 3 GENERALIZED LYMPHORETICULAR NEOPLASMS IN MALES AND 3 IN FEMALES AS WELL AS A POORLY DIFFERENTIATED SARCOMA. 3 SQUAMOUS CELL CARCINOMAS OCCURRED AT THE SITE OF INJECTION IN FEMALES. PULMONARY ADENOMAS WERE ALSO OBSERVED IN 3 MALE AND 1 FEMALE MICE. OF ANIMALS GIVEN THE LOW DOSE LEVEL, 3 MALES AND 1 FEMALE DEVELOPED NEOPLASMS. AMONG CONTROLS 2 MALE AND 1 FEMALE MICE HAD RETICULUM CELL SARCOMAS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 170 (1981)]**PEER REVIEWED**

A GROUP OF 50 FEMALE NMRI MICE, 65 DAYS OLD, RECEIVED 52 WEEKLY SC INJECTIONS OF 26 MG/KG BODY WT (7% OF LD50) CYCLOPHOSPHAMIDE (TOTAL DOSE, 1352 MG/KG BODY WT); ANOTHER GROUP OF 50 FEMALES SERVED AS CONTROLS. THE AVERAGE LIFESPAN OF TREATED AND CONTROL ANIMALS WAS 630 + OR - 130 DAYS. IN THE CONTROL GROUP, 3/46 (6%) MICE DEVELOPED STEM CELL LEUKEMIA AND NO OTHER MALIGNANT TUMOR WAS OBSERVED. OF THE TREATED MICE, 28/46 (61%) DEVELOPED MALIGNANT TUMORS: 3 LEUKEMIAS, 12 MAMMARY CARCINOMAS & 1 OTHER MAMMARY TUMOR, 4 OVARIAN CARCINOMAS, 1 FIBROSARCOMA OF THE THORAX, 1 SKIN CARCINOMA, 2 SARCOMAS @ INJECTION SITE & 4 LUNG TUMORS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 171 (1981)]**PEER REVIEWED**

FOUR GROUPS OF 15 MALE AND 15 FEMALE A/J MICE, 4-6 WK OLD, WERE GIVEN IP INJECTIONS OF CYCLOPHOSPHAMIDE IN WATER 3 TIMES A WK FOR 4 WK (TOTAL DOSES, 420, 135, 34 AND 8 MG/KG BODY WT). OF 165 MALE AND 195 FEMALE CONTROLS INJECTED WITH WATER ONLY, 37% OF MALE AND 27% OF FEMALE SURVIVORS DEVELOPED LUNG TUMORS WITHIN 39 WK, WITH 0.48 AND 0.29 TUMORS/MOUSE. AFTER 39 WK, 4/30, 27/30, 26/30 AND 30/30 ANIMALS WERE STILL ALIVE IN THE RESPECTIVE DOSE GROUPS. AMONG SURVIVING ANIMALS, THE NUMBERS WITH LUNG NEOPLASMS WERE 2/4 (2.5 TUMORS/MOUSE), 20/27 (74%; 1.3 TUMORS/MOUSE), 11/26 (42%; 0.6 TUMORS/MOUSE) AND 12/30 (40%; 0.4 TUMOR/MOUSE, RESPECTIVELY. THE INCIDENCE OF LUNG TUMORS IN TREATED MICE WAS SIGNIFICANTLY GREATER THAN THAT IN CONTROLS ONLY FOR THOSE GIVEN THE SECOND HIGHEST DOSE LEVEL. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 171 (1981)]**PEER REVIEWED**

A GROUP OF 29 DD MICE AND A GROUP OF 25 A MICE OF BOTH SEXES, 4-5 WK OLD, RECEIVED IP INJECTIONS OF 5 MG/KG BODY WT CYCLOPHOSPHAMIDE IN SALINE TWICE WEEKLY FOR 15 SUCCESSIVE WK; 20 AND 16 CONTROL MICE OF EACH STRAIN WERE INJECTED WITH ISOTONIC SALINE ONLY. NEOPLASMS DEVELOPED IN VARIOUS ORGANS IN 12/22 DD MICE THAT SURVIVED MORE THAN 48 WK AFTER THE BEGINNING OF THE TREATMENT; THESE OCCURRED PREDOMINANTLY IN LUNG, LIVER, TESTIS & MAMMARY GLAND. 3 OF 10 CONTROL DD MICE THAT LIVED BEYOND THE SAME PERIOD ALSO HAD NEOPLASMS. NEOPLASMS DEVELOPED IN 6/16 STRAIN A MICE THAT SURVIVED MORE THAN 42 WK AND INCLUDED 6 IN THE LUNG AND 1 IN THE ORBIT. TWO OF 11 CONTROL A MICE HAD NEOPLASMS, BOTH IN THE LUNG. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 171 (1981)]**PEER REVIEWED**

TWO GROUPS, EACH OF 25 MALE AND 25 FEMALE OUTBRED SWISS-WEBSTER-DERIVED MICE, 6 WK OLD, WERE GIVEN IP INJECTIONS OF 12 OR 25 MG/KG BODY WT CYCLOPHOSPHAMIDE 3 TIMES A WK FOR 6 MO. ANIMALS THAT SURVIVED OVER 100 DAYS WERE OBSERVED FOR UP TO 12 FURTHER MO, AT WHICH TIME THEY WERE KILLED. LUNG NEOPLASMS OCCURRED IN 7/30 MALES COMBINED FROM BOTH TREATMENT GROUPS AND IN 10/35 FEMALES; BLADDER PAPILLOMAS WERE FOUND IN 4/30 MALES. THE INCIDENCES OF THE TWO TUMOR TYPES WERE REPORTED TO BE STATISTICALLY GREATER THAN THOSE IN POOLED CONTROLS. THE WORKING GROUP CONSIDERED THAT THE INADEQUATE REPORTING OF CERTAIN ITEMS, SUCH AS SURVIVAL TIMES, THE AMALGAMATION OF VARIOUS EXPERIMENTAL GROUPS AND TUMOR TYPES, AS WELL AS THE LACK OF ADE-ADJUSTMENT IN THE ANALYSES PRECLUDED A COMPLETE EVALUATION OF THIS STUDY. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 171 (1981)]**PEER REVIEWED**

TWO GROUPS, EACH OF 25 MALE AND 25-28 FEMALE CHARLES RIVER CD RATS, 6 WK OLD, WERE GIVEN IP INJECTIONS OF 5 OR 10 MG/KG BODY WT CYCLOPHOSPHAMIDE 3 TIMES A WK FOR 6 MO. ANIMALS THAT SURVIVED OVER 100 DAYS WERE OBSERVED FOR 12 FURTHER MO, AT WHICH TIME THEY WERE KILLED. MAMMARY CARCINOMAS OCCURRED IN 9/53 FEMALES COMBINED FROM BOTH TREATMENT GROUPS AND IN 1/50 MALES, & MAMMARY ADENOMAS OCCURRED IN 24/53 FEMALES. THE INCIDENCE OF ADENOCARCINOMAS IN CONTROL FEMALES WAS 13/181; THE INCIDENCES OF THE TWO MAMMARY TUMOR TYPES WERE REPORTED TO BE INCR TO A STATISTICALLY SIGNIFICANT EXTENT OVER THOSE IN POOLED FEMALE CONTROLS. THE WORKING GROUP CONSIDERED THAT THE INADEQUATE REPORTING OF CERTAIN ITEMS, SUCH AS SURVIVAL TIMES, THE AMALGAMATION OF VARIOUS EXPERIMENTAL GROUPS AND TUMOR TYPES, AS WELL AS THE LACK OF AGE ADJUSTMENT IN THE ANALYSES PRECLUDED A COMPLETE EVALUATION OF THIS STUDY. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 172 (1981)]**PEER REVIEWED**

A GROUP OF 32 MALE SPRAGUE DAWLEY RATS, 3 MO OLD RECEIVED WEEKLY IV INJECTIONS OF 13 MG/KG BODY WT CYCLOPHOSPHAMIDE (TOTAL DOSE, 670 MG/KG BODY WT). A GROUP OF 52 UNTREATED RATS SERVED AS CONTROLS. MALIGNANT TUMORS DEVELOPED IN 14/32 TREATED RATS WITHIN 510 + OR - 90 DAYS: THERE WERE 3 RETICULUM CELL SARCOMAS, 6 HEMANGIOENDOTHELIOMAS IN VARIOUS ORGANS, 1 NEUROGENIC SARCOMA OF MEDIASTINUM, 1 SARCOMA OF THE HEART & 1 LEUKEMIA; TWO RATS HAD 2 MALIGNANT TUMORS. EACH: ONE HAD OSTEOSARCOMA OF PARANASAL SINUS & A PHEOCHROMOCYTOMA, AND THE OTHER HAD AN ANGIOSARCOMA OF THE ABDOMEN AND A PHEOCHROMOCYTOMA. OF THE CONTROLS, 6/52 DEVELOPED MALIGNANT TUMORS WITHIN 670 + OR - 150 DAYS: 3 RETICULUM CELL SARCOMAS, 1 PHEOCHROMOCYTOMA, 1 HEMANGIOSARCOMA OF THE LUNG AND 1 SARCOMA OF THE KIDNEY. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. 26 173 (1981)]**PEER REVIEWED**

A SINGLE IP DOSE OF CYCLOPHOSPHAMIDE CAUSES MARKED NECROSIS OF THE BLADDER AND OF THE TUBULAR AND PELVIC EPITHELIUM IN MICE, RATS, & DOGS; RELATIVELY LITTLE DAMAGE WAS OBSERVED IN LIVER, EVEN AFTER PROLONGED ADMINISTRATION. NECROSIS OF BLADDER TISSUE IS FOLLOWED BY RAPID EPITHELIAL REGENERATION OF DIPLOID CELLS & LATER PRODUCTION OF TETRAPLOID, OCTOPLOID & OCCASIONAL HYPERPLOID CELLS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 143 (1975)]**PEER REVIEWED**

CYCLOPHOSPHAMIDE IS TERATOGENIC IN SEVERAL SPECIES, INCL MICE, RATS, RABBITS, & CHICKENS. IT PRODUCES A VARIETY OF SKELETAL, SOFT TISSUE & OTHER MALFORMATIONS & INCR NUMBER OF RESORPTIONS; THE TYPE AND FREQUENCY OF MALFORMATIONS ARE STRICTLY DOSE & TIME DEPENDENT. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 176 (1981)]**PEER REVIEWED**

CYCLOPHOSPHAMIDE IS ALSO TERATOGENIC IN THE RHESUS MONKEY WHEN GIVEN INTRAMUSCULARLY FOR VARIOUS PERIODS BETWEEN DAYS 25 AND 43 OF PREGNANCY AT DOSES RANGING BETWEEN 2.5 AND 20 MG/KG BODY WT. THE INDUCED ABNORMALITIES INCLUDED CLEFT LIP WITH CLEFT PALATE, EXOPHTHALMUS, A MARKED UNDERDEVELOPMENT OF THE MIDFACIAL BONES AND MENINGOENCEPHALOCELE. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 176 (1975)]**PEER REVIEWED**

Teratogenic effects were induced in outbred mice by treatment of 8 wk old pregnant females with 1 of 5 different doses (5, 10, 20, 30, & 40 mg/kg, ip) of cyclophosphamide. Most malformations were induced with 20, 30, or 40 mg/kg, whereas 5 & 10 mg of cyclophosphamide/kg caused no alterations of the fetuses.
[REZNIK G, HECHT J; ARZNEIM-FORSCH 29 (3): 479 (1979)]**PEER REVIEWED**

TEN PREGNANT FEMALE RABBITS WERE TREATED WITH A DAILY INJECTION OF 50 MG CYCLOPHOSPHAMIDE (DNA SYNTHESIS INHIBITOR), FROM DAY 11 TO DAY 14, WHICH IS A PERIOD THAT PRECEDES FORMATION OF THE FACE. THE CONTROL SAMPLE COMPRISED FIVE FEMALE RABBITS. THE FETUSES WERE OBTAINED BY CESAREAN SECTION ON DAY 28 & STAINED WITH ALIZARIN. SIX OF THE TEN TREATED ANIMALS PRODUCED OFFSPRING THAT HAD TEMPOROMANDIBULAR JOINT SYNOTOSIS (TMJ).
[BACON W; AM J ORTHOD 83 (6): 507-12 (1983)]**PEER REVIEWED**

Pregnant CBA/CA mice were injected subcutaneously with 0, 4, 20, or 40 mg/kg of cyclophosphamide 60 hr after copulation. At each of the doses tested, cyclophosphamide significantly reduced the number of blastocyst cells and caused dose related increase in chromosome aberrations in the blastocysts. Cyclophoshamide increased the number of cells with chromosome breaks at all three doses and also increased chromosome rearrangements in the 20 and 40 mg/kg treated groups. The number of cells with ring chromosomes in the 40 mg/kg group was significantly increased. Cyclophosphamide inhibited the synthesis of DNA and of histones in the 20 and 40 mg/kg groups. On a subsequent culture study, it was observed that treatment of the mothers with 20 or 40 mg/kg, significantly inhibited the in vitro hatching of blastocysts from the zona pellucida. Trophoblast expansion and the attachment of embryos to the glass coverslip were also inhibited.
[Kola I et al; Teratog Carcinog Mutagen 6: 115-27 (1986)]**PEER REVIEWED**

Five groups of C57BL/6J pregnant mice were treated as follows: 1) 1 ug/g daily iv of saline or cyclophosphamide on day 9-12 or 14-17 of gestation (vehicle and drug were given by injection into the tail vein); 2) 5 ug/g iv vehicle or cyclophosphamide on day 12 of gestation; 3) 1, 2.5, or 5 ug/g ip vehicle or cyclophosphamide on day 12 of gestation; 4) 5, 10, or 20 ug/g ip vehicle or cyclophosphamide on day 17 of gestation; and 5) 10 or 20 ug/g ip vehicle or cyclophosphamide on day 17 of gestation. Number of offspring per female at weaning was similar in controls and all groups except for group 2 in which no offspring of treated dams survived. No gross terata were present. No effect on cell mediated or immune function was observed in offsprings of treated dams. The 5 and 9 week old progeny exposed to 20 ug/g on gestational day 17 had reduced body weight. Decreased numbers of antibody forming cells per spleen were found in 8 week old offspring in group 3.
[Luebke RW et al; J Toxicol Environ Health 18: 25-39 (1986)]**PEER REVIEWED**

CYCLOPHOSPHAMIDE ... HAS BEEN TESTED BY INJECTION INTO THE ANTERIOR CHAMBER OF RABBIT EYES, BUT PROVED EXCESSIVELY DAMAGING TO THE CORNEA TO ALLOW ITS USE IN TREATMENT OF EPITHELIAL INVASION OF THE ANTERIOR CHAMBER. HOWEVER, INJECTIONS INTO THE VITREOUS BODY IN RABBITS IN CONCENTRATIONS UP TO 10 MG/ML HAVE BEEN TOLERATED WITHOUT EXCESSIVE INFLAMMATION ... .
[Grant, W.M. Toxicology of the Eye. 3rd ed. Springfield, IL: Charles C. Thomas Publisher, 1986. 299]**PEER REVIEWED**

Cyclophosphamide & two of its metabolites, 4-hydroxycyclophosphamide & phosphoramide mustard were analyzed for their ability to induce sister chromatid exchanges in mouse peripheral blood lymphocytes in vitro & in vivo. In the in vivo experiments each animal received a single ip injection of the cmpd in question at varying doses. In the first experiment on phosphoramide mustard effects, the SCEs/metaphase was 16.04 at a dose of 19.0 uM/kg, the only result significantly different from the control (13.24). In a second experiment, exposure to 50 uM/kg of either cyclophosphamide or phosphoramide mustard induced sister chromatid exchange frequencies of 28.06 & 21.81, compared with the control, 12.02. In the third experiment, both phosphoramide mustard & 4-hydroxycyclophosphamide induced dose dependent incr in sister chromatid exchange frequency (max, about 30 at 150 uM/kg for each cmpd compared with the control of about 10). At equimolar concns of 1 uM, the mean sister chromatid exchange frequency was about 10 for the control & cyclophosphamide, about 21 for phosphoramide mustard, & about 26 for 4-hydroxycyclophosphamide. The in vitro exposures used mononuclear lymphocytes isolated from whole blood pooled from 18 male mice. Lymphocytes were then inoculated into 1 ml of culture media containing 1 uM of either cyclophosphamide phosphoramide mustard, or 4-hydroxycyclophosphamide & incubated for 21 hr. The cells were then washed & the medium replenished, this time without mitogen but containing 5 uM 5-bromo-2'-deoxyuridine.
[Bryant MF et al; Mutat Res 222 (3): 271-7 (1989)]**PEER REVIEWED**

The carcinogenic agent cyclophosphamide was sc admin at 0 (controls), 13, and 26 mg/kg for life to groups of 30 female AKR mice, and to groups of 30 NMRI mice. No symptoms of acute or subacute toxicity were observed. CPA dose-dependently incr the median life span in AKR mice by 27% at 13 mg/kg (from 188 to 238 days) and 76% at mg/kg (to 330 days), and decr the incidence in leukemias by 17% and 37%. In NMRI mice, cyclophosphamide significantly increased the incidence of leukemias by 46% at the low dose and 26% at the high dose, respectively. The number of benign and malignant tumors for the high, low, and control groups were 16, 19, and 4 an 3 for NMRI mice. For AKR mice, the tumor numbers were 22, 27, and 30, respectively. Histologically, malignant tumors of the lymphoproliferative system were found to be lyphocytic leukemias (98%) and the malignant thymomas (2%).
[Petru E et al; Cancer Lett 44 (3): 221-6 (1989)]**PEER REVIEWED**

Virtually all nonobese diabetic/WEHI mice spontaneously develop a lymphocytic infiltration of pancreatic islets (insulitis), but very few progress to diabetes ( < 10% in females and < 1% in males at 220 days of age). Cyclophosphamide was admin to non-obese diabetic/WEHI mice at 0, 50, 100, 150, 200, or 300 mg/kg ip in 200 ul phosphate-buffered saline. Diabetes was produced in both sexes 10 to 16 days after admin. There were no significant changes in body wt, and the mortality was < 5% within 28 days. Diabetes incidence decr with decr doses of cyclophosphamide and with < 100 mg/kg, there is no incr in incidence over controls. Cells in the insulitis lesion were mainly T-lymphocytes with an initial preponderance of L3T4 cells. Cyclophosphamide dramatically depleted splenic cell numbers from a baseline of (1.2 + or - 0.4) x 10+8 to (1.4 + or - 0.5) x 10+7 by day 4. In expt 2, 3 mice of each sex from the strains Biozzi, BALB/c, BALB/c nude, C3H/He, C3H/HeJ, C57BL/6, C57/Bg, C57 nude, DBA/2, CBA/Ca and CBA nude were injected twice at a 14 day interval with 300 mg/kg ip cyclophosphamide. Non-obese diabetic/WEHI mice (19 female and 15 male) received the same treatment and served as controls. No mice were hyperglycemic 14 days after the second dose, except for the non-obese diabetic mice (13 females and 8 males. Normal islets were found in all non-obese diabetic mice. In exp 3, male non-obese diabetic/WEHI mice were given either an organcultured fetal pancreas isograft, or cyclophosphamide followed 3 days later with a pancreas isograft. Beta cell damage and insulitis in the host pancreas were paralleled in the fetal pancreas isograft. Admin of cyclophosphamide to mice 3 days before grafting caused greater graft infiltration and beta cell loss, and in some cases, no beta-cells were present in the graft. In exp 4, 20 normoglycemic female non-obese diabetic/WEHI mice received a 300 mg/kg ip dose of cyclophosphamide and then either given: (1) (n= 12) iv injections at 8, 24, 48, 96, and 168 hr, with 300 uL of mononuclear cell suspension from female non-obese diabetic/WEHI mice; (2) (n= 12) also injected with phosphate-buffered saline/FCS at the same time; (3) (n= 4) injections with cells obtained from acutely diabetic non-obese diabetic mice. The transfer of lymph node and spleen mononuclear cells to non-obese diabetic mice given cyclophosphamide prevented diabetes. The transfer of sufficient lymphoid cells from young (nondiabetic) mice prevented the
[Charlton B et al; Diabetes 38 (4): 441-7 (1989)]**PEER REVIEWED**

To investigate the early ovarian changes after cyclophosphamide treatment, immature rats primed for 48 hr with pregnant mare serum gonadotropin were given injections ip of cyclophosphamide (100 mg/kg) at 1, 2, 4, 16, and 24 hr before decapitation. Serum estradiol dropped significantly after 24 hr of exposure to cyclophosphamide (p< 0.001). Following 16 and 24 hr of cyclophosphamide exposure, the number of granulosa cells expressed from each ovary decr (p< 0.05 and p< 0.01, respectively); the number of nucleated bone marrow cells decr (p< 0.01 and p< 0.01), and their median nuclear size was significantly reduced (p< 0.05 and p< 0.05) as measured by Coulter Counter and C-256 channelyzer; and the mean follicular diameter and the number of follicles with diameters > 300 uM were significantly lower than in control. After 4, 16, and 24 hr of exposure, median granulosa cell nuclear size significantly incr (p < 0.05, p < 0.01, and p < 0.01, respectively), DNA cross-link in granulosa cells, measured by alkaline elution, reached a max at 2 hr of exposure and decr thereafter.
[Ataya KM et al; Cancer Res 49 (7): 1660-4 (1989)]**PEER REVIEWED**

Swiss Webster mice treated orally with cyclophosphamide (1, 2.5 or 5 mg/kg) once daily on gestational days 6 through 18 gave birth to pups which appeared to be normal and the majority of which survived to adulthood. There were no overt signs of maternal toxicity or any changes in maternal body wt gains. Treatment caused a reduction of mean pup weight at birth (1.5 at 5 mg/kg cyclophosphamide vs 1.8 for controls, and an incr in cumulative pup mortality (32/151 at 5 mg/kg cyclophosphamide vs 5/76 for controls). However, pregnancy outcome and mean pup body, spleen, and thymus weights, when measured at 4 weeks of age, were within the control ranges. Hematological profiles, serum immunoglobulin (IgG, IgM) levels and histology of lymphoid tissue (spleen and thymus), assessed at 4 weeks of age, were not affected by the maternal treatment. Treatment with 7.5 mg/kg Cyclophosphamide not only resulted in reduced litter size (5.6 + or - 1.0 vs 12.6 + or - 0.3, but also increased the cumulative pup mortality (71/68 vs 5/76 for controls). With 7.5 mg/kg cyclophosphamide, histopathological changes were observed in the thymus in 2 and 3 week old pups. The morphology of the thymus in 4 week old pups was unremarkable. At the dose of 10 mg/kg, no live births were recorded. Treatment with 7.5 or 10 mg/kg cyclophosphamide resulted in significant reduction in the maternal wt gain, compared with controls.
[Liakopoulou A et al; Res Comm Chem Pathol Pharmacol 64 (2): 241-54 (1989)]**PEER REVIEWED**

The cytostatic agent cyclophosphamide (1X10-5, 10-7 and 10-9 mg/ml) was tested in the initiator tRNA acceptance assay for carcinogens in the presence of 2 concn of microsomal enzymes and NADPH. Treatment of tRNA resulted in a 75% inhibition of its acceptance of L-methionine. Cyclophosphamide also inhibited the charging of unfractionated tRNA from rat liver with L-alanine, L-lysine, L-phenylalanine and L-valine.
[Hradec J et al; Carcinogenesis 10 (8): 1413-7 (1989)]**PEER REVIEWED**

Studies in animals have shown that cyclophosphamide is teratogenic in mice, rats, rabbits, and monkeys given 0.02, 0.08, 0.5, and 0.07 times the human dose, respectively.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

7 to 10 mg/kg were administered to rats and with treatment on the 11th or 12th day the fetuses developed skeletal defects, cleft palates and exencephaly or encephalocele. This compound was shown to be relatively more embryolethal than chloroambucil when the fetal-maternal toxicity ratios of the two were compared. The compound was found to be teratogenic in mice. In the rabbit, a high incidence of cleft lip and-or palate and reduction defects of the extremities using intravenously 30 mg/kg on single days 11, 12 or 13 was found. In the rhesus monkey, 10 mg/kg on days 27 through 29 produced facial clefts and when given on days 32 through 40, meningoencephalocele was observed.
[Shepard, T.H. Catalog of Teratogenic Agents. 5th ed. Baltimore, MD: The Johns Hopkins University Press, 1986. 159]**PEER REVIEWED**

A number of studies of the metabolism of cyclophosphamide & its products in in vitro cultures with rat embryos have shown that the cmpd must be bioactivated by a liver monofunctional oxygenase system in order to be teratogenic. The morphologic changes found in vitro were very similar to those seen in vivo. Phosphoramide mustard in equimolar doses caused effects similar to those of bioactivated cyclophosphamide in vitro & when given intraamnioticaly. Acrolein was toxic but its effect was difficult to assess because of protein binding. The other stable metabolite, 4-ketocyclophosphoramide, was only weakly teratogenic in vitro. /It was/ concluded that phosphoramide mustard was the active teratogenic metabolite in a mouse blastocyst system. The monofunctional form of phosphoramide mustard (with only one chloroethyl side chain) has been shown to have the same embryotoxicity as cyclophosphamide.
[Shepard, T.H. Catalog of Teratogenic Agents. 5th ed. Baltimore, MD: The Johns Hopkins University Press, 1986. 159]**PEER REVIEWED**

1.4, 3.4 or 5.1 mg/kg were administered daily before mating to male rats. On the day of mating the males were not treated. Minimal changes in the male reproductive tract were found but malformations and retardation of growth were found in the offspring of the untreated females they bred with. There was a dose-dependent increase in resorptions and fetal deaths. In the offspring of males treated at 7-9 weeks there were 4 defects in 57 compared to one in 254 of the controls. The defects were hydrocephalus, micrognathia and edema. Growth retardation occurred in 7% of the fetuses in this group.
[Shepard, T.H. Catalog of Teratogenic Agents. 5th ed. Baltimore, MD: The Johns Hopkins University Press, 1986. 159]**PEER REVIEWED**

When used clinically, the important side effects of cyclophosphamide are bone marrow suppression, with both leukopenia & thrombocytopenia. Nausea & vomiting are rare. Sterile necrotizing hemorrhagic cystitis has been associated with chronic admin & is a cause for stopping therapy. To decr the incidence of this cystitis, which is manifested by bloody urine, the drug should be administered in the morning & animals should be encouraged to urinate frequently. Alopecia occurs occasionally in dogs with continuous hair growth (eg, Poodles, Old English Sheepdogs).
[Booth, N.H., L.E. McDonald (eds.). Veterinary Pharmacology and Therapeutics. 5th ed. Ames, Iowa: Iowa State University Press, 1982. 789]**PEER REVIEWED**

Treatment of male rats with low dosages of cyclophosphamide causes a dramatic incr in early embryo death among their progeny without significantly affecting the general health of the male. It is hypothesized that cyclophosphamide exerts its effects by targeting specific components of spermatozoal nuclei. The purpose of the present studies was to investigate the effects of chronic cyclophosphamide treatment on spermatozoal DNA. Two approaches were pursued. The first was to determine total DNA damage by using the alkaline elution method. The second was to study spermatozoal DNA template function by using an in vitro DNA synthesis system. Adult male rats were treated with saline or cyclophosphamide (6.1 mg/kg/day) daily for 1 or 6 wk. Cauda epididymal spermatozoa were collected & subjected to alkaline elution using DNA-DNA dot hybridization to quantify the fractionated DNA. One week of treatment with cyclophosphamide caused DNA single strand breaks that could be detected only in the presence of proteinase K in the lysis soln; no DNA cross-links were observed in the animals that received l-wk drug treatment. In contrast, 6 wk of treatment with cyclophosphamide induced a significant incr in both DNA single strand breaks & cross-links in spermatozoal nuclei; the cross-links were attributable primarily to DNA-DNA linkages. The availability of spermatozoal DNA for template function was not affected by 1 wk of treatment with cyclophosphamide but was markedly affected after 6 wk of treatment with this drug. It is proposed that during chromatin transition processes the male genome may be in an open dynamic state with many exposed sites that are vulnerable to alkylating agents. Since there is no DNA repair during spermiogenesis, damage to the genome by alkylation at this stage may be cumulative, resulting in the production of dysfunctional germ cells.
[Qiu J et al; Biol Reprod 53 (6): 1465-73 (1995)]**PEER REVIEWED**

Exposure of the male germ cell to cyclophosphamide during spermatogenesis and sperm maturation can interfere with development of the embryo. When male rats were treated with a chronic low dose of cyclophosphamide for 4 wk there was a dramatic increase in early postimplantation loss in their progeny, characterized by implantation sites selectively lacking in embryonic tissues. The present study was designed t determine the earliest appearance of a paternal effect of cyclophosphamide treatment and to examine whether the embryonic lineage was selectively affected. Male Sprague-Dawley rats were orally dosed for 4-5 wk with saline or 6 mg/kg per day of cyclophosphamide; their progeny were obtained on Days 2, 2.5, 3, 4, and 4.5 of gestation. Paternal cyclophosphamide treatment had no effect on the mean number of embryos per pregnant female. However, as early as Day 3 of gestation, there was a significant decrease in cell number among the embryos sired by cyclophosphamide-treated males, increasing to a greater than 50% decrease in cell number by Day 4. The cell doubling time in embryos sired by treated males (16 hr) was longer than that of controls (12 hr). This decreased proliferation rate was confirmed by a dramatic decrease in the capacity of both Day 3 and Day 4 embryos sired by cyclophosphamide-treated males to incorporate (3)H-thymidine over a 26-hr culture period. Cytogenetic analysis in a limited number of blastomeres entering metaphase revealed no evidence of chromosomal abnormalities. Both the trophectoderm and the inner cell mass cells were proportionally decreased in Day 4.5 embryos sired by cyclophosphamide-treated males. Thus, paternal cyclophosphamide exposure affected both cell lineages in the conceptus as early as Day 3 of gestation.
[Austin SM et al; Biol Reprod 50 (1): 55-64 (1994)]**PEER REVIEWED**

A study of cyclophosphamide (CP)-induced DNA damage and repair occurring in vivo was conducted in the brown Norway rat myelocytic leukemia (BNML) model. DNA single-strand breaks (SSB), DNA-DNA interstrand cross-links (DIC), DNA-protein cross-links (DPC), and DNA double-strand breaks (DSB) were measured by alkaline and neutral elution. After ip injection of 50 ng/kg CP, DIC were detectable at 1 hr and peaked at 8 hr. DPC were detectable at 2 hr and peaked at 6 hr. Both DIC and DPC persisted at a relatively high level until 28 hr. Dose-response curves for both DIC and DPC were determined at 4 hr after CP injection over the dose range of 25-150 mg/kg. These doses ranged from the minimally effective dose to doses curative for rats bearing this leukemia (1- to 9-log kill of leukemia cells). No SSB or DSB was observed at 4 hr after CP injection over the dose range of 15-250 mg/kg, but a low level of SSB was observed at 18-28 hr after CP treatment. These data suggest that the cytotoxic effect of CP in vivo is mediated mostly by DIC and DPC. SSB appearing late after CP injection in vivo may be a reflection of repair of DIC and DPC and an indication of the optimal timing for administration of DNA-repair inhibitors. This observation is of interest since our earlier work demonstrated that hydroxyurea can potentiate the therapeutic benefit of CP in this model when it is given over the 4-day period immediately after CP treatment.
[Wang JY et al; Cancer Chemother Pharmacol 31 (5): 381-6 (1993)]**PEER REVIEWED**

Strain differences in cytochrome P450 (P450) expression were investigated in Sprague-Dawley (SDs) compared with Fischer 344s (F344s) rats after admin of cyclophosphamide (CPA). Animals received a single dose of CPA with sacrifice occurring 6 days post-treatment. At 130 mg/kg, male F344s displayed a greater sensitivity to CPA, as evidenced by a 68% loss of total hepatic microsomal P450 compared with only 35% in SDs. The most dramatic change in P450 was the loss of 2C11 (84% in F344s, 52% in SDs). In the SD, individual rat 2C11 activity was correlated (r sq=0.76), with the level of plasma thyroxine in that animal. In male F344s admin CPA at 50 mg/kg, 43 & 44% losses in 2C11 activity (P<0.05) & thyroxine (P<0.01), respectively, were observed, whereas activities characteristic of P450s 2C11, 3A2, 2A2, 2C6 & 2E1/1A2 were unaffected in SDs at this dose. CPA also produced suppression of P450 in female SDs, including female-specific 2C12. Correlation was observed between the loss of P450 expression & change in body weight after treatment in both male & female animals, suggesting that CPA downregulated P450 expression secondary to decr caloric intake. The anorectic effect of CPA is believed to result from potent CNS stimulation, accompanied by a state of adaptive hypothyroidism.
[Kraner JC et al; J Pharmacol Exp Ther (276) 1: 258-64 (1996)]**PEER REVIEWED**

CP /cyclophosphamide/ decreased the activity of the female rat hepatic enzymes 2A1, 2C6 &/or 2C12 & 2E1, NADPH-P450 oxidoreductase & 17 beta-oxidoreductase & the pulmonary enzyme 2B, 7 days after its admin. The decr in the activity of the enzymes 2E1 & NADPH-P450 oxidoreductase were accompanied by a corresponding change in the amt of enzyme protein indicating that the alteration in expression of these enzymes occurred via changes in transcription &/or translation or protein degradation ... CP also impaired its own activation 7 days after its admin to the female rat ... The change in female enzyme profile was accompanied by a reduction in the hormones oestradiol, T4 & T3 7 days after CP admin ... Despite an apparent trend for an incr in activity on day 5, a decr on day 8 & a subsequent incr on day 11, repeat doses of CP to the male rat generally did not alter the P450 isoforms 2A2, 2B1, 2C11, 2E1 & 3A2 or 17 beta-oxidoreductase, NADPH-P450 oxidoreductase & steroid 5 alpha-reductase ... Chronic admin of CP to the male rat significantly reduced erythromycin demethylase & NADPh-P450 oxidoreductase 8 days following commencement of dosing & significantly incr statistically significant incr in pulmonary 2B 5 days following commencement of dosing ... Plasma testosterone & TSH were unchanged following repeated dosing with CP while T3 was significantly decr on days 5, 8 & 11 & T4 was significantly decr on day 8.
[Angley MT et al; Xenobiotica 25 (10): 1051-62 (1995)]**PEER REVIEWED**

Paracoccidioidomycosis is an endemic fungal disease widely distributed throughout Latin America. The potent immunosuppressor cyclophosphamide (CY) has been used to modulate host immune response to Paracoccidioides brasiliensis in an experimental model. Inbred male Buffalo/Sim rats weighing 250-300 g were inoculated with 5X10+6 P. brasiliensis cells of the yeast phase form by intracardiac route. One group of animals was treated with 20 mg/kg body weight at days +4, +5, +6, +7, +ll and +l2 post-infection, while a control group was infected alone. No mortality was recorded in either group. Treated rats presented: a) a decrease in granuloma size, which contained less fungal cells; b) a lack of specific antibodies up to 35 days post-infection, and c) a significant increase in the footpad swelling test (DTH) against paracoccidioidin. Splenic cell transfer from CY-treated P. brasiliensis-infected donors to recipients infected alone led to a significant increase in DTH response in the latter versus untreated infected controls. Likewise, in treated infected recipients transferred with untreated infected donor spleen cells, footpad swelling proved greater than in controls. Thus, it would seen that each successive suppressor T lymphocyte subset belonging to the respective cascade may be sensitive to repeated CY doses administered up to 12 days post-infection. Alternatively, such CY schedule may induce the appearance of a T cell population capable of amplifying DTH response.
[Blejer JL et al; Rev Inst Med Trop Sao Paulo 37 (3): 219-24 (1995)]**PEER REVIEWED**

Liver microsomes were obtained from male Hooded Wistar rats admin a single dose (ip) of saline or cyclophosphamide (200 mg/kg). Rats receiving cyclophosphamide (CP) were killed 1, 4, 7, 10 or 14 days after CP admin. The O-demethylation of dextromethorphan to dextrorphan was used to monitor 2D1 activity ... The mean Vmax for dextrorphan formation was reduced significantly (p < 0.0001) 7, 10 and 14 days after CP admin compared with the control group (control, 0.32 + or - 0.07; 7-day, 0.20 + or - 0.08; 10-day, 0.11 + or - 0.02; and 14-day group, 0.15 + or - 0.02 nmol/mg/min) ... Western blotting revealed that there was a significant reduction (p < 0.0005) in the microsomal relative 2D1 content 10 days after CP admin compared with the control group (control, 1.25 + or - 0.44; and 10-day group, 0.65 + or - 0.14) ... The activity of reduced nicotinamide adenine dinucleotide phosphate P450 reductase was significantly reduced (p < 0.0001) 7, 10 and 14 days following CP admin (control, 215 + or - 24; 7-day, 102 + or - 20; 10-day, 59 + or - 4 and 14-day group, 76 + or - 8 nmol/mg/min). Cytochrome b5 content was significantly reduced (p < 0.0001) 7 and 10 days following CP admin (control, 0.46 + or - 0.13; 7-day, 0.28 + or - 0.07 and 10-day group, 0.20 + or - 0.03 nmol/mg) ... The significant reductions in the activity or rat hepatic microsomal 2D1 following CP admin, as seen by the alterations in mean Vmax for dextrorphan formation, do not appear to be due to a single factor, but may result from a combo of several events, incl reductions in relative 2D1 content, reduced nicotinamide adenine dinucleotide phosphate P450-reductase activity and cytochrome b5 content.
[Laslett TJ et al; Xenobiotica 25 (10): 1031-9 (1995)]**PEER REVIEWED**

The testicular toxicity of cyclophosphamide (Cp) in rats was evaluated by quantitative morphometry of spermatogenic cycle stages. Nine-week-old male Sprague-Dawley rats in Group 1 were given a single oral administration of 100 mg/kg of Cp, and were sacrificed at 1, 7, 14 and 21 days thereafter. Rats in Group 2 were orally given 100 mg/kg/day of Cp for 2 days, followed by 50 mg/kg/day for the next 3 days, and were sacrificed at 1 and 4 days after the last administration. The numbers of seminiferous epithelia were counted in the seminiferous tubules of stages II, V, VII and XII of the spermatogenic cycle. The data were expressed as numbers of spermatogenic cells per Sertoli cells per seminiferous tubule cross section. Animals in Group 1 showed decreased preleptotene spermatocytes at Day 7, decreased zygotene spermatocytes at Day 14, and decreased pachytene spermatocytes at Day 21. In group 2, testicular toxicity could also be clearly detected by this morphometric approach. The present morphometric study thus indicates that testicular toxicity can be detected from Day 7 even after a single administration of Cp.
[Matsui H et al; J Toxicol Sci 20 (4): 407-14 (1995)]**PEER REVIEWED**

As a first step in developing a potentially more sensitive assay, micronucleus induction by cyclophosphamide (CP) was assessed in an in vivo/in vitro system using rat bone marrow and spleen cells. In each of two independent experiments, two rats/dose were treated i.p. with 0, 20, or 40 mg CP/kg and killed 6 hr later. Cultures were then established in the presence of growth stimulants (interleukin-3 and granulocyte-macrophage colony stimulating factor for bone marrow; lipopolysaccharide and concanavalin A for spleen) and cytochalasin B, a cytokinesis inhibitor. Bone marrow cells were harvested and slides prepared 24 hr after initiation, while spleen cells were harvested at 48 hr. One thousand cells/tissue/group were scored for cell cycle kinetics and 1000 binucleate (BN) cells were scored for micronuclei. In addition, spleen cells were concurrently assayed for chromosome aberrations. A dose-related cell cycle delay was observed in both tissues in both experiments. Bone marrow showed a 6% average background frequency of micronucleated BN cells, while the low dose induced an average of 20%, and the high dose 31%. For spleen, the average control frequency of micronucleated BN cells was 3%, the low dose induced a 40% average frequency, and the high dose 65%. Also in splenocytes, a dose-dependent incr in chromosome aberrations was observed, with an almost 40-fold incr observed over the control value at the high dose.
[Moore FR et al; Mutat Res 335 (2): 191-9 (1995)]**PEER REVIEWED**

Cyclophosphamide is a cyclic phosphamide derivative of mechlorethamine that requires metabolic activation by the cytochrome p450 oxidation system in the liver. Cyclophosphamide is given PO or IV, and dose limiting leukopenia associated with bone marrow suppression is the primary toxicity. Sterile hemorrhagic cystitis caused by acrolein, a metabolite of cyclophosphamide, can occur and should be treated by active diuresis and intravesicular administration of N-acetyleysteine. Mesna, a drug that acts to detoxify metabolites of cyclophosphamide, has been used in human medicine to preclude hemorrhagic cystitis.
[Aiello, S.E. (ed). The Merck Veterinary Manual. 8th ed. Merck & Co., Inc., National Publishing Inc., Philadelphia, PA. 1998. 1835]**PEER REVIEWED**

Alkylating agents are cytotoxic and kill rapidly dividing neoplastic and normal cells and have drastic effects on cells of the immune system. For example, CY at high doses (300 mg/kg) can deplete mice of their T and B lymphocytes ... . At lower doses (50-100 mg/kg), CY transiently depletes B but not T cells in mice ... . Compensatory responses result in twice the normal number of lymphocyte in spleens of mice 12-15 days following treatment, whereas normal numbers return by day 30. CY can also reduce macrophage and NK numbers and function ... . /Alkylating agents/
[Foye, W.O. (ed.). Cancer Chemotherapeutic Agents. ACS Professional Reference Book. Washington, D.C.: American Chemical Society, 1995. 468]**PEER REVIEWED**

There is a need for a rapid assay to identify agents that damage mitochondria because the mitochondrion may be an important target for numerous environmental mitotoxins. Certainly at least one chemotherapeutic regimen (CHOP therapy) that includes doxorubicin can induce cardiomyopathy through mitochondrial genotoxicity in cardiac muscle cells. Yeast cells (1.5 x 10(6)-10(7)) in water are spread on a YEPD plate, and, when the suspension of cells has dried, a small well (12 mm diameter) is cut into the agar; 200-400 microl of a solution of the presumptive mitochondrial genotoxin is placed in the well, and the plates are incubated for 2 days. The genotoxin forms a concentration gradient through the agar and affects the growing cells. An overlay containing tetrazolium chloride is added, and the plates are incubated for 6-24 hr. Respiring cells turn red, and nonrespiring cells, with damaged DNA or inhibited respiratory chains, that are adjacent to the well, are white. A white ring, or a more lightly colored red ring, around the well indicates the presence of cells with lowered respiratory activity which may be fully reversible when the mitochondrial genotoxin is removed. In preliminary experiments, doxorubicin (= adriamycin) shows strong activity with this assay; cyclophosphamide is negative, and 4-hydroxycyclophosphamide, a metabolite of cyclophosphamide, is weakly positive. Ethidium bromide, methotrexate, 5-fluorouracil, and 5-fluorocytosine also are mitochondrial genotoxins. Antifungal agents similar to 5-fluorocytosine and anthelmintic compounds such as pyrvinium iodide can be powerful mitochondrial genotoxins.
[Barclay BJ, et al; Environ Mol Mutagen 38 (2-3): 153-158. 2001.]**PEER REVIEWED**

In a previous study, we showed that soluble low-molecular-mass tumor-associated antigens (sTAA) promote the anti-tumor effect of the anticancer drug cyclophosphamide (CPA) on rat mammary carcinogenesis. In this report, we analyzed the underlaying mechanisms. Studies were performed on the spleen and lymph nodes from the following groups of mammary tumor-bearing rats: i) control rats, ii) rats treated with sTAA, iii) rats treated with CPA, iv) rats treated with CPA and sTAA. Different zones of the spleen and lymph nodes were measured and their T cell content (CD4+ and CD8+ cells) was analyzed immunohistochemically. CPA decreased the size and cell content of follicles, splenic areas related to the production of B cells, of the marginal zone and to a lesser extent of the periarterial lymph sheath, and decreased the number of CD4+ and, at a lower rate, of CD8+ T cells in the spleen. Addition of sTAA restored activity in the splenic zones producing these cells. Similar effects of CPA and sTAA were found in lymph nodes with accumulation of B lymphocytes in the primary and secondary follicles and of T lymphocytes, including both CD4+ and CD8+ cells, in the paracortical zone. We suggest that inhibition of the functional activity of the immune system is one of the main reasons for the toxic effects of chemotherapeutic drugs such as CPA and that the tumor-suppressive antitoxic effects of sTAA result from their activation of B- and T-lymphocyte production in this system, particularly in the spleen and lymph nodes.
[Ben-Hur H, et al; Int J Mol Med 9 (3): 311-316 (2002)]**PEER REVIEWED**

Trypanosoma cruzi-infected juvenile rats develop severe cardiac sympathetic denervation in parallel with acute myocarditis. This aspect has not been studied in adult rats, thought to be resistant to this infection. The mechanism involved in T. cruzi-induced neuronal damage remains to be completely elucidated. In juvenile rats, the mortality during the acute phase depends on T. cruzi populations, ranging from 30% to 100%. Therefore, studies of mechanisms through hazardous procedures such as immunosuppression are restricted. The current paper shows that adult rats infected with T. cruzi (Y strain) develop severe acute myocarditis and cardiac sympathetic denervation, despite null mortality and virtual absence of patent parasitaemia followed by negative haemoculture. Recovery from the myocarditis and denervation occurred but PCR studies showed persistence of parasite DNA at least until day 111 post inoculation. Immunosuppression by cyclophosphamide treatment increased the parasitaemia, prevented the acute myocarditis and the sympathetic denervation without significant alteration of the myocardial parasitism. These results argue against a direct role for parasite-derived products and implicate the inflammatory cells in the denervation process. As previous studies in juvenile animals have discarded an essential role for radiosensitive cells, the macrophages remain as the possible effectors for the T. cruzi-induced neuronal damage.
[Guerra LB, et al; Trans R Soc Trop Med Hyg 95 (5): 505-509. 2001.]**PEER REVIEWED**

Cyclophosphamide (Cy) is an alkylating agent widely used in cancer chemotherapy. It has a bimodal effect on the immune system, depending on the dose and schedule of administration. We have previously demonstrated that a single low dose of Cy has an antimetastatic effect, achieved through immunomodulation, in lymphoma bearing rats. Such a treatment reduced the splenic production of IL-10, TGF-beta, and NO, restoring the lymphoproliferative capacity. A shift from immunosuppression to immunopotentiation induced by low-dose Cy treatment was mainly mediated by a decrease in IL-10 production. The present study focused on the analysis of the modulation of type-1 cytokine levels by treatment with a single low dose of Cy and the effect these cytokines (IL-2 and IFN-gamma) and IL-10 have on primary tumor and metastatic cell growth. Our results suggest that a single low dose of Cy induces a Th2/Th1 shift in the cytokine profile of lymphoma-bearing rats, which may be responsible for its antimetastatic effect. A direct action of IL-10 as a growth factor and IFN-gamma as a cytotoxic factor on metastatic cells is also shown.
[Matar P, et al; Cancer Immunol Immunother 50 (11): 588-596 (2002)]**PEER REVIEWED**

ICA69 (islet cell Ag 69 kDa) is a diabetes-associated autoantigen with high expression levels in beta cells & brain. Its function is unknown, but knockout of its Caenorhabditis elegans homologue, ric-19, compromised neurotransmission. We disrupted the murine gene, ica-1, in 129-strain mice. These animals aged normally, but speed-congenic ICA69(null) nonobese diabetic (NOD) mice developed mid-life lethality, reminiscent of NOD-specific, late lethal seizures in glutamic acid decarboxylase 65-deficient mice. In contrast to wild-type and heterozygous animals, ICA69(null) NOD congenics fail to generate, even after immunization, cross-reactive T cells that recognize the dominant Tep69 epitope in ICA69, and its environmental mimicry Ag, the ABBOS epitope in BSA. This antigenic mimicry is thus driven by the endogenous self Ag, and not initiated by the environmental mimic. Insulitis, spontaneous, and adoptively transferred diabetes develop normally in ICA69(null) NOD congenics. Like glutamic acid decarboxylase 65, ICA69 is not an obligate autoantigen in diabetes. Unexpectedly, ICA69(null) NOD mice were resistant to cyclophosphamide (CY)-accelerated diabetes. Transplantation experiments with hemopoietic and islet tissue linked CY resistance to ICA69 deficiency in islets. CY-accelerated diabetes involves not only ablation of lymphoid cells, but ICA69-dependent drug toxicity in beta cells that boosts autoreactivity in the regenerating lymphoid system.
[Winer S, et al; J Immunol 168 (1): 475-482 (2002)]**PEER REVIEWED**

The selective cytotoxic effect of CY on the different T and B cell subsets results in modulation of the immune response in ... animals. The effect of these agents on nucleic acid synthesis led initial investigators to classify them as immunosuppressants. The surprising finding of Maguire and Ettore that CY augmented guinea pig immune response to contact sensitizers compelled many investigators to test CYinduced immune stimulation in their systems. CY can suppress antibody formation against a variety of antigens when given 2-3 days after immunization. Similarly, when administered after the antigen, CY can also suppress T cell mediated immunity generated against agents producing contact sensitivity allografts and tumors. However, CY administration prior antigen stimulation results in augmented T cell response against contact sensitizing agents and hapten modified syngenetic cells. Under certain conditions, CY can augment T cell mediated antitumor immunity and facilitate adoptive transfer of antitumor immunity. CY, when administered just before or just after tumor implantation, induces complete regression of a CY resistant murine lymphoma growing in normal immunocompetent host. This regression was immunologically mediated because equivalent CY doses have no effect on the growth of this tumor in T cell deficient mice. ... The most likely mechanism by which CY augments immune responses relates to preferential elimination of suppressor and relative sparing of effector and helper cells. Thus, precursors and mature murine suppressor cells are very sensitive to CY whereas the mature effector cells are relatively insensitive. CY induced immunological regression of murine leukemia is reversed by the infusion of normal spleen cells as a source of precursors of suppressor cells. Memory and helper T cells are relatively resistant to the cytotoxic effect of CY. NK activity against YAC lymphoma targets by non T and non B cells is depressed by CY. Melphalan augments antitumor immunity in a fashion similar to CY and increases ADCC. Nitrosoureas (BCNU) have been shown to inhibit ADCC activity.
[Foye, W.O. (ed.). Cancer Chemotherapeutic Agents. ACS Professional Reference Book. Washington, D.C.: American Chemical Society, 1995. 469]**PEER REVIEWED**

It appears that hepatic damage is minimized by these secondary reactions, whereas significant amounts of the active metabolites, such as 4-hydroxycyclophosphamide & its tautomer, aldophosphamide, are transported to the target sites by the circulatory system. In tumor cells, the aldophosphamide cleaves spontaneously, generating stoichiometric amounts of phosphoramide mustard & acrolein. The former is believed to be responsible for antitumor effects. The latter compound may be responsible for the hemorrhagic cystitis seen during therapy with cyclophosphamide.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

Non-Human Toxicity Values:

LD50 Rat oral 160 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Rat ip 40 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Rat sc 144 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Rat iv 148 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Mouse oral 137 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Mouse sc 200 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Mouse iv 140 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

LD50 Mouse parenteral 315 mg/kg
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 972]**PEER REVIEWED**

Ongoing Test Status:

The NTP Toxicology Research and Testing Program releases a Management Status Report on a quarterly basis. This report gives the status of chemicals studied, under study, or proposed for study by NTP. The 07/11/2001 issue indicates that the prechronic study for cyclophosphamide monohydrate is completed, and the chemical is in review for further evaluation. Route: gavage; Species: transgenic model evaluation, mice. /Cyclophosphamide monohydrate/
[NTP; Division of Toxicology Research and Testing; Management Status Report; 07/11/2001; p.21]**PEER REVIEWED**

The NTP Toxicology Research and Testing Program releases a Management Status Report on a quarterly basis. This report gives the status of chemicals studied, under study, or proposed for study by NTP. The 07/11/2001 issue indicates that the prechronic study for cyclophosphamide monohydrate is completed, and the chemical is in review for further evaluation. Route: topical; Species: transgenic model evaluation, mice. /Cyclophosphamide monohydrate/
[NTP; Division of Toxicology Research and Testing; Management Status Report; 07/11/2001; p.21]**PEER REVIEWED**

TSCA Test Submissions:

Cyclophosphamide (CAS # 50-18-0) was evaluated for chromosomal effects. The test substance was examined in an in vitro cytogenetic assay with Chinese hamster ovary (CHO) cells with and without S-9 metabolic activation. It was determined that the test substance can be detected as a promutagen efficiently using this method. No further information was available due to the poor reading quality of the document.
[PROCTER & GAMBLE CO; Evaluation of an In Vitro Cytogenetic Assay with Chinese Hamster Ovary Cells on Seven Compounds; 04/19/82; EPA Doc No. 86-870001351; Fiche No. OTS0515512] **UNREVIEWED**

Metabolism/Pharmacokinetics:

Metabolism/Metabolites:

... /Cyclophosphamide/ is activated by the hepatic cytochrome P450 system. Cyclophosphamide is first converted to 4-hydroxycyclophosphamide, which is in a steady state with the acyclic tautomer aldophosphamide. In vitro studies with human liver microsones & cloned P450 isoenzymes have shown that cyclophosphamide is activated by the CYP2B group of P450 isoenzymes... . 4-hydroxycyclophosphamide may be oxidized further by aldehyde oxidase either in liver or in tumor tissue & perhaps by other enzymes, yielding the metabolites carboxyphosphamide & 4-ketocyclophsphamide, neither of which possesses significant biological activity. It appears that hepatic damage is minimized by theses secondary reactions, whereas significantl amoutns of the active metabolies, such as 4-hydroxycyclophosphamide & its tautomer, aldophosphamed, are transported to the target sites by the circulatory system. In tumor cells, the aldophosphamide cleaves spontaneously, generating stoichiometric amounts of phosphoramide mustard & acrolein. The former is believed to be responsible for antitumor effects. The latter cmpd may be responsible for the hemorrhagic cystitis seen during therapy with cyclophosphamide. Cystitis can be reduced in intensity or prevented by the pareneteral admin of mesna, a sulfhydryl cmpd that reacts readily with acrolein in the acid environment of the urinary tract. ... Urinary & fecal recovery of unchanged cyclophosphamide is minimal after iv admin. Maximal concns in plasma are achieved 1 hr after oral admin, & the half-life in plasma is about 7 hr.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

SHEEP WERE ORALLY DOSED WITH CYCLOPHOSPHAMIDE. IN COLLECTED URINE, 2 METABOLITES WERE OBSERVED AND CHARACTERIZED AS O-(2-CARBOXYETHYL)-N,N-BIS (2-CHLOROETHYL)PHOSPHORODIAMIDATE & 2-(BIS (2-CHLOROETHYL)AMINO)TETRAHYDRO-2H-1,3,2-OXAZOPHOSPHORINE 2,4-DIOXIDE (4-KETOCYCLOPHOSPHAMIDE).
[Menzie, C. M. Metabolism of Pesticides, An Update. U.S. Department of the Interior, Fish, Wild-life Service, Special Scientific Report - Wildlife No. 184, Washington, DC: U.S. GovernmentPrinting Office, l974. 119]**PEER REVIEWED**

A REACTIVE METABOLITE, N,N-BIS-(2-CHLOROETHYL)PHOSPHORODIAMIDIC ACID, WHICH POSSESSES POTENT ALKYLATING & CYTOTOXIC PROPERTIES, HAS RECENTLY BEEN ISOLATED FROM THE OXYGENATION PRODUCTS OF CYCLOPHOSPHAMIDE AND MOUSE LIVER MICROCHROMOSOMES.
[The Chemical Society. Foreign Compound Metabolism in Mammals Volume 3. London: The Chemical Society, 1975. 473]**PEER REVIEWED**

Cyclophosphamide is well absorbed orally, and peak plasma levels appear about one hour after oral use. It is also administered intravenously. This drug is metabolized in the liver to the cytotoxic metabolite, 4-hydroxycyclophosphamide, which is in equilibrium with the acyclic tautomer, aldophosphamide. Although the major fraction of these metabolites is oxidized further to inactive products, some aldophosphamide is converted to phophoramidemustard, which alkylates DNA, and to acrolein.
[American Medical Association, Council on Drugs. AMA Drug Evaluations Annual 1994. Chicago, IL: American Medical Association, 1994. 2012]**PEER REVIEWED**

Acrolein is the metabolite of cyclophosphamide (CP) believed to be involved in the bladder toxicity associated with this anticancer drug. The mechanism by which this extremely reactive intermediate is delivered to the bladder is not known. Glutathione (GSH) readily conjugates with acrolein, and the acrolein mercapturate 5-(3-hydroxypropyl)-N-acetylcysteine (3-hydroxy-PrMCA) has been found in the urine of animals and man given CP. The objectives of this study were to prepare and characterize synthetic standards of the GSH acrolein adduct (3-oxopropyl)glutathione (3-oxoPrGSH), the acrolein mercapturates S-(3-oxopropyl)-N-acetylcysteine (3-oxoPrMCA) and 3-hydroxyPrMCA, and the S-oxidation product of 3-oxoPrMCA (3-oxoPrMCA S-oxide). In addition, the release of acrolein from, and the bladder toxicity of, these conjugates was determined. 3-OxoPrGSH and 3-oxoPrMCA were prepared with a 99% yield by condensing acrolein with GSH and N-acetylcysteine, respectively.
[Ramu K et al; Chem Res Toxicol 8 (4): 515-24 (1995)]**PEER REVIEWED**

An important feature of cytochrome P450 (CYP) 2B1 is its high ability to convert the prodrug cyclophosphamide (CPA) to therapeutically cytotoxic metabolites, resulting in interstrand DNA-cross-linking & cell death. We have examined whether & how the phosphorylation of CYP2B1 influences CPA metabolic activation in vitro & in vivo. We found first that only part of the total CYP2B1 pool undergoes phosphorylation. This part is fully inactivated. Second, phosphorylation of CYP2B1 in intact hepatocytes reduced by up to 75% toxification of CPA to mutagenic metabolites (totally dependent on the same preferentially CYP2B-catalyzed 4-hydroxylation of CPA as is the generation of highly cytotoxic species). Third, the phosphoacceptor-serine 128 of CYP2B1 in the consensus sequence for interaction with the protein kinase A represents an on/off switch for the activation of CPA depending on the phosphorylation conditions in the cell. Fourth, evidence is presented that the above-described events also occur in vivo. In conclusion, a successful therapy with CPA, helped by forced expression of CYP2B1 in tumor cells (as recently proposed) will, in addition, be profoundly modified by its phosphorylation status.
[Oesch-Bartlomowicz B, et al; Int J Cancer 94 (5): 733-742 (2001)]**PEER REVIEWED**

Cyclophosphamide (CPA), a widely used oxazaphosphorine anti-cancer prodrug, is inactive until it is metabolized by cytochrome P450 to yield phosphoramide mustard and acrolein, which alkylate DNA and proteins, respectively. Tumor cells transduced with the human cytochrome P450 gene CYP2B6 are greatly sensitized to CPA, however, the pathway of CPA-induced cell death is unknown. The present study investigates the cytotoxic events induced by CPA in 9L gliosarcoma cells retrovirally transduced with CYP2B6, or induced in wild-type 9L cells treated with mafosfamide (MFA) or 4-hydroperoxyifosfamide (4OOH-IFA), chemically activated forms of CPA and its isomer ifosfamide. CPA and MFA were both shown to effect tumor cell death by stimulating apoptosis, as evidenced by the induction of plasma membrane blebbing, DNA fragmentation, and cleavage of the caspase 3 and caspase 7 substrate poly(ADP-ribose) polymerase (PARP) in drug-treated cells. Caspase 9 was identified as the regulatory upstream caspase activated in 9L cells treated with CPA, MFA, or 4OOH-IFA, implicating the mitochondrial apoptotic pathway in oxazaphosphorine-induced tumor cell death. Correspondingly, expression of the mitochondrial proapoptotic factor Bax enhanced caspase 9 activation, plasma membrane blebbing, and drug-induced cytotoxicity. Conversely, overexpression of the mitochondrial antiapoptotic factor Bcl-2 blocked caspase 9 activation, leading to an inhibition of drug-induced plasma membrane permeability and blebbing, terminal deoxynucleotidyl transferase dUTP nick-end labeling positivity, PARP cleavage, Annexin V positivity, and drug-induced cell death. Although Bcl-2 thus blocked the cytotoxic effects of activated CPA, it did not inhibit the drug's cytostatic effects. CPA induced S-phase cell cycle arrest followed by conversion to an apoptotic pre-G1 state in wild-type 9L cells; by contrast, Bcl-2-expressing 9L cells accumulated in G2/M in response to CPA treatment. Intratumoral expression of Bcl-2 and related family members, including both apoptotic and antiapoptotic factors, is thus an important determinant of the responsiveness of tumor cells to CPA and ifosfamide, both in the context of conventional chemotherapy and in patients sensitized to these oxazaphosphorine drugs by the use of cytochrome P450-based gene therapy.
[Schwartz PS, Waxman DJ; Mol Pharmacol 60 (6): 1268-1279 (2001)]**PEER REVIEWED**

Specimens of whole bronchial tissue from the main or lobar bronchi and peripheral parenchyma were removed at surgery of 21 male patients undergoing lung resection for lung cancer (n= 18) or other, non-neoplastic,lung diseases (n= 3). Post-mitochondrial S-12 fractions were obtained. In parallel, the same preparations were used to assess the activation of a promutagen, cyclophosphamide (CPA, 4000 ug/plate), to metabolites reverting his(-) Salmonella typhymurium strain TA1535. Parenchyma compared favorably to bronchus preparations in activating CPA to mutagenic metabolites (n= 6 paired observations).
[Petruzzelli S et al; Am Rev Respir Dis 140 (2,1): 417-22 (1989)]**PEER REVIEWED**

Absorption, Distribution & Excretion:

Cyclophosphamide is well absorbed orally.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

PLACENTAL TRANSFER OF (14)CARBON-CYCLOPHOSPHAMIDE HAS BEEN DEMONSTRATED IN MICE; AND A POSITIVE CORRELATION BETWEEN THE ALKYLATION OF EMBRYONIC DNA AND PRODUCTION OF CONGENITAL ABNORMALITIES IN MICE HAS BEEN REPORTED. A SIMILAR CORRELATION HAS BEEN FOUND FOR NUCLEAR-DNA-DEPENDENT RNA POLYMERASES IN RAT EMBRYOS. IN MOST SPECIES, CYCLOSPHSPHAMIDE IS RAPIDLY ABSORBED, METABOLIZED AND EXCRETED. IN RATS, THE SPECIFIC ACTIVITY IN TISSUES IS HIGHEST WITHIN 20-30 MIN FOLLOWING IP INJECTION; UP TO 75% OF THE RADIOACTIVITY IS EXCRETED WITHIN 5-8 HR. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 176 (1981)]**PEER REVIEWED**

AFTER ITS IV INJECTION, THE DRUG IS RAPIDLY ABSORBED FROM THE BLOOD. IN PATIENTS RECEIVING 6.7-80 MG/KG BODY WT PER DAY OF RING LABELLED CYCLOPHOSPHAMIDE, RADIOACTIVITY WAS DISTRIBUTED RAPIDLY TO ALL TISSUES: ITS HALF LIFE IN THE PLASMA WAS 6.5 HOURS. NO RADIOACTIVITY WAS FOUND IN THE EXPIRED AIR OR FECES. RECOVERY OF RADIOACTIVITY IN URINE HAS BEEN REPORTED TO BE BETWEEN 50-68%, MAINLY IN THE FORM OF CARBOXYPHOSPHAMIDE AND PHOSPHORAMIDE MUSTARD; 10-40% OF THE DRUG WAS EXCRETED UNCHANGED; AND 56% OF THE REACTIVE METABOLITES WERE BOUND TO PLASMA PROTEINS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 181 (1981)]**PEER REVIEWED**

In a cross sectional study, the urine of 20 hospital workers occupationally exposed to cyclophosphamide and 21 unexposed controls was monitored for excretion of cyclophosphamide. During the week in which samples were collected, most of the workers handled cyclophosphamide fewer than 5 times and the amount handled each time ranged from 100-1000 mg (mean + or - 350 mg). All workers claimed to have taken regular safety precautions; ie, at least wearing gloves during handling. The drug was identified in 5 cases (range: 0.7-2.5 ug cyclophosphamide excreted/24 hr urine). A clear relationship between cyclophosphamide handling and urinary detection was shown. 4 of 5 persons with detectable urinary cyclophosphamide had handled cyclophosphamide 10 times or more during the week.
[Evelo CTA et al; Int Arch Occup Environ Health 58: 151-5 (1986)]**PEER REVIEWED**

A group of four adult male Sprague Dawley rats received each a bolus iv injection of (14)C-cyclophosphamide (50 uCi/rat) and 10 mg/kg of cyclophosphamide, dissolved in saline. Samples of plasma, seminal fluid, and tissues were obtained and analyzed. Cyclophosphamide was first found in seminal vesicle fluid within 10 min and reached equilibrium with plasma radioactivity within 30 min. These concentrations were maintained after drug administration for at least 2 hr. In a second experiment, male rats received an ip injection of cyclophosphamide in saline (10 mg/kg unlabeled cyclophosphamide plus 50 uCi/rat of (14)C-cyclophosphamide) 1 hr before exposure to females. The males were killed and blood, urine, and seminal fluid samples were obtained. Females were killed and uterus content plus several tissues were obtained for analysis. More than 5 hr after the males received an ip injection of 14(C)-cyclophosphamide the radiolabeled drug was transmitted to the females and was widely distributed in their seminal plug, vagina, cervix, kidney, and other tissues. In a third experiment, groups of 10 male rats were injected ip with 10, 30, or 100 mg/kg cyclophosphamide in saline, and controls were given saline. Each male was mated with 2 females. On day 20 of gestation, fetuses were removed and studied. The number of pregnant females per sperm positive females ranged from 73 to 92%, with no significant difference in any of the treated groups. The number of implantations per pregnant female decreased with cyclophosphamide treatment and at 30 mg/kg, this decrease was significantly different from controls. The highest dose of cyclophosphamide increased the preimplantation loss per litter, while the percentage of implantation loss per total corpora lutea was almost doubled.
[Hales BF et al; Toxicol Appl Pharmacol 84: 423-30 (1986)]**PEER REVIEWED**

Cyclophosphamide is excreted into breast milk.
[Briggs, G.G, R.K. Freeman, S.J. Yaffe. A Reference Guide to Fetal and Neonatal Risk. Drugs in Pregnancy and Lactation. 4th ed. Baltimore, MD: Williams & Wilkins 1994. 237]**PEER REVIEWED**

Oral bioavailability approximately =100%; must be activated in liver by microsomal enzymes to active compds & toxic metabolites; renal elimination of 22% parent drug & 60% of metabolites; t1/2 = 3-10 hr (parent); 6.5- >or=8 hr (alkylating activity) /from table/
[Young, L.Y., M.A. Koda-Kimble (eds.). Applied Therapeutics. The Clinical Use of Drugs. 6th ed. Vancouver, WA., Applied Therapeutics, Inc. 1995.,p. 90-11]**PEER REVIEWED**

Biological Half-Life:

Maximal concns in plasma are achieved 1 hr after oral admin, & the half-life in plasma is about 7 hr.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

Mechanism of Action:

The chemotherapeutic alkylating agents have in common the property of becoming strong electrophiles through the formation of carbonium ion intermediates or of transition complexes with the target molecules. These reactions result in the formation of covalent linkages by alkylation of various nucleophilic moieties such as phosphate, amino, sulfhydryl, hydroxyl, carboxyl, & imidazole groups. The chemotherapeutic & cytotoxic effects are directly related to the alkylation of DNA. The 7 nitrogen atom of guanine is particularly susceptible to the formation of a covalent bond with bifunctional alkylating agents & may well represent the key target that determines their biological effects. It must be appreciated, however, that other atoms in the purine & pyrimidine bases of DNA- particularly, the 1 & 3 nitrogens of adenine, the 3 nitrogen of cytosine, & the 6 oxygen of guanine- also may be alkylated, as will be the phosphate atoms of the DNA chains & amino & sulfhydryl groups of proteins. /Alkylating agents/
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1389]**PEER REVIEWED**

Cyclophosphamide can be used to cause immunologically mediated regression of the immunogenic, cyclophosphamide-resistant L5178Y lymphoma in syngeneic and semisyngeneic mice (B6D2F1 (C57BL/6 x DBA/2) females). In order to cause tumor regression it was necessary to give cyclophosphamide (125-200 mg/kg of body wt, iv shortly before or shortly after tumor implantation. Regardless of whether cyclophosphamide was given before or after tumor implantation, tumor regression was associated with the presence in the spleen of an incr number of Lyt-2+ T-cells capable of passively transferring immunity to tumor bearing recipients. This augmented level of immunity was sustained throughout the period of tumor regression. In contrast, a lower level of concomitant immunity generated by control tumor bearers decayed after day 12 of tumor growth. Because the therapeutic effect of cyclophosphamide could be inhibited by passive transfer of L3T4+ T-cells from normal donor mice it is apparent that the therapeutic effect of cyclophosphamide is based on its ability to preferentially destroy L3T4+ suppressor T-cells. These putative precursor suppressor T-cells were regenerated 4 days after being destroyed by cyclophosphamide.
[Awwad M, North RJ; Cancer Res 49 (7): 1649-54 (1989)]**PEER REVIEWED**

These studies enable the pattern of emesis and nausea for 3 days following high-dose cyclophosphamide to be described and give some insight into the mechanisms of emesis which may be operating. Nausea and vomiting induced by cyclophosphamide-based chemotherapy has long latency of onset (8-13 hr) and continues for at least 3 days. These findings are of particular importance as many of these patients receive chemotherapy as outpatients and emphasize the need for appropriate anti-emetic prophylaxis for patients at home. Ondansetron was extremely effective over this time in the control of emesis and nausea. These results suggest that high-dose cyclophosphamide-induced emesis over days 1-3 is largely mediated via 5-hydroxytryptamine (5-HT) and 5-HT3 receptors.
[Beck TM; Anticancer Dugs 6 (2): 237-42 (1995)]**PEER REVIEWED**

The most likely mechanism by which cyclophosphamide augments immune responses relates to preferential elimination of suppressor and relative sparing of effector and helper cells. Thus, precursors and mature murine suppressor cells are very sensitive to cyclophosphamide whereas the mature effector cells are relatively insensitive ... . Cyclophosphamide induced immunological regression of murine leukemia is reversed by the infusion of normal spleen cells as a source of precursors of suppressor cells ... . Memory and helper T cells are relatively resistant to the cytotoxic effect of cyclophosphamide ... . NK activity against YAC lymphoma targets by non T and non B cells is depressed by cyclophosphamide ... .
[Foye, W.O. (ed.). Cancer Chemotherapeutic Agents. ACS Professional Reference Book. Washington, D.C.: American Chemical Society, 1995. 469]**PEER REVIEWED**

Interactions:

PRIOR TREATMENT WITH ALLOPURINOL SIGNIFICANTLY PROLONGS /THE HALF-LIFE OF CYCLOPHOSPHAMIDE/.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1217]**PEER REVIEWED**

CYCLOPHOSPHAMIDE MAY ENHANCE NEUROMUSCULAR BLOCKADE PRODUCED BY SUCCINYLCHOLINE BY INHIBITING ITS METABOLISM.
[Evaluations of Drug Interactions. 2nd ed. and supplements. Washington, DC: American Pharmaceutical Assn., 1976, 1978. 600]**PEER REVIEWED**

THE ENZYME INHIBITOR SKF 525-A, WHICH INCREASES THE TERATOGENICITY OF CYCLOPHOSPHAMIDE, CAUSED AN INCREASE IN THE CONCN OF CYCLOPHOSPHAMIDE IN THE MOUSE EMBRYO & ALSO CAUSED A DECREASE IN METABOLITE FORMATION AFTER ADMIN OF CYCLOPHOSPHAMIDE TO PREGNANT MICE.
[The Chemical Society. Foreign Compound Metabolism in Mammals. Volume 2: A Review of the Literature Published Between 1970 and 1971. London: The Chemical Society, 1972. 434]**PEER REVIEWED**

Cultured human osteosarcoma cell lines (OST strain and HT 1080) and specimens obtained during surgery on humans (osteosarcoma, malignant fibrous histiocytoma, rhabdomyosarcoma, epithelioid sarcoma, mesenchymal chondrosarcoma, synovial sarcoma, leiomyosarcoma, and malignant giant cell tumor) were used to study the synergistic effect of caffeine on anticancer drugs, including cyclophosphamide as its active form 4-hydroxyperoxycyclophosphamide. Cell concentrations were 10,000 per dish for the osteosarcoma strain, 50,000 per dish for the HT 1080 strain, and 100,000 to 500,000 for the fresh cells. After a 1 hour exposure of the cells to the anticancer agent, caffeine was added to the top layer for the subsequent 10 day to 3 week combined exposure. Treatment with 3.0 ug/ml (1/10 of the usual peak plasma concentration) cyclophosphamide alone showed colony inhibition of 14.2% in the OST strain and 8.5% in the HT 1080 strain. Addition of 0.2 mM caffeine showed synergism, 27.8% and 56.2% inhibition, respectively. When 2 mM caffeine was used with cyclophosphamide, colony inhibition was 57.1% in the OST strain. At a cyclophosphamide concentration of 0.3 ug/ml and either 0.2 or 2 mM caffeine, synergism still was observed. Using fresh human tumor specimens with cyclophosphamide alone (3.0 ug/ml) 4 of 18 specimens showed positive sensitivity. With 2 mM caffeine exposure in combination, 8 of 18 specimens (44.4%) showed a significant synergistic effect; of these, 7 showed positive sensitivity. An additive effect was observed in one specimen and a subadditive effect in 3 specimens. Continuous exposure to 0.2 mM caffeine in combination resulted in significant synergism in specimens. For comparison, caffeine alone at 0.2 mM produced colony inhibition of 9.2% (OST strain) and 12.5% (HT 10890 strain) in the cultured cells; at 2.0 mM, 15.0% (OST strain) and 100.0% (HT 1080 strain). In fresh sarcoma specimens, caffeine alone at 2 mM produced inhibition of 0.0% to 48.2% (mean, 19.1%) and there was no case with positive sensitivity.
[Tomita K, Tsuchiya H; Jpn J Cancer Res 80 (1): 83-8 (1989)]**PEER REVIEWED**

DBA/2NCr1BR F1 mice received a single iv injection of cyclophosphamide (70, 120 or 200 mg/kg) alone or 2 hr before an ip injection of 1,000 mg/kg of diethyldithiocarbamate. 24 hr after, survival of bone marrow colony forming units spleen and granulocyte macrophage colony forming cells, was determined. On the whole, administration of diethyldithiocarbamate reduced the toxic effect of cyclophosphamide on hemopoietic progenitors. The effect was in general more evident at the lower than at the higher doses of the antitumor drug.
[Pannacciulli IM et al; Br J Cancer 59 (3): 371-4 (1989)]**PEER REVIEWED**

Leukopenic and/or thrombocytopenic effects of cyclophosphamide may be increased with concurrent use or recent therapy if these medications /blood dyscrasia-causing medications/ cause the same effects; dosage adjustment of cyclophosphamide, if necessary, should be based on blood counts.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Additive bone marrow depression may occur; dosage reduction may be required when two or more bone marrow depressants, including radiation, are used concurrently or consecutively /with cyclophosphamide/.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Cyclophosphamide may raise the concentration of blood uric acid; dosage adjustment of antigout agents /allopurinol or colchicine or probenecid or sulfinpyrazone/ my be necessary to control hyperuricemia and gout; uricosuric antigout agents may increase risk of uric acid nephropathy. Concurrent use with allopurinol may enhance the bone marrow toxicity of cyclophosphamide; if concurrent use is required, close observation of toxic effects should be considered.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Inhibition of cholinesterase activity by cyclophosphamide reduces or slows cocaine metabolism, thereby increasing and/or prolonging its effects and increasing the risk of toxicity.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use of high-dose cytarabine with cyclophosphamide for bone marrow transplant preparation has bee reported to result in an increase in cardiomyopathy with subsequent death.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use /of daunorubicin or doxorubicin/ with cyclophosphamide may result in increased cardiotoxicity; it is recommended that the total dose of daunorubicin or doxorubicin not exceed 400 mg/sq m of body surface.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

These agents /hepatic enzyme inducers/ may induce microsomal metabolism to increase formation of alkylating metabolites of cyclophosphamide, thereby reducing the half-life and increasing the activity of cyclophosphamide.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use of other immunosuppressants such as: azathioprine; chlorambucil; corticosteroids, glucocorticoid; cyclosporine; mercaptopurine; muromonab-CD3/ with cyclophosphamide may increase the risk of infection and development of neoplasms.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use /of lovastatin with cyclophosphamide/ in cardiac transplant patients may be associated with an increased risk of rhabdomyolysis and acute renal failure.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Cyclophosphamide may decrease plasma concentrations or activity of pseudocholinesterase, the enzyme that metabolizes succinylcholine, thereby enhancing the neuromuscular blockage of succinylcholine. Increased or prolonged respiratory depression or paralysis (apnea) may occur but is of minor clinical significance while the patient is being mechanically ventilated; however, caution and careful monitoring of the patient are recommended during and following concurrent or sequential use, especially if there is a possibility of incomplete reversal of neuromuscular blockage postoperatively.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

The effect of high molecular carboxymethyl-chitin-glucan (CMCG), admin either ip, iv or orally prior to cyclophosphamide injection, on the frequency of micronucleated reticulocytes was evaluated in peripheral blood of female ICR mice. Both ip and iv admin of CMCG decreased the clastogenic effect of cyclophosphamide. The protective effect of CMCG was concn dependent, with a higher decrease achieved by 100 mg/kg than by 50 mg/kg body weight. On the other hand, no even five peroral pretreatments with CMCG in the dose of 200 mg/kg body weight during the week prior to simultaneous admin of CMCG and cyclophosphamide induced a decrease of micronucleated reticulocytes in peripheral blood.
[Chorvatovi cov'a D and J Sandula; Mutat Res 346 (1): 43-8 (1995)]**PEER REVIEWED**

Synergistically enhanced sister chromatid exchange (SCE) frequency by cyclophosphamide (CP) was observed when L1210 lymphoid tumor cells were exposed in vivo to a non-toxic concn of 3-aminobenzamide (3-AB). Additive effects in SCE induction in vivo were observed when either Ehrlich ascites tumor (EAT) cells or P388 lymphocytic leukemia cells treated with CP were exposed to 3-AB in vivo. 3-AB enhanced the survival time of L1210 tumor bearing BDF1 mice treated with CP. However, the combined CP plus 3-AB treatment did not increase the survival of either EAT BALB/c- or P388 BDF1-tumor bearing mice compared with the effect on survival by CP alone. Therefore the in vivo differential antitumor effect, by CP in conjunction with 3-AB, appears to correlated well with the in vivo differential effect on cytogenetic damage caused by the combined CP plus 3-AB treatment. In the Salmonella typhimurium/mammalian microsome test CP appears to have a dose dependent ability to induce base-pair substitutions in strains TA 100 and TA 1535 and frameshift mutations in strains TA 98 and TA 1537. Both types of mutation were synergistically increased in the presence of 3-AB.
[Eliopoulos P et al; Mutat Res 342 (3-4): 141-6 (1995)]**PEER REVIEWED**

Treatment with Caralluma tuberculata extract induced complex biochemical and cytological changes in mice. Its cytotoxicity in the bone marrow cells of mice was comparable with that of the standard drug cyclophosphamide (C); however, unlike C, C. tuberculata was not clastogenic (as shown by the micronucleus assay). A dose-dependent decrease in the RNA content of liver and testes was produced by C. tuberculata treatment whereas there was no effect on the content of nucleic acid and protein in the brain. In the extract-treated animals there was a significant and dose-dependent increase in the DNA content of the liver, with a negligible effect on the protein content. Combined treatment with C. tuberculata and C showed that C. tuberculata diminished the effect of C on DNA levels; however, RNA levels were further suppressed, resulting in increased cytotoxicity. Pretreatment with C. tuberculata extract significantly reduced the clastogenicity of C. These results indicated the involvement of different phytoconstituents acting by different routes.
[al-Bekairi AM et al; Food Chem Toxicol 30 (8): 719-22 (1992)]**PEER REVIEWED**

The effect of pretreatment with carboxymethylglucan (CMG) on the frequency of micronuclei induced by cyclophosphamide administration in mice was evaluated. Two doses of CMG (50 mg/kg body weight) injected either intraperitoneally 24 hr or intravenously 1 hr prior to two cyclophosphamide administrations (80 mg/kg) significantly decreased the frequency of micronucleated PCE in bone marrow. Of two evaluated derivatives of carboxymethylglucan, the K3 derivative was most efficient. The results show that it is possible to achieve a suppressive effect of soluble carboxymethylglucan prepared from Saccharomyces cerevisiae against cyclophosphamide mutagenicity. The notion may be useful for glucan's effects against pharmacocarcinogenesis. Therapeutic application of glucan with cyclophosphamide therapy may provide a remarkable decrease of the secondary tumor risk. The utilization of these results for human patients needs to be considered.
[Chorvatovi cov'a D, Navarov'a J; Mutat Res 282 (3): 147-50 (1992)]**PEER REVIEWED**

The modulatory effect of vitamin C (Vit C) on the mutagenic effect of the antineoplastic drug cyclophosphamide (CP) was assessed in the in vivo micronucleus test in Swiss mice. Simultaneous oral administration of Vit C with ip administration of CP was found to decrease the frequency of micronucleated polychromatic erythrocytes elevated by CP. Vit C exhibited a significant antimutagenic effect over a wide dose range (1.56-200 mg/kg). The dose-response relationship was highly significant. These results demonstrated the ability of the in vivo micronucleus test to detect in vivo modulation of CP mutagenicity by Vit C. Our earlier results and those from other laboratories also indicate that this model system is suitable for primary in vivo screening of modulation of mutagenesis.
[Ghaskadbi S et al; Teratog Carcinog Mutagen 12 (1): 11-7 (1992)]**PEER REVIEWED**

A total of 78 patients with second recurrence or progression of histologically verified breast cancer were treated with single-agent cyclophosphamide given at 2.5 g/sq m by iv infusion every 3 wk along with mesna support. All had previously been treated with epirubicin and cisplatin or epirubicin alone. Toxicity was predominantly hematologic: WHO grade III+IV toxicity was found in 95% of cases. The overall response rate was 26.7% (95% CI, 15.8-41.4%), with 7% of patients achieving a complete response (CR) and 19.7%, a partial response (PR). The median duration of CRs and PRs was 11 and 5 mo, respectively. The response rate observed for patients previously treated with epirubicin alone was 30.5% in contrast to the 8.3% recorded for patients previously treated with cisplatin plus epirubicin. Thus, an indication of cross-resistance was absent between cyclophosphamide and epirubicin but possible between cyclophosphamide and cisplatin.
[Hansen F et al; Cancer Chemother Pharmacol 37 (4): 377-81 (1996)]**PEER REVIEWED**

The effect of WR-2721 against cyclophosphamide-induced clastogenicity was studied using the in vivo micronucleus assay. The frequency of micronuclei in polychromatic erythrocytes in the peripheral blood of mice treated with WR-2721 and cyclophosphamide (CP), each of the cmpd at a dose of 200 mg/kg body weight, was evaluated during the 15-day period. The suppressing effect of WR-2721, given 30 min prior to CP admin, on micronuclei induced by the alkylating agent was demonstrated ... The modulatory effect of WR-2721 on the clastogenic activity of CP in the erythropoietic system by the mouse micronucleus test was shown.
[Czy'zewska A and L Mazur; Teratog Carcinog Mutagen 15 (3): 109-14 (1995)]**PEER REVIEWED**

/It was/ ... demonstrated in an earlier paper that capsaicin, the pungent principle of red hot chili, has a potent anti-oxidant property that interferes with free-radical involved mechanisms. In the present paper we demonstrate that capsaicin significantly inhibits cyclophosphamide-induced (ip) chromosomal aberrations and DNA strand breakages. This protective action of capsaicin against CP-induced toxicity may possibly be linked with its already reported 'desensitization' effect against chemical irritant-induced damages.
[De AK et al; Mutat Res 335 (3): 253-8 (1995)]**PEER REVIEWED**

In the rat, the mortality from cyclophosphamide had prevented the administration of sufficient dosages to produce detectible damage to stem spermatogonia. To overcome this problem, we used bone marrow transplantation and sodium 2-mercaptoethanesulfonate (Mesna) treatment to raise the lethal dose for 50% of the animals (LD50) for cyclophosphamide from 275 to > 400 mg/kg body weight. In addition we used irradiation, 2 weeks prior to injection of cyclophosphamide, to greatly enhance the measured toxicity of cyclophosphamide towards stem spermatogonia. Whereas sperm counts at 9 weeks after a 300 mg/kg cyclophosphamide dose were reduced by only a factor of 1.6 without prior irradiation, they were reduced by a factor of 60 when 2.5 Gy of irradiation had been given. Dramatic protection against this toxicity was produced by hormone treatment with a gonadotropin-releasing hormone (GnRH) antagonist (Nal-Glu) and an antiandrogen (flutamide) following the radiation but prior to cyclophosphamide. This hormone treatment did not modify the stem cell toxicity of the radiation and it therefore must be protecting stem cells against cyclophosphamide-induced damage.
[Meistrich ML et al; J Androl 16 (4): 334-41 (1995)]**PEER REVIEWED**

Hamster to rat renal xenotransplantation was performed with recipient nephrectomies. Recipients were treated beginning on day 0 with continuous FK 506 monotherapy, a 7-day or open-ended monotherapeutic course of cyclophosphamide (CP), and the two drug regiments combined. CP alone (10 mg/kg/day) prevented a xenospecific antibody response and tripled median survival of the kidney (defined as recipient death) from 6 (control) to 18.5 days whereas FK 506 alone had no effect. The drugs in combination were no better than CP alone (15 days) unless the 5-day course of CP was given at a higher dose (15 mg/kg) and started 3 days preoperatively (79 days). In further experiments, adjuvant measures were added to the minimally effective FK 506/7-day CP regimen which gave a median survival of only 15 days. In the most successful modification, intraoperative antibody depletion by the temporary transplantation of third party hamster liver or en bloc kidneys increased median survival from 15 to 34 and 48 days, respectively. An intraoperative i.v. dose administration of the anticomplement drug K76 instead of antibody depletion increased survival to 26 days. Although the events of kidney rejection were similar to those of heart xenografts and partially forestalled by the antibody inhibiting CP treatment, or by antibody depletion, survival for > 100 days was accomplished in only 5 of 86 treated animals.
[Miyazawa H et al; Transplantation 59 (8): 1183-8 (1995)]**PEER REVIEWED**

Hemorrhagic cystitis is a common problem following cyclophosphamide or radiation therapy. Chitosan has been shown to be an effective hemostatic agent and promoter of wound healing in animal experiments. We evaluated the safety and efficacy of intravesical chitosan in an animal model of cyclophosphamide cystitis. Hemorrhagic cystitis was induced in female F344 rats by intraperitoneal cyclophosphamide, 100 mg/kg Chitosan soln (0.3 ml) was instilled intravesically on day 1 (Group 1), on days 1, 3, and 5 (Group 2), or 1 hr after the admin of cyclophosphamide (Group 3). The rats in group 4 were treated with chitosan diluent on day 1 after cyclophosphamide, and the rats in group 5 received intravesical chitosan without cyclophosphamide. Sequential examination revealed decr mortality and lower incidences of severe bladder bleeding, necrosis and inflammation in Group 3. Treatment delayed until after the appearance of the cystitis, esp repeated treatments, appeared to make the cyclophosphamide-induced changes worse. Used within 1 hr of cyclophosphamide admin, before the cystitis develops, chitosan seemed to have the possibility to inhibit the appearance of hemorrhagic cystitis. In addition to the changes in the bladder, severe changes occurred in the kidneys secondary to cyclophosphamide.
[Okamura T et al; Hinyokika Kiyo 41 (4): 289-96 (1995)]**PEER REVIEWED**

The effect of pretreatment with miltefosine (MIL) on the antineoplastic activity of cyclophosphamide (CPA) was evaluated in sc benzo(a)pyrene-induced sarcomas (BPS) of the rat. MIL alone had no antineoplastic effect on this autochthonous tumor, but enhanced the chemotherapeutic effect of CPA. Conversely, MIL counteracted the myelotoxicity of CPA in normal adult rats. Although the nadir of the leucocyte count remained unchanged, the recovery phase was considerably shortened, an effect which resembled the pharmacological action of GM-CSF.
[Stekar J et al; Eur J Cancer 31A (3): 372-4 (1995)]**PEER REVIEWED**

The effect of protein malnutrition and alcohol consumption on the yield of chromosomal damage induced by cyclophosphamide (CP) was studied. Chromosomal damage induced in bone marrow cells of BALB/c mice was established by scoring the frequency of dicentric chromosomes in C-banded slides. Results obtained showed that CP induced a significant incr of chromosomal damage in comparison with untreated mice. In addition, the yield of dicentric chromosomes was higher in mice fed with the hypoproteic diet. The animals which received ethanol in drinking water before treatment with CP exhibited the highest frequency of dicentric chromosomes, with no relation with the diet.
[Terreros MC et al; J Vet Med Sci 57 (1): 5-8 (1995)]**PEER REVIEWED**

Cyclophosphamide causes lung injury in rats through its ability to generate free radicals with subsequent endothelial and epithelial cell damage. In order to observe the protective effects of a potent anti-inflammatory antioxidant, curcumin (diferuloyl methane) on cyclophosphamide-induced early lung injury, healthy, pathogen free male Wistar rats were exposed to 20 mg/100 g body weight of cyclophosphamide, intraperitoneally as a single injection. Prior to cyclophosphamide intoxication oral administration of curcumin was performed daily for 7 days. At various time intervals (2, 3, 5 and 7 days post insult) serum and lung samples were analyzed for angiotensin converting enzyme, lipid peroxidation, reduced glutathione and ascorbic acid Bronchoalveolar lavage fluid was analyzed for biochemical constituents. The lavage cells were examined for lipid peroxidation and glutathione content. Excised lungs were analyzed for antioxidant enzyme levels. Biochemical analyses revealed time course increases in lavage fluid total protein, albumin, angio+ensin converting enzyme (ACE), lactate dehydrogenase, N-acetyl-beta-D-glucosaminidase, alkaline phosphatase, acid phosphatase, lipid peroxide levels and decreased levels of glutathione (GSH) and ascorbic acid 2, 3, 5 and 7 days after cyclophosphamide intoxication. Increased levels of lipid peroxidation and decreased levels of glutathione and ascorbic acid were seen in serum, lung tissue and lavage cells of cyclophosphamide groups. Serum angiotensin converting enzyme activity increased which coincided with the decrease in lung tissue levels. Activities of antioxidant enzymes were reduced with time in the lungs of cyclophosphamide groups.
[Venkatesan N and G Chandrakasan; Mol Cell Biochem 142 (1) 79-87 (1995)]**PEER REVIEWED**

Therapeutic Uses:

Alkylating Agents; Antineoplastic Agents, Alkylating; Antirheumatic Agents; Carcinogens; Immunosuppressive Agents; Mutagens; Teratogens
[National Library of Medicine's Medical Subject Headings online file (MeSH, 1999)]**PEER REVIEWED**

MEDICATION (VET): ... CYTOTOXIC AGENT FOR CARCINOMA, LEUKOSIS, ADENOMA, FIBROMA, & MIXED MAMMARY TUMORS OF DOGS ... MYCOTIC DERMATITIS ... OF SHEEP & TRYPANOSOMIASIS ... OF CATTLE ... ALSO ... CYTOTOXIC ... & IMMUNOSUPPRESSIVE IN RATS ... AGAINST EXPTL ALLERGIC ENCEPHALOMYELITIS.
[Rossoff, I.S. Handbook of Veterinary Drugs. New York: Springer Publishing Company, 1974. 148]**PEER REVIEWED**

The clinical spectrum of activity for cyclophosphamide is very broad. It is an essential component of many effective drug combinations for non-Hodgkin's lymphomas. Complete remissions & presumed cures have been reported when cyclophosphamide was given as a single agent for Burkitt's lymphoma. It is frequently used in combination with methotrexate (or doxorubicin) & fluorouracil as adjuvant therapy after surgery for carcinoma of the breast. Notable advantages of this drug are the availability of the oral route of admin & the possibility of giving fractionated doses over prolonged periods. For these reasons it possesses a versatility of action that allows an intermediate range of use, between that of the highly reactive iv mechlorethamine & that of oral chlorambucil. Beneficial results have been obtained in multiple myeloma; chronic lymphocytic leukemia; carcinomas of the lung, breast, cervix, & ovary; & neuroblastoma, retinoblastoma, & other neoplasms of childhood. Because of its potent immunosuppressive properties, cyclophosphamide has received considerable attention for the control of organ refection after transplantation & in nonneoplastic disorders associated with altered immune reactivity, including Wegener's granulomatosis, rheumatoid arthritis, & the nephrotic syndrome in children.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

Furosemide may improve, renal blood flow, decrease resorption of sodium and chloride, and increase free water excretion. The initial dose of furosemide is 2 mg/kg, IV. This dosage can be doubled or tripled if urine output does not increase within 1 hr. However, if there is no response to 6 mg/kg, another approach should be tried. If effective, furosemide can be given parenterally at 2 mg/kg, tid., to maintain a diuresis.
[Aiello, S.E. (ed). The Merck Veterinary Manual. 8th ed. Merck & Co., Inc., National Publishing Inc., Philadelphia, PA. 1998. 1732]**PEER REVIEWED**

/EXPL THER:/ To find out which anticancer drugs could utilize to the best advantage a syngeneic bone marrow transplantation (BMT) in high-dose chemotherapy for cancer, cyclophosphamide was tested in Sprague Dawley rats. Two or three varying doses of cyclophosphamide (100-400 mg/kg) were administered iv on day 0, followed by the injection of syngeneic bone marrow cells (50,000,000, iv) on day 2, & the animals were observed for over 60 days. A beneficial effect of bone marrow transplantation was observed only with cyclophosphamide (300-400 mg/kg) & nimustine hydrochloride (40 mg/kg). In order to enhance the beneficial effect of bone marrow transplantation observed with cyclophosphamide & nimustine hydrochloride, a way of drug admin was designed & carried out. Consequently a higher survival rate was obtained in the following experimental groups; (cyclophosphamide 200 mg/kg, days 0 & 1) + bone marrow transplantation > (cyclophosphamide 400 mg/kg, day 0) + bone marrow transplantation, (nimustine hydrochloride 20 mg/kg, days 0 & 1) + bone marrow transplantation > (nimustine hydrochloride 40 mg/kg, day 0) + bone marrow transplantation; (cyclophosphamide 200 mg/kg + nimustine hydrochloride 20 mg/kg, day 0) + bone marrow transplantation > (cyclophosphamide 400 mg/kg or nimustine hydrochloride 40 mg/kg, day 0) + bone marrow transplantation; (cyclophosphamide 200 mg/kg, day 0) + (nimustine hydrochloride 20/kg, day 1) + bone marrow transplantation > (nimustine hydrochloride 20 mg/kg, day 0) + (cyclophosphamide 200 mg/kg, day 1) + bone marrow transplantation.
[Mizushima Y et al; Cancer Res 49 (10): 2561-6 (1989)]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of acute lymphoblastic (stem-cell) leukemia in children (including during remission to prolong the duration), and for treatment of acute myelogenous and acute monocytic leukemia. /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1101]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of chronic granulocytic leukemia (it is usually ineffective in acute blastic crisis) and chronic lymphocytic leukemia. /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1101]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of adenocarcinoma of the ovary, breast carcinoma, neuroblastoma (in patients with disseminated disease /NOT included in US product labeling/), retinoblastoma, ... . /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1101]**PEER REVIEWED**

... /Cyclophosphamide is indicated for treatment of/ small cell and non-small cell lung carcinoma, cervical carcinoma, and for endometrial carcinoma, bladder carcinoma, prostatic carcinoma, testicular carcinoma, and Wilms' tumor and adrenocortical carcinoma (Evidence rating: IIID). /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc.,p. 1101-2]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of Stage III and IV (Ann Arbor or Peter's Staging System) Hodgkin's disease and non-Hodgkin's lymphomas including nodular or diffuse lymphocytic lymphoma, mixed-cell type lymphoma, histiocytic lymphoma, Burkitt's lymphoma, (and lymphoblastic lymphosarcoma /NOT included in US product labeling/). /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of multiple myeloma. /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of advanced mycosis fungoides. /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated as an immunosuppressant in the treatment of steroid-resistant or frequently relapsing steroid-sensitive biopsy proven minumal-change nephrotic syndrome in children (and adults /NOT included in US product labeling/). /Included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of various sarcomas, including Ewing's sarcoma, osteosarcoma, and soft tissue sarcomas. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of Waldenstrom's macroglobulinemia. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated as first-line therapy, as a single agent or in combination with other chemotherapeutic agents, for treatment of Histiocytosis X (Letterer-Siwe disease). (Evidence rating: IIID) /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is indicated for treatment of thymoma. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is used for treatment of germ cell ovarian, primary brain, and gestational trophoblastic tumors. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is used for its immunosuppressant activity, for prevention of rejection in homotransplantation. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is used as an immunosuppressant in the treatment of rheumatoid arthritis and other autoimmune diseases such as polymyositis (systemic dermatomyositis), multiple sclerosis, Wegener's granulomatosis, systemic lupus erythematosus, and other types of vasculitis. /NOT included in US product labeling/
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Cyclophosphamide is used as an antitumor agent and experimentally for removal of fleece in adult sheep. The likelihood that cyclophosphamide residues will occur or pose a problem is remote.
[Booth, N.H., L.E. McDonald (eds.). Veterinary Pharmacology and Therapeutics. 5th ed. Ames, Iowa: Iowa State University Press, 1982. 1095]**PEER REVIEWED**

Severe aplastic anemia (SAA) can be successfully treated with allogeneic bone marrow transplantation (BMT) or immunosuppressive therapy. However, the majority of patients with SAA are not eligible for BMT because they lack an HLA-identical sibling. Conventional immunosuppressive therapy also has major limitations; many of its remissions are incomplete and relapse or secondary clonal disease is common. Cyclophosphamide is a potent immunosuppressive agent that is used in all BMT conditioning regimens for patients with SAA. Preliminary evidence suggested that high-dose cyclophosphamide, even without BMT, may be beneficial to patients with SAA. Therefore, 10 patients with SAA and lacking an HLA-identical sibling were treated with high-dose cyclophosphamide (45 mg/kg/day) for 4 consecutive days with or without cyclosporine. A complete response (hemoglobin level, > 13 g/dL; absolute neutrophil count, > 1.5 x 10(9)/L, and platelet count > 125 x 10(9)/L) was achieved in 7 of the 10 patients. One of the complete responders died from the acquired immunodeficiency syndrome 44 months after treatment with high-dose cyclophosphamide. The 6 remaining patients are alive and in continuous complete remission, with a median follow-up of 10.8 years (range, 7.3 to 17.8 years). The median time to last platelet transfusion and time to 0.5 x 10(9) neutrophils/L were 85 and 95 days, respectively. None of the complete responders has relapsed or developed a clonal disease. These results suggest that high-dose cyclophosphamide, even without BMT, may be more effective than conventional immunosuppressive therapy in restoring normal hematopoiesis and preventing relapse or secondary clonal disorders. Hence, further studies confirming the efficacy of this approach in SAA are indicated.
[Brodsky RA et al; Blood 87 (2): 491-4 (1996)]**PEER REVIEWED**

The objective of this study was to determine the tolerance and toxicities of high-dose cyclophosphamide (CPA) at 7 g/sq m given in four fractions over 8 hr in children with advanced solid tumors ... Twenty children aged 1 1/2-19 years (median, 12 years) received 24 courses of high-dose CPA at 7 g/sq m for the treatment of advanced malignant solid tumor. CPA was given in four l-hr infusions of 1.75 g/sq m each, with 1 hr of rest between each dose. MESNA was used as a uroprotective agent and was continued for 24 hr after the final dose of CPA. With only one exception, all patients were discharged at the end of MESNA infusion and received granulocyte colony-stimulating factor, prophylactic ciprofloxacin, and co-trimoxazole ... Severe but transient myelosuppression was observed. The median time to neutrophil and platelet recovery was 17 and 19 days, respectively. Fever developed after 13 of the 24 courses, and hospitalization was required. Extramedullary toxicities were mild. No patient showed cardiomyopathy or hemorrhagic cystitis. Forty-six percent of the courses were managed entirely on an outpatient basis. Objective tumor response was seen in five patients ... CPA at 7 g/sq m is well tolerated by children with advanced malignancies and should be considered in earlier phases of antineoplastic therapy.
[Chan LL et al; J Pediatr Hematol Oncol 18 (1): 63-7 (1996)]**PEER REVIEWED**

Cyclophosphamide (CTX) is an active drug in breast cancer & presents a well-established dose-response relationship. To explore further this relationship, the present pilot study investigated the therapeutic efficacy of cyclophosphamide at intermediate dose in 2 groups of untreated patients with advanced breast cancer. Nine women received the drug alone at 3-4 g/sq m iv every 2 wk for a total of 3 doses. The same dose schedule was also given to 11 women following the admin of 4 cycles of Adriamycin, at 75 mg/sq m iv every 3 wk. We documented 1 partial remission in untreated women & 4 partial responses in Adriamycin-treated patients. The major toxicity was represented by leukopenia & neutropenia. Myelosuppression was relevant but of short duration, & the use of G-CSF appeared useful in controlling this side effect. In spite of the high dose intensity of the present cyclophosphamide dose schedule (9 g/sq m in 4 wk), i.e., almost 3 times superior to that conventionally employed, present results do not suggest its superiority over the current chemotherapeutic regimens utilized in advanced disease.
[Zambetti M et al; Am J Clin Oncol 19 (1): 82-6 (1996)]**PEER REVIEWED**

Antineoplastic
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 200]**PEER REVIEWED**

MEDICATION (VET): ANTINEOPLASTIC
[Rossoff, I.S. Handbook of Veterinary Drugs. New York: Springer Publishing Company, 1974. 148]**PEER REVIEWED**

HAS BEEN TESTED AS AN INSECT CHEMOSTERILANT. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 138 (1975)]**PEER REVIEWED**

... PROPOSED AS DEFLEECING AGENT FOR SHEEP.
[Budavari, S. (ed.). The Merck Index - Encyclopedia of Chemicals, Drugs and Biologicals. Rahway, NJ: Merck and Co., Inc., 1989. 429]**PEER REVIEWED**

Most first-line regimens /for treating ovarian cancer/ currently include cisplatin & cyclophosphamide ... .
[Young, L.Y., M.A. Koda-Kimble (eds.). Applied Therapeutics. The Clinical Use of Drugs. 6th ed. Vancouver, WA., Applied Therapeutics, Inc. 1995.,p. 93-13]**PEER REVIEWED**

A 78-yr-old man was hospitalized on February 29, 2000 because of dyspnea. A chest radiograph showed diffuse bilateral interstitial shadows associated with pulmonary volume loss. We could not obtain histological evidence of idiopathic interstitial pneumonia (IIP) because of his advanced age & severe respiratory dysfunction. IIP was diagnosed on the basis of radiographic findings & clinical symptoms. The patient was intubated & mechanical ventilation was performed. After one course of pulsed cyclophosphamide (CPM) & methylprednisolone therapy, the hypoxemia improved & it became possible to wean the patient from the ventilator. After 5 courses of pulsed CPM therapy, the dose of oral corticosteroid was tapered. CPM was administered safely without any severe side effects. Pulsed CPM therapy appears to be a viable alternative method of treatment for IIP.
[Umemura S, et al; Nihon Kokyuki Gakkai Zasshi 39 (10): 781-786. 2001.]**PEER REVIEWED**

 

Drug Warnings:

Appropriate caution is advised when the drug is considered for use in ... /nonneoplastic/ conditions, not only because of its acute toxic effects but also because of its high potential for inducing sterility, teratogenic effects, & leukemia. ... Administration of the drug should be interrupted at the first indication of dysuria or hematuria. The syndrome of inappropriate secretion of antidiuretic hormone (ADH) has been observed in patients receiving cyclophosphamide, usually at doses higher than 50 mg/kg. It is important to be aware of the possibility of water intoxication, since these patients are usually vigorously hydrated.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

POTENTIAL ADVERSE EFFECTS ON FETUS: Various fetal malformations, especially skeletal defects and dysmorphic features, but other chemotherapeutic agents given concurrently. POTENTIAL SIDE EFFECTS ON BREAST-FED INFANT: Transient neutropenia from cyclophosphamide with prednisone and vincristine. Potential mutagenicity, carcinogenicity, adverse effects on fetus. FDA Category: D (D = There is evidence of human fetal risk, but the potential benefits from use in pregnant women may be acceptable despite the potential risks (e.g., if the drug is needed in a life-threatening situation or for a serious disease for which safer drugs cannot be used or are ineffective.)) /from Table II/
[Stockton DL and Paller AS; J Am Acad Dermatol 23 (1):87-103 (1990)]**PEER REVIEWED**

Drugs that are Contraindicated during Breast-Feeding: Cyclophosphamide: Possible immune suppression; unknown effect on growth or association with carcinogenesis; neutropenia. /from Table 1./
[Report of the American Academy of Pediatrics Committee on Drugs in Pediatrics 93 (1): 138 (1994)]**PEER REVIEWED**

THE DRUG IS MOST TOXIC TO THE HUMAN FETUS DURING 1ST 3 MO & CONGENITAL ABNORMALITIES HAVE BEEN DETECTED AFTER IV INJECTION OF LARGE DOSES TO PREGNANT WOMEN DURING THIS PERIOD OF PREGNANCY. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 146 (1975)]**PEER REVIEWED**

For routine clinical use, ample fluid intake is recommended.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1396]**PEER REVIEWED**

Cyclophosphamide is distributed into breast milk. Breast-feeding is not recommended during chemotherapy because of the risks to the infant (adverse effects, mutagenicity, carcinogenicity).
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Prepubescent girls treated with cyclophosphamide usually develop secondary sexual characteristics normally, have regular menses, and subsequently conceive; however, ovarian fibrosis and apparent complete loss of germ cells after prolonged treatment in late prepubescence have been reported. Prepubescent boys treated with cyclophosphamide develop secondary sexual characteristics normally, but may have oligospermia or azoospermia, increased gonadotropin secretion, and some degree of testicular atrophy; azoospermia may be reversible, although possibly not for several years after the end of cyclophosphamide therapy.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

Although appropriate studies on the relationship of age to the effects of cyclophosphamide have not been performed in the geriatric population, geriatrics-specific problems are not expected to limit the usefulness of this medication in the elderly. However, elderly patients are more likely to have age-related renal function impairment, which may require caution in patients receiving cyclophosphamide.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1102]**PEER REVIEWED**

The bone marrow depressant effects of cyclophosphamide may result in an increased incidence of microbial infection, delayed healing, and gingival bleeding. Dental work, whenever possible should be completed prior to initiation of therapy or deferred until blood counts have returned to normal. Patients should be instructed in proper oral hygiene during treatment, including caution in use of regular tooth brushes, dental floss, and toothpicks. Cyclophosphamide may also rarely cause stomatitis associated with considerable discomfort.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Because normal defense mechanisms may be suppressed by cyclophosphamide therapy, concurrent use with a live virus vaccine may potentiate the replication of the vaccine virus, may increase the side/adverse effects of the vaccine virus, and/or may decrease the patient's antibody response to the vaccine; immunization of these patients should be undertaken only with extreme caution after careful review of the patient's hematologic status and only with the knowledge and consent of the physician managing the cyclophosphamide therapy. The interval between discontinuation of medication that cause immunosuppression and restoration of the patient's ability to respond to the vaccine depends on the intensity and type of immunosuppression-causing medications used, the underlying disease, and other factors; estimates vary from 3 months to 1 year. Patients with leukemia in remission should not receive live virus vaccine until at least 3 months after their last chemotherapy. In addition, immunization with oral polio-virus vaccine should be postponed in persons in close contact with the patient, especially family members.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Anorexia, nausea, and vomiting occur commonly with cyclophosphamide, especially at high doses; some clinicians reported that these effects respond to treatment with antiemetics. Occasionally, diarrhea, hemorrhagic colitis, mucosal irritation, and oral ulceration have been reported. Rarely, aphthous stomatitis, enterocolitis, and hepatotoxicity as evidenced by jaundice and hepatic dysfunction have occurred.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Alopecia occurs frequently in patients who receive cyclophosphamide and patients should be forewarned of this possibility. In usual doses, about 33% of patients who receive the drug experience alopecia, generally beginning about 3 weeks after initiation of therapy; the condition is usually reversible but new hair may be a different color or texture. Transverse ridging, retarded growth, and/or pigmentation of fingernails may occur, as well as skin pigmentation. Nonspecific dermatitis has also been reported.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

Other reported adverse effects of cyclophosphamide include headache, dizziness, and myxedema. Faintness, facial flushing, diaphoresis, and oropharyngeal sensation have occurred following IV administration of cyclophosphamide, have been reported. The drug may interfere with normal wound healing.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements).,p. 960-1]**PEER REVIEWED**

Some patients who have received cyclophosphamide alone, as part of a combination regimen, or as adjunctive therapy have developed secondary malignancies, most frequently urinary bladder, myeloproliferative, & lymphoproliferative malignancies. Although a causal relationship has not been definitely established, the possibility of development of a secondary malignancy should be considered in weighing the possible benefit from the drug against the potential risk. Secondary malignancies have occurred most frequently in patients who have been treated with cyclophosphamide for primary myeloproliferative & lymphoproliferative malignancies & primary nonmalignant diseases in which immune processes are believed to be involved. Secondary urinary bladder malignancies generally have occurred in patients who previously developed hemorrhagic cystitis. In some cases, the secondary malignancy was not detected until several years after discontinuance of cyclophosphamide therapy. Long-term follow-up of women who received cyclophosphamide-containing adjuvant chemotherapy regimens for the treatment of early breast cancer indicates that the incidence of other solid tumors & secondary leukemia in these women is not substantially greater than that in the general population.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 961]**PEER REVIEWED**

CAREFUL EVALUATION OF BONE MARROW FUNCTION IS IMPERATIVE AND PROLONGED THERAPY IS GUIDED BY KEEPING THE TOTAL LEUKOCYTE COUNT BETWEEN 2500 AND 4000 CELLS PER CUBIC MILLIMETER OF BLOOD OR BY OBTAINING THE DESIRED RESPONSE OF THE TUMOR.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1218]**PEER REVIEWED**

Potentially fatal cardiotoxicity also has occurred when cyclophosphamide (given concomitantly with mesna /2-mercaptoethane sulfonic acid sodium salt/ and followed with autologous bone marrow transplant) was administered inadvertently in a dosage of 4 g/sq m daily for 4 doses rather than in a total dose of 4 g/sq m administered over 4 days in equally divided doses of 1 g/sq m daily as part of a phase I protocol.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

One of the major and dose limiting adverse effects of cyclophosphamide is hematologic toxicity, which is usually reversible after discontinuance of the drug. Hematopoietic adverse effects include leukopenia, thrombocytopenia, hypothrombinemia, and anemia. Leukopenia is considered to be an expected effect of cyclophosphamide therapy and may be severe. Leukopenia nadirs generally occur at 8-15 days following a single dose of cyclophosphamide and recovery usually occurs within 17-28 days. Thrombocytopenia is reportedly less common, with nadirs occurring 10-15 days after administration of the drug. Anemia, particularly after large doses or prolonged therapy, and rarely hypoprothrombinemia have been reported. Rarely, cyclophosphamide has been reported to produce positive direct antiglobulin (Coombs') test results and hemolytic anemia.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

In children treated with cyclophosphamide a transient blurring of vision has been reported in 5 out of 59, coming on in minutes after intravenous injection in two and within 24 hours in the other three. The duration of blurring ranged from one hour to two weeks, but vision returned to normal in all.
[Grant, W.M. Toxicology of the Eye. 3rd ed. Springfield, IL: Charles C. Thomas Publisher, 1986. 299]**PEER REVIEWED**

Cyclophosphamide can cause sterility in people of either sex. It can damage the germinal cells in prepubertal, pubertal and adult males, and causes premature ovarian failure in females.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 180 (1981)]**PEER REVIEWED**

... To analyse the treatment-related complications of busulphan and cyclophosphamide (BU-CY) as the conditioning regimen for allogeneic peripheral blood stem cell transplantation (allo-PBSCT). ... The clinical data of 40 leukemia patients undergoing allo-PBSCT between June 1997 and May 1999 in our BMT center were retrospectively analysed. ... Recovery of neutrophil and platelet was achieved at a median of day +13 (9 similar 28) and day +12 (7 similar 60) respectively. Acute GVHD occurred in 17 of 40 patients (42.5%) with grade II-IV in 10 patients (25%). Chronic GVHD developed in 21 out of 30 evaluable patients (70%). Mild to severe mucositis occurred in 30 patients (75%), and 4 of them had severe esophagitis with bleeding. Haemorrhagic cystitis developed in 8/40 (20%) patients, the median time of its onset was day +100 (+7 to +165). Six of 40 patients (15%) developed interstitial pneumonia (IP), 5 of them were due to cytomegalovirus infection, and the remaining one due to pneumocystis carinii infection. No hepatic veno-occlusive disease was observed and no seizure occurred. During the median follow-up of 480 (300 similar 1000) days, 4 (10%) patients relapsed and 8 (20%) patients died of the transplant-related complications. The 3 year leukemia-free survival rate was 70%. ... BU (domestic busulfan)-CY regimen is relatively easy to administer and well tolerated, with low extramedullary toxicities.
[Zhu K, et al; Zhonghua Xue Ye Xue Za Zhi 21 (8): 403-405. 2000.]**PEER REVIEWED**

... We now described five patients receiving monthly cycles of iv CP /cyclophosphamide/ whose allergic reactions included clinical features of type I hypersensitivity but were atypical in their markedly delayed onset (i.e., 8 to 16 hr in patients 1 to 4 and 10 days in patient 5) ... The objective was to investigate these late-developing clinical reactions by skin testing with CP and two of its major metabolites ... The five patients and a control group receiving iv CP uneventfully were studied by the same skin test protocol ... The four individual in the control group were unreactive to CP or its metabolites. All five patients with late-onset allergic reactions had positive immediate skin test results to CP metabolites but not to CP itself. We propose that the allergic reactions in patients 1 to 4 were mediated, wholly or in major part, by IgE antibodies reactive with allergens derived from time-dependent drug metabolites.
[Popescu NA et al; J Allergy Clin Immunol 97 (1 Pt 1): 26-33 (1996)]**PEER REVIEWED**

Sterile hemorrhagic cystitis has been reported to occur in up to 20% of patients (especially children) on long-term cyclophosphamide therapy. The effect, which rarely can be severe and even fatal, is attributed to chemical irritation by active metabolites of cyclophosphamide that accumulate in concentrated urine. Hematuria usually resolves spontaneously within a few days after discontinuance of cyclophosphamide therapy but may persist for several months. Fibrosis of the bladder (sometimes extensive), with or without cystitis, also has occurred, but less frequently. Atypical epithelial cells may be found in the urinary sediment. These adverse effects appear to be related to the dosage and duration of cyclophosphamide therapy. Nephrotoxicity, including hemorrhagic ureteritis and renal tubular necrosis, has been reported; such lesions reportedly resolve in most instances following discontinuance of cyclophosphamide therapy.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 960]**PEER REVIEWED**

THERE HAVE BEEN AT LEAST 30 CASE REPORTS OF MALIGNANCY IN PATIENTS TREATED WITH CYCLOPHOSPHAMIDE FOR NONMALIGNANT DISORDERS, MAINLY RHEUMATOID ARTHRITIS AND CHRONIC GLOMERULONEPHRITIS. THESE INCLUDED 17 ACUTE NONLYMPHOCYTIC LEUKEMIAS, ONE CHRONIC NONLYMPHOCYTIC LEUKEMIA, ONE ACUTE LYMPHOCYTIC LEUKEMIA, ONE CHRONIC LYMPHOCYTIC LEUKEMIA, TWO BLADDER CANCERS, ONE SQUAMOUS CELL CANCER OF THE SKIN, THREE RETICULUM CELL SARCOMAS, ONE HODGKIN'S DISEASE, ONE MELANOMA, TWO CEREBRAL GLIOMAS, ONE CERVICAL CANCER AND ONE PLEURAL SARCOMA. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 182 (1981)]**PEER REVIEWED**

Gonadal suppression, resulting in amenorrhea or azoospermia, may occur in patients taking antineoplastic therapy, especially with the alkylating agents. In general, these effects appear to be related to dose & length of therapy & may be irreversible. Prediction of the degree of testicular or ovarian function impairment is complicated by the common use of combinations of several antineoplastics, which makes it difficult to assess the effects of individual agents. However, there have been numerous reports of gonadal suppression with use of cyclophosphamide, which seems to depend on dose, duration, & state of gonadal function at the time of therapy, sterility may be irreversible in some patients.
[McEvoy, G.K. (ed.). American Hospital Formulary Service- Drug Information 2002. Bethesda, MD: American Society of Health-System Pharmacists, Inc. 2002 (Plus Supplements). 1102]**PEER REVIEWED**

THERE WAS INCR IN NUMBER OF CHROMOSOMAL ABERRATIONS IN THE PERIPHERAL BLOOD LYMPHOCYTES OF CHILDREN TREATED WITH CYCLOPHOSPHAMIDE (3-5 MG/DAY FOR 6-8 MONTHS) FOR NONMALIGNANT CONDITIONS & OF PATIENTS WITH RHEUMATOID ARTHRITIS FOLLOWING CYCLOPHOSPHAMIDE TREATMENT. SIMILAR INCR WERE OBSERVED IN LYMPHOCYTES OF WOMEN WITH RECURRENT OVARIAN OR UTERAL CARCINOMA 3 OR 24 HR AFTER AN IV ADMIN OF 2.0 G & IN THE BONE MARROW & LYMPH NODE CELLS OF PATIENTS WITH LYMPHOGRANULOMATOSIS 24-72 HR AFTER SINGLE DOSE OF 400 MG CYCLOPHOSPHAMIDE. INCR LEVELS OF SISTER CHROMATID EXCHANGE IN PERIPHERAL BLOOD LYMPHOCYTES HAVE BEEN OBSERVED IN PATIENTS TREATED WITH CYCLOPHOSPHAMIDE. THESE HAVE INCLUDED PATIENTS WITH MALIGNANT LYMPHOMA & NEPHROTIC SYNDROME, A PATIENT WITH RETICULOSARCOMA, 3 PATIENTS WITH UNSPECIFIED MALIGNANT TUMORS & 1 PATIENT WITH ACUTE GLOMERULONEPHRITIS. /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 181 (1981)]**PEER REVIEWED**

LEUKOPENIA IS INEVITABLE SIDE EFFECT & IS USED AS INDEX OF DOSAGE ... HYPOPROTHROMBINEMIA ... .
[Osol, A. (ed.). Remington's Pharmaceutical Sciences. 16th ed. Easton, Pennsylvania: Mack Publishing Co., 1980. 1088]**PEER REVIEWED**

Nausea & vomiting, myelosuppression with platelet sparing, & alopecia are common to virtually all regimens using cyclophosphamide. Mucosal ulcerations &, less frequently, interstitial pulmonary fibrosis also may result from cyclophosphamide treatment. Extravasation of the drug into subcutaneous tissues does not produce local reactions, & thrombophlebitis does not complicate iv admin. The occurrence of sterile hemorrhagic cystitis has been reported in 5%-10% of patients. As noted above, this has been attributed to chemical irritation produced by acrolein. Its incidence is significantly reduced by coadministration of mesna. For routine clinical use, ample fluid intake is recommended. Admin of the drug should be interrupted at the first indication of dysuria or hematuria. The syndrome of inappropriate secretion of antidiuretic hormone (ADH) has been observed in patients receiving cyclophosphamide, usually at doses higher then 50 mg/kg. It is important to be aware of the possibility of water intoxication, since these patients usually are vigorously hydrated.
[Hardman, J.G., L.E. Limbird, P.B. Molinoff, R.W. Ruddon, A.G. Goodman (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 9th ed. New York, NY: McGraw-Hill, 1996. 1395]**PEER REVIEWED**

 

Interactions:

PRIOR TREATMENT WITH ALLOPURINOL SIGNIFICANTLY PROLONGS /THE HALF-LIFE OF CYCLOPHOSPHAMIDE/.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1217]**PEER REVIEWED**

CYCLOPHOSPHAMIDE MAY ENHANCE NEUROMUSCULAR BLOCKADE PRODUCED BY SUCCINYLCHOLINE BY INHIBITING ITS METABOLISM.
[Evaluations of Drug Interactions. 2nd ed. and supplements. Washington, DC: American Pharmaceutical Assn., 1976, 1978. 600]**PEER REVIEWED**

THE ENZYME INHIBITOR SKF 525-A, WHICH INCREASES THE TERATOGENICITY OF CYCLOPHOSPHAMIDE, CAUSED AN INCREASE IN THE CONCN OF CYCLOPHOSPHAMIDE IN THE MOUSE EMBRYO & ALSO CAUSED A DECREASE IN METABOLITE FORMATION AFTER ADMIN OF CYCLOPHOSPHAMIDE TO PREGNANT MICE.
[The Chemical Society. Foreign Compound Metabolism in Mammals. Volume 2: A Review of the Literature Published Between 1970 and 1971. London: The Chemical Society, 1972. 434]**PEER REVIEWED**

Cultured human osteosarcoma cell lines (OST strain and HT 1080) and specimens obtained during surgery on humans (osteosarcoma, malignant fibrous histiocytoma, rhabdomyosarcoma, epithelioid sarcoma, mesenchymal chondrosarcoma, synovial sarcoma, leiomyosarcoma, and malignant giant cell tumor) were used to study the synergistic effect of caffeine on anticancer drugs, including cyclophosphamide as its active form 4-hydroxyperoxycyclophosphamide. Cell concentrations were 10,000 per dish for the osteosarcoma strain, 50,000 per dish for the HT 1080 strain, and 100,000 to 500,000 for the fresh cells. After a 1 hour exposure of the cells to the anticancer agent, caffeine was added to the top layer for the subsequent 10 day to 3 week combined exposure. Treatment with 3.0 ug/ml (1/10 of the usual peak plasma concentration) cyclophosphamide alone showed colony inhibition of 14.2% in the OST strain and 8.5% in the HT 1080 strain. Addition of 0.2 mM caffeine showed synergism, 27.8% and 56.2% inhibition, respectively. When 2 mM caffeine was used with cyclophosphamide, colony inhibition was 57.1% in the OST strain. At a cyclophosphamide concentration of 0.3 ug/ml and either 0.2 or 2 mM caffeine, synergism still was observed. Using fresh human tumor specimens with cyclophosphamide alone (3.0 ug/ml) 4 of 18 specimens showed positive sensitivity. With 2 mM caffeine exposure in combination, 8 of 18 specimens (44.4%) showed a significant synergistic effect; of these, 7 showed positive sensitivity. An additive effect was observed in one specimen and a subadditive effect in 3 specimens. Continuous exposure to 0.2 mM caffeine in combination resulted in significant synergism in specimens. For comparison, caffeine alone at 0.2 mM produced colony inhibition of 9.2% (OST strain) and 12.5% (HT 10890 strain) in the cultured cells; at 2.0 mM, 15.0% (OST strain) and 100.0% (HT 1080 strain). In fresh sarcoma specimens, caffeine alone at 2 mM produced inhibition of 0.0% to 48.2% (mean, 19.1%) and there was no case with positive sensitivity.
[Tomita K, Tsuchiya H; Jpn J Cancer Res 80 (1): 83-8 (1989)]**PEER REVIEWED**

DBA/2NCr1BR F1 mice received a single iv injection of cyclophosphamide (70, 120 or 200 mg/kg) alone or 2 hr before an ip injection of 1,000 mg/kg of diethyldithiocarbamate. 24 hr after, survival of bone marrow colony forming units spleen and granulocyte macrophage colony forming cells, was determined. On the whole, administration of diethyldithiocarbamate reduced the toxic effect of cyclophosphamide on hemopoietic progenitors. The effect was in general more evident at the lower than at the higher doses of the antitumor drug.
[Pannacciulli IM et al; Br J Cancer 59 (3): 371-4 (1989)]**PEER REVIEWED**

Leukopenic and/or thrombocytopenic effects of cyclophosphamide may be increased with concurrent use or recent therapy if these medications /blood dyscrasia-causing medications/ cause the same effects; dosage adjustment of cyclophosphamide, if necessary, should be based on blood counts.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Additive bone marrow depression may occur; dosage reduction may be required when two or more bone marrow depressants, including radiation, are used concurrently or consecutively /with cyclophosphamide/.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Cyclophosphamide may raise the concentration of blood uric acid; dosage adjustment of antigout agents /allopurinol or colchicine or probenecid or sulfinpyrazone/ my be necessary to control hyperuricemia and gout; uricosuric antigout agents may increase risk of uric acid nephropathy. Concurrent use with allopurinol may enhance the bone marrow toxicity of cyclophosphamide; if concurrent use is required, close observation of toxic effects should be considered.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Inhibition of cholinesterase activity by cyclophosphamide reduces or slows cocaine metabolism, thereby increasing and/or prolonging its effects and increasing the risk of toxicity.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use of high-dose cytarabine with cyclophosphamide for bone marrow transplant preparation has bee reported to result in an increase in cardiomyopathy with subsequent death.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use /of daunorubicin or doxorubicin/ with cyclophosphamide may result in increased cardiotoxicity; it is recommended that the total dose of daunorubicin or doxorubicin not exceed 400 mg/sq m of body surface.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

These agents /hepatic enzyme inducers/ may induce microsomal metabolism to increase formation of alkylating metabolites of cyclophosphamide, thereby reducing the half-life and increasing the activity of cyclophosphamide.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use of other immunosuppressants such as: azathioprine; chlorambucil; corticosteroids, glucocorticoid; cyclosporine; mercaptopurine; muromonab-CD3/ with cyclophosphamide may increase the risk of infection and development of neoplasms.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Concurrent use /of lovastatin with cyclophosphamide/ in cardiac transplant patients may be associated with an increased risk of rhabdomyolysis and acute renal failure.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

Cyclophosphamide may decrease plasma concentrations or activity of pseudocholinesterase, the enzyme that metabolizes succinylcholine, thereby enhancing the neuromuscular blockage of succinylcholine. Increased or prolonged respiratory depression or paralysis (apnea) may occur but is of minor clinical significance while the patient is being mechanically ventilated; however, caution and careful monitoring of the patient are recommended during and following concurrent or sequential use, especially if there is a possibility of incomplete reversal of neuromuscular blockage postoperatively.
[MICROMEDEX Thomson Health Care. USPDI - Drug Information for the Health Care Professional. 22nd ed. Volume 1. MICROMEDEX Thomson Health Care, GreenwoodVillage, CO. 2002. Content Reviewed and Approved by the U.S. Pharmacopeial Convention, Inc. 1103]**PEER REVIEWED**

The effect of high molecular carboxymethyl-chitin-glucan (CMCG), admin either ip, iv or orally prior to cyclophosphamide injection, on the frequency of micronucleated reticulocytes was evaluated in peripheral blood of female ICR mice. Both ip and iv admin of CMCG decreased the clastogenic effect of cyclophosphamide. The protective effect of CMCG was concn dependent, with a higher decrease achieved by 100 mg/kg than by 50 mg/kg body weight. On the other hand, no even five peroral pretreatments with CMCG in the dose of 200 mg/kg body weight during the week prior to simultaneous admin of CMCG and cyclophosphamide induced a decrease of micronucleated reticulocytes in peripheral blood.
[Chorvatovi cov'a D and J Sandula; Mutat Res 346 (1): 43-8 (1995)]**PEER REVIEWED**

Synergistically enhanced sister chromatid exchange (SCE) frequency by cyclophosphamide (CP) was observed when L1210 lymphoid tumor cells were exposed in vivo to a non-toxic concn of 3-aminobenzamide (3-AB). Additive effects in SCE induction in vivo were observed when either Ehrlich ascites tumor (EAT) cells or P388 lymphocytic leukemia cells treated with CP were exposed to 3-AB in vivo. 3-AB enhanced the survival time of L1210 tumor bearing BDF1 mice treated with CP. However, the combined CP plus 3-AB treatment did not increase the survival of either EAT BALB/c- or P388 BDF1-tumor bearing mice compared with the effect on survival by CP alone. Therefore the in vivo differential antitumor effect, by CP in conjunction with 3-AB, appears to correlated well with the in vivo differential effect on cytogenetic damage caused by the combined CP plus 3-AB treatment. In the Salmonella typhimurium/mammalian microsome test CP appears to have a dose dependent ability to induce base-pair substitutions in strains TA 100 and TA 1535 and frameshift mutations in strains TA 98 and TA 1537. Both types of mutation were synergistically increased in the presence of 3-AB.
[Eliopoulos P et al; Mutat Res 342 (3-4): 141-6 (1995)]**PEER REVIEWED**

Treatment with Caralluma tuberculata extract induced complex biochemical and cytological changes in mice. Its cytotoxicity in the bone marrow cells of mice was comparable with that of the standard drug cyclophosphamide (C); however, unlike C, C. tuberculata was not clastogenic (as shown by the micronucleus assay). A dose-dependent decrease in the RNA content of liver and testes was produced by C. tuberculata treatment whereas there was no effect on the content of nucleic acid and protein in the brain. In the extract-treated animals there was a significant and dose-dependent increase in the DNA content of the liver, with a negligible effect on the protein content. Combined treatment with C. tuberculata and C showed that C. tuberculata diminished the effect of C on DNA levels; however, RNA levels were further suppressed, resulting in increased cytotoxicity. Pretreatment with C. tuberculata extract significantly reduced the clastogenicity of C. These results indicated the involvement of different phytoconstituents acting by different routes.
[al-Bekairi AM et al; Food Chem Toxicol 30 (8): 719-22 (1992)]**PEER REVIEWED**

The effect of pretreatment with carboxymethylglucan (CMG) on the frequency of micronuclei induced by cyclophosphamide administration in mice was evaluated. Two doses of CMG (50 mg/kg body weight) injected either intraperitoneally 24 hr or intravenously 1 hr prior to two cyclophosphamide administrations (80 mg/kg) significantly decreased the frequency of micronucleated PCE in bone marrow. Of two evaluated derivatives of carboxymethylglucan, the K3 derivative was most efficient. The results show that it is possible to achieve a suppressive effect of soluble carboxymethylglucan prepared from Saccharomyces cerevisiae against cyclophosphamide mutagenicity. The notion may be useful for glucan's effects against pharmacocarcinogenesis. Therapeutic application of glucan with cyclophosphamide therapy may provide a remarkable decrease of the secondary tumor risk. The utilization of these results for human patients needs to be considered.
[Chorvatovi cov'a D, Navarov'a J; Mutat Res 282 (3): 147-50 (1992)]**PEER REVIEWED**

The modulatory effect of vitamin C (Vit C) on the mutagenic effect of the antineoplastic drug cyclophosphamide (CP) was assessed in the in vivo micronucleus test in Swiss mice. Simultaneous oral administration of Vit C with ip administration of CP was found to decrease the frequency of micronucleated polychromatic erythrocytes elevated by CP. Vit C exhibited a significant antimutagenic effect over a wide dose range (1.56-200 mg/kg). The dose-response relationship was highly significant. These results demonstrated the ability of the in vivo micronucleus test to detect in vivo modulation of CP mutagenicity by Vit C. Our earlier results and those from other laboratories also indicate that this model system is suitable for primary in vivo screening of modulation of mutagenesis.
[Ghaskadbi S et al; Teratog Carcinog Mutagen 12 (1): 11-7 (1992)]**PEER REVIEWED**

A total of 78 patients with second recurrence or progression of histologically verified breast cancer were treated with single-agent cyclophosphamide given at 2.5 g/sq m by iv infusion every 3 wk along with mesna support. All had previously been treated with epirubicin and cisplatin or epirubicin alone. Toxicity was predominantly hematologic: WHO grade III+IV toxicity was found in 95% of cases. The overall response rate was 26.7% (95% CI, 15.8-41.4%), with 7% of patients achieving a complete response (CR) and 19.7%, a partial response (PR). The median duration of CRs and PRs was 11 and 5 mo, respectively. The response rate observed for patients previously treated with epirubicin alone was 30.5% in contrast to the 8.3% recorded for patients previously treated with cisplatin plus epirubicin. Thus, an indication of cross-resistance was absent between cyclophosphamide and epirubicin but possible between cyclophosphamide and cisplatin.
[Hansen F et al; Cancer Chemother Pharmacol 37 (4): 377-81 (1996)]**PEER REVIEWED**

The effect of WR-2721 against cyclophosphamide-induced clastogenicity was studied using the in vivo micronucleus assay. The frequency of micronuclei in polychromatic erythrocytes in the peripheral blood of mice treated with WR-2721 and cyclophosphamide (CP), each of the cmpd at a dose of 200 mg/kg body weight, was evaluated during the 15-day period. The suppressing effect of WR-2721, given 30 min prior to CP admin, on micronuclei induced by the alkylating agent was demonstrated ... The modulatory effect of WR-2721 on the clastogenic activity of CP in the erythropoietic system by the mouse micronucleus test was shown.
[Czy'zewska A and L Mazur; Teratog Carcinog Mutagen 15 (3): 109-14 (1995)]**PEER REVIEWED**

/It was/ ... demonstrated in an earlier paper that capsaicin, the pungent principle of red hot chili, has a potent anti-oxidant property that interferes with free-radical involved mechanisms. In the present paper we demonstrate that capsaicin significantly inhibits cyclophosphamide-induced (ip) chromosomal aberrations and DNA strand breakages. This protective action of capsaicin against CP-induced toxicity may possibly be linked with its already reported 'desensitization' effect against chemical irritant-induced damages.
[De AK et al; Mutat Res 335 (3): 253-8 (1995)]**PEER REVIEWED**

In the rat, the mortality from cyclophosphamide had prevented the administration of sufficient dosages to produce detectible damage to stem spermatogonia. To overcome this problem, we used bone marrow transplantation and sodium 2-mercaptoethanesulfonate (Mesna) treatment to raise the lethal dose for 50% of the animals (LD50) for cyclophosphamide from 275 to > 400 mg/kg body weight. In addition we used irradiation, 2 weeks prior to injection of cyclophosphamide, to greatly enhance the measured toxicity of cyclophosphamide towards stem spermatogonia. Whereas sperm counts at 9 weeks after a 300 mg/kg cyclophosphamide dose were reduced by only a factor of 1.6 without prior irradiation, they were reduced by a factor of 60 when 2.5 Gy of irradiation had been given. Dramatic protection against this toxicity was produced by hormone treatment with a gonadotropin-releasing hormone (GnRH) antagonist (Nal-Glu) and an antiandrogen (flutamide) following the radiation but prior to cyclophosphamide. This hormone treatment did not modify the stem cell toxicity of the radiation and it therefore must be protecting stem cells against cyclophosphamide-induced damage.
[Meistrich ML et al; J Androl 16 (4): 334-41 (1995)]**PEER REVIEWED**

Hamster to rat renal xenotransplantation was performed with recipient nephrectomies. Recipients were treated beginning on day 0 with continuous FK 506 monotherapy, a 7-day or open-ended monotherapeutic course of cyclophosphamide (CP), and the two drug regiments combined. CP alone (10 mg/kg/day) prevented a xenospecific antibody response and tripled median survival of the kidney (defined as recipient death) from 6 (control) to 18.5 days whereas FK 506 alone had no effect. The drugs in combination were no better than CP alone (15 days) unless the 5-day course of CP was given at a higher dose (15 mg/kg) and started 3 days preoperatively (79 days). In further experiments, adjuvant measures were added to the minimally effective FK 506/7-day CP regimen which gave a median survival of only 15 days. In the most successful modification, intraoperative antibody depletion by the temporary transplantation of third party hamster liver or en bloc kidneys increased median survival from 15 to 34 and 48 days, respectively. An intraoperative i.v. dose administration of the anticomplement drug K76 instead of antibody depletion increased survival to 26 days. Although the events of kidney rejection were similar to those of heart xenografts and partially forestalled by the antibody inhibiting CP treatment, or by antibody depletion, survival for > 100 days was accomplished in only 5 of 86 treated animals.
[Miyazawa H et al; Transplantation 59 (8): 1183-8 (1995)]**PEER REVIEWED**

Hemorrhagic cystitis is a common problem following cyclophosphamide or radiation therapy. Chitosan has been shown to be an effective hemostatic agent and promoter of wound healing in animal experiments. We evaluated the safety and efficacy of intravesical chitosan in an animal model of cyclophosphamide cystitis. Hemorrhagic cystitis was induced in female F344 rats by intraperitoneal cyclophosphamide, 100 mg/kg Chitosan soln (0.3 ml) was instilled intravesically on day 1 (Group 1), on days 1, 3, and 5 (Group 2), or 1 hr after the admin of cyclophosphamide (Group 3). The rats in group 4 were treated with chitosan diluent on day 1 after cyclophosphamide, and the rats in group 5 received intravesical chitosan without cyclophosphamide. Sequential examination revealed decr mortality and lower incidences of severe bladder bleeding, necrosis and inflammation in Group 3. Treatment delayed until after the appearance of the cystitis, esp repeated treatments, appeared to make the cyclophosphamide-induced changes worse. Used within 1 hr of cyclophosphamide admin, before the cystitis develops, chitosan seemed to have the possibility to inhibit the appearance of hemorrhagic cystitis. In addition to the changes in the bladder, severe changes occurred in the kidneys secondary to cyclophosphamide.
[Okamura T et al; Hinyokika Kiyo 41 (4): 289-96 (1995)]**PEER REVIEWED**

The effect of pretreatment with miltefosine (MIL) on the antineoplastic activity of cyclophosphamide (CPA) was evaluated in sc benzo(a)pyrene-induced sarcomas (BPS) of the rat. MIL alone had no antineoplastic effect on this autochthonous tumor, but enhanced the chemotherapeutic effect of CPA. Conversely, MIL counteracted the myelotoxicity of CPA in normal adult rats. Although the nadir of the leucocyte count remained unchanged, the recovery phase was considerably shortened, an effect which resembled the pharmacological action of GM-CSF.
[Stekar J et al; Eur J Cancer 31A (3): 372-4 (1995)]**PEER REVIEWED**

The effect of protein malnutrition and alcohol consumption on the yield of chromosomal damage induced by cyclophosphamide (CP) was studied. Chromosomal damage induced in bone marrow cells of BALB/c mice was established by scoring the frequency of dicentric chromosomes in C-banded slides. Results obtained showed that CP induced a significant incr of chromosomal damage in comparison with untreated mice. In addition, the yield of dicentric chromosomes was higher in mice fed with the hypoproteic diet. The animals which received ethanol in drinking water before treatment with CP exhibited the highest frequency of dicentric chromosomes, with no relation with the diet.
[Terreros MC et al; J Vet Med Sci 57 (1): 5-8 (1995)]**PEER REVIEWED**

Cyclophosphamide causes lung injury in rats through its ability to generate free radicals with subsequent endothelial and epithelial cell damage. In order to observe the protective effects of a potent anti-inflammatory antioxidant, curcumin (diferuloyl methane) on cyclophosphamide-induced early lung injury, healthy, pathogen free male Wistar rats were exposed to 20 mg/100 g body weight of cyclophosphamide, intraperitoneally as a single injection. Prior to cyclophosphamide intoxication oral administration of curcumin was performed daily for 7 days. At various time intervals (2, 3, 5 and 7 days post insult) serum and lung samples were analyzed for angiotensin converting enzyme, lipid peroxidation, reduced glutathione and ascorbic acid Bronchoalveolar lavage fluid was analyzed for biochemical constituents. The lavage cells were examined for lipid peroxidation and glutathione content. Excised lungs were analyzed for antioxidant enzyme levels. Biochemical analyses revealed time course increases in lavage fluid total protein, albumin, angio+ensin converting enzyme (ACE), lactate dehydrogenase, N-acetyl-beta-D-glucosaminidase, alkaline phosphatase, acid phosphatase, lipid peroxide levels and decreased levels of glutathione (GSH) and ascorbic acid 2, 3, 5 and 7 days after cyclophosphamide intoxication. Increased levels of lipid peroxidation and decreased levels of glutathione and ascorbic acid were seen in serum, lung tissue and lavage cells of cyclophosphamide groups. Serum angiotensin converting enzyme activity increased which coincided with the decrease in lung tissue levels. Activities of antioxidant enzymes were reduced with time in the lungs of cyclophosphamide groups.
[Venkatesan N and G Chandrakasan; Mol Cell Biochem 142 (1) 79-87 (1995)]**PEER REVIEWED**

 

Maximum Drug Dose:

A total of 23 patients were treated at five dose escalations with high dose combination cyclophosphamide, cis-platin, and melphalan with autologous bone marrow support. The max tolerated doses of cyclophosphamide, cis-platin, and melphalan were 5,525, 180, and 80 mg/sq m, respectively. The dose limiting toxicity was cardiac toxicity. Objective tumor regression occurred in 14 of 18 evaluable cases, with a median duration of 3.5 mo.
[Peters WP et al; Cancer Chemother Pharmacol 23 (6): 377-83 (1989)]**PEER REVIEWED**

 

Environmental Fate & Exposure:

 

 

Environmental Fate/Exposure Summary:

Cyclophosphamide's production and use as antineoplastic may result in its release to the environment through various waste streams. If released to air, an estimated vapor pressure of 4.5 mm Hg at 25 deg C indicates cyclophosphamide will exist in both the vapor and particulate phases in the ambient atmosphere. Vapor-phase cyclophosphamide will be degraded in the atmosphere by reaction with photochemically-produced hydroxyl radicals; the half-life for this reaction in air is estimated to be 5.5 hrs. Particulate-phase cyclophosphamide will be removed from the atmosphere by wet and dry deposition. Cyclophosphamide is sensitive to light. If released to soil, cyclophosphamide is expected to have high mobility based upon an estimated Koc of 52. Volatilization from moist soil surfaces is not expected to be an important fate process based upon an estimated Henry's Law constant of 1.4X10-11 atm-cu m/mole. Cyclophosphamide has shown to be non-biodegradable using sewage sludge tests. If released into water, cyclophosphamide is not expected to adsorb to suspended solids and sediment based upon the estimated Koc. Volatilization from water surfaces is not expected to be an important fate process based upon this compound's estimated Henry's Law constant. An estimated BCF of 3 suggests the potential for bioconcentration in aquatic organisms is low. The neutral hydrolysis calculated half-life for cyclophosphamide at 25 deg C is 41 days. Occupational exposure to cyclophosphamide may occur through inhalation and dermal contact with this compound at workplaces where cyclophosphamide is produced or used. Workers involved in formulating and dispensing the drug may be exposed through dermal contact (with the dry powder or solutions), or inhalation of dust. Direct human exposure occurs through ingestion of the drug (when dispensed in tablet form) and through injection (when administered intravenously). (SRC)
**PEER REVIEWED**

 

Probable Routes of Human Exposure:

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The danger to health-care personnel from handling a hazardous drug stems from a combination of its inherent toxicity and the extent to which workers are exposed to the drug in the course of carrying out their duties. This exposure may be through inadvertent ingestion of the drug on foodstuffs (eg, workers' lunches), inhalation of drug dusts or droplets or direct skin contact. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 752]**PEER REVIEWED**

NIOSH (NOES Survey 1981-1983) has statistically estimated that 30,026 workers (20,745 of these are female) are potentially exposed to cyclophosphamide in the US(1). Occupational exposure to cyclophosphamide may occur through inhalation and dermal contact with this compound at workplaces where cyclophosphamide is produced or used(SRC). Workers involved in formulating and dispensing the drug may be exposed through dermal contact (with the dry powder or solutions), or inhalation of dust(SRC). Direct human exposure occurs through ingestion of the drug (when dispensed in tablet form) and through injection (when administered intravenously)(2).
[(1) NIOSH; National Occupational Exposure Survey (NOES) (1983) (2) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Lyon, France: World Health Org, Inter Agency Res Cancer 26: 165-202 (1981)]**PEER REVIEWED**

Air monitoring conducted in a West German manufacturing facility in April 1984 found cyclophosphamide levels ranging from 0.1 to 810 ug/cu m(1). Air concentrations of 2-480 ug/cu m were detected in a production area of a plant involved weighing cyclophosphamide and formulating it into tablets(1). No detectable levels (detection limit of 0.05 ug/cu m) were found in air samples (taken from flow hoods) from a hospital dispensing and administering cyclophosphamide; however, filter media from the flow hoods contained measurable quantities suggesting that some exposure can occur(1). Concentrations of cyclophosphamide in personal air samplers from a manufacturing facility ranged from less than the detection limit to 97.0 ug/cu m, and in a laminar-flow hood, the concentrations ranged from 0-60 ng/cu m(2).
[(1) Pyy, L et al; Am Ind Hyd Assoc J 49: 314-317 (1988) (2) Sorsa, M et al; Mutat Res 204: 465-79 (1988)]**PEER REVIEWED**

 

Body Burden:

In a cross-sectional study, the urine of 20 hospital workers occupationally exposed to cyclophosphamide and 21 unexposed controls was monitored for excretion of cyclophosphamide. During the week in which samples were collected, most of the workers handled cyclophosphamide fewer than 5 times and the amount handled each time ranged from 100-1000 mg (mean +/- 350 mg). All workers claimed to have taken regular safety precautions, ie, at least wearing gloves during handling. The drug was identified in 5 cases (range: 0.7-2.5 ug excreted/24 hr urine). A clear relationship between cyclophosphamide handling and urinary detection was shown. 4 of 5 persons with detectable urinary cyclophosphamide had handled cyclophosphamide 10 times or more during the week.
[Evelo CTA et al; Int Arch Occup Environ Health 58: 151-5 (1986)]**PEER REVIEWED**

Cyclophosphamide (along with ifosfamide) was detected in the urine of 8 pharmacy technicians and nurses (along with ifosfamide) at amounts ranging from <0.001-0.5 ug(1). 21 nurses and pharmacy personnel in a Munich, Germany hospital were monitored for compound exposure; on days when 3,900 mg/l cyclophosphamide was mixed, 12 of 31 urine samples tested positive with concentrations ranging from 3.5 to 38 ug/24 hr urine(2).
[(1) Sessink, PJM et al; Int Arch Occup Environ Health 64: 105-112 (1992) (2) Ensslin AS et al; Occup Environ Med 51: 229-33 (1994)]**PEER REVIEWED**

 

Natural Pollution Sources:

Cyclophosphamide is not known to occur in nature(1).
[(1) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva, Switzerland: World Health Org, Inter Agency Res Cancer, 9: 135-56 (1975)]**PEER REVIEWED**

 

Artificial Pollution Sources:

Cyclophosphamide's production and use as an antineoplastic(1) may result in its release to the environment through various waste streams(SRC).
[(1) Lewis RJ, Sr, ed; Hawley's Condensed Chemical Dictionary. 13th ed. NY, NY: John Wiley & Sons, Inc. p. 327 (1997)]**PEER REVIEWED**

 

Environmental Fate:

TERRESTRIAL FATE: Based on a classification scheme(1), an estimated Koc value of 52(SRC), determined from a log Kow of 0.63(2) and a regression-derived equation(3), indicates that cyclophosphamide is expected to have high mobility in soil(SRC). Volatilization of cyclophosphamide from moist soil surfaces is not expected to be an important fate process(SRC) given an estimated Henry's Law constant of 1.4X10-11 atm-cu m/mole(SRC), using a fragment constant estimation method(4). Cyclophosphamide is not expected to volatilize from dry soil surfaces(SRC) based upon an estimated vapor pressure of 4.4X10-5 mm Hg(SRC), determined from a fragment constant method(5). Cyclophosphamide has been shown to be non-biodegradable using laboratory-scale sewage treatment studies(6), suggesting that biodegradation in soil may be slow(SRC).
[(1) Swann RL et al; Res Rev 85: 17-28 (1983) (2) Hansch C et al; Exploring QSAR. Hydrophobic, Electronic, and Steric Constants. ACS Prof Ref Book. Heller SR, consult. ed., Washington, DC: Amer Chem Soc p. 35 (1995) (3) Lyman WJ et al; Handbook of Chemical Property Estimation Methods. Washington, DC: Amer Chem Soc pp. 4-9 (1990) (4) Meylan WM, Howard PH; Environ Toxicol Chem 10: 1283-93 (1991) (5) Lyman WJ; p. 31 in Environmental Exposure From Chemicals Vol I, Neely WB, Blau GE, eds, Boca Raton, FL: CRC Press (1985) (6) Halling-Sorensen B et al; Chemosphere 36: 357-93 (1998)]**PEER REVIEWED**

AQUATIC FATE: Based on a classification scheme(1), an estimated Koc value of 52(SRC), determined from a log Kow of 0.63(2) and a regression-derived equation(3), indicates that cyclophosphamide is not expected to adsorb to suspended solids and sediment(SRC). Volatilization from water surfaces is not expected(3) based upon an estimated Henry's Law constant of 1.4X10-11 atm-cu m/mole(SRC), developed using a fragment constant estimation method(4). The neutral hydrolysis calculated half-life for cyclophosphamide at 25 deg C is 41 days(5). According to a classification scheme(6), an estimated BCF of 3(SRC), from its log Kow(2) and a regression-derived equation(7), suggests the potential for bioconcentration in aquatic organisms is low(SRC). Cyclophosphamide has been shown to be non-biodegradable using laboratory-scale sewage treatment studies(8).
[(1) Swann RL et al; Res Rev 85: 17-28 (1983) (2) Hansch C et al; Exploring QSAR. Hydrophobic, Electronic, and Steric Constants. ACS Prof Ref Book. Heller SR, consult. ed., Washington, DC: Amer Chem Soc p. 35 (1995) (3) Lyman WJ et al; Handbook of Chemical Property Estimation Methods. Washington, DC: Amer Chem Soc pp. 4-9, 15-1 to 15-29 (1990) (4) Meylan WM, Howard PH; Environ Toxicol Chem 10: 1283-93 (1991) (5) Ellington, JJ; Hydrolysis Rate Constants for Enhancing Property-Reactivity Relationships. Report 1989. Washington, DC: USEPA/600/3-89/063. NTIS PB89-220479 pp. 59 (1989) (6) Franke C et al; Chemosphere 29: 1501-14 (1994) (7) Meylan WM et al; Environ Toxicol Chem 18: 664-72 (1999) (8) Halling-Sorensen B et al; Chemosphere 36: 357-93 (1998)]**PEER REVIEWED**

ATMOSPHERIC FATE: According to a model of gas/particle partitioning of semivolatile organic compounds in the atmosphere(1), cyclophosphamide, which has an estimated vapor pressure of 4.4X10-5 mm Hg at 25 deg C(SRC), determined from a fragment constant method(2), will exist in both the vapor and particulate phases in the ambient atmosphere. Vapor-phase cyclophosphamide is degraded in the atmosphere by reaction with photochemically-produced hydroxyl radicals(SRC); the half-life for this reaction in air is estimated to be 5.5 hrs(SRC), calculated from its rate constant of 7.0X10-11 cu cm/molecule-sec at 25 deg C(SRC) that was derived using a structure estimation method(3). Particulate-phase cyclophosphamide may be removed from the air by wet and dry deposition(SRC). Cyclophosphamide is susceptible to light(4) and therefore the potential for direct photolysis exists(SRC).
[(1) Bidleman TF; Environ Sci Technol 22: 361-367 (1988) (2) Lyman WJ; p. 31 in Environmental Exposure From Chemicals Vol I, Neely WB, Blau GE, eds, Boca Raton, FL: CRC Press (1985) (3) Meylan WM, Howard PH; Chemosphere 26: 2293-99 (1993) (4) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Lyon, France: World Health Org, Inter Agency Res Cancer 26: 166 (1981)]**PEER REVIEWED**

 

Environmental Biodegradation:

AEROBIC: Cyclophosphamide has been shown to be non-biodegradable in a laboratory-scale sewage treatment studies(1-3). During 29 days of 10 ug/l compound addition, a mean effluent recovery of 83% was established(2). Cyclophosphamide, present at 160 mg/l, indicated no DOC elimination in four weeks using an activated sludge inoculum at 0.2 g/l and the Zahn-Wellens test(2). The compound is confirmed to be non-biodegradable according to the OECD confirmatory test using both single compound and compound mixtures run from a period of 10-14 days at concentrations ranging from 150 to 750 mg/l and that employs a sewage sludge inoculum(3).
[(1) Halling-Sorensen B et al; Chemosphere 36: 357-93 (1998) (2) Steger-Hartmann T et al; Ecotox Environ Safety 36: 174-9 (1997) (3) Kiffmeyer T et al; Fres J Anal Chem 361: 185-91 (1998)]**PEER REVIEWED**

 

Environmental Abiotic Degradation:

The rate constant for the vapor-phase reaction of cyclophosphamide with photochemically-produced hydroxyl radicals has been estimated as 7.0X10-11 cu cm/molecule-sec at 25 deg C(SRC) using a structure estimation method(1). This corresponds to an atmospheric half-life of about 5.5 hours at an atmospheric concentration of 5X10+5 hydroxyl radicals per cu cm(1). Hydrolysis occurs at temperatures above 30 deg C, with removal of chlorine atoms(2). The neutral hydrolysis rate constant for cyclophosphamide at 25 deg C has been experimentally determined to be 7.1X10-4/hour which corresponds to a calculated half-life of 41 days(3). Cyclophosphamide is reported to be sensitive to oxidation, moisture, and light(4); it darkens on exposure to light(2).
[(1) Meylan WM, Howard PH; Chemosphere 26: 2293-99 (1993) (2) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Lyon, France: World Health Org, Inter Agency Res Cancer 9: 136 (1975) (3) Ellington, JJ; Hydrolysis Rate Constants for Enhancing Property-Reactivity Relationships. Report 1989. Washington, DC: USEPA/600/3-89/063. NTIS PB89-220479 pp. 59 (1989) (4) IARC; Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Lyon, France: World Health Org, Inter Agency Res Cancer 26: 166 (1981)]**PEER REVIEWED**

 

Environmental Bioconcentration:

An estimated BCF of 3 was calculated for cyclophosphamide(SRC), using a log Kow of 0.63(1) and a regression-derived equation(2). According to a classification scheme(3), this BCF suggests the potential for bioconcentration in aquatic organisms is low(SRC).
[(1) Hansch C et al; Exploring QSAR. Hydrophobic, Electronic, and Steric Constants. ACS Prof Ref Book. Heller SR, consult. ed., Washington, DC: Amer Chem Soc p. 35 (1995) (2) Meylan WM et al; Environ Toxicol Chem 18: 664-72 (1999) (3) Franke C et al; Chemosphere 29: 1501-14 (1994)]**PEER REVIEWED**

 

Soil Adsorption/Mobility:

The Koc of cyclophosphamide is estimated as 52(SRC), using a log Kow of 0.63(1) and a regression-derived equation(2). According to a classification scheme(3), this estimated Koc value suggests that cyclophosphamide is expected to have high mobility in soil.
[(1) Hansch C et al; Exploring QSAR. Hydrophobic, Electronic, and Steric Constants. ACS Prof Ref Book. Heller SR, consult. ed., Washington, DC: Amer Chem Soc p. 35 (1995) (2) Lyman WJ et al; Handbook of Chemical Property Estimation Methods. Washington, DC: Amer Chem Soc pp. 4-9 (1990) (3) Swann RL et al; Res Rev 85: 17-28 (1983)]**PEER REVIEWED**

 

Volatilization from Water/Soil:

The Henry's Law constant for cyclophosphamide is estimated as 1.4X10-11 atm-cu m/mole(SRC) using a fragment constant estimation method(1). This Henry's Law constant indicates that cyclophosphamide is expected to be essentially nonvolatile from water surfaces(2). Cyclophosphamide is not expected to volatilize from dry soil surfaces(SRC) based upon an estimated vapor pressure of 4.5X10-5 mm Hg(SRC), determined from a fragment constant method(3).
[(1) Meylan WM, Howard PH; Environ Toxicol Chem 10: 1283-93 (1991) (2) Lyman WJ et al; Handbook of Chemical Property Estimation Methods. Washington, DC: Amer Chem Soc pp. 15-1 to 15-29 (1990) (3) Lyman WJ; p. 31 in Environmental Exposure From Chemicals Vol I, Neely WB, Blau GE, eds, Boca Raton, FL: CRC Press (1985)]**PEER REVIEWED**

Effluent Concentrations:

Cyclophosphamide concentrations of 149 ng/l(1) and 19 ng/l to 4.5 ug/l(2) were detected in hospital sewage samples from unspecified locations.
[(1) Daughton CG, Ternes TA; Environ Health Perspect 107, Suppl 6: 907-938 (1999) (2) Steger-Hartmann T et al; Ecotox Environ Safety 36: 174-9 (1997)]**PEER REVIEWED**

Atmospheric Concentrations:

SOURCE DOMINATED: Air monitoring conducted in a West German manufacturing facility in April 1984 found cyclophosphamide levels ranging from 0.1 to 810 ug/cu m(1). Air concentrations of 2-480 ug/cu m were detected in a production area of a plant involved weighing cyclophosphamide and formulating it into tablets(1).
[(1) Pyy, L et al; Am Ind Hyd Assoc J 49: 314-317 (1988)]**PEER REVIEWED**

Environmental Standards & Regulations:

CERCLA Reportable Quantities:

Persons in charge of vessels or facilities are required to notify the National Response Center (NRC) immediately, when there is a release of this designated hazardous substance, in an amount equal to or greater than its reportable quantity of 10 lb or 4.54 kg. The toll free number of the NRC is (800) 424-8802; In the Washington D.C. metropolitan area (202) 426-2675. The rule for determining when notification is required is stated in 40 CFR 302.4 (section IV. D.3.b).
[40 CFR 302.4 (7/1/2001)]**PEER REVIEWED**

RCRA Requirements:

U058; As stipulated in 40 CFR 261.33, when cyclophosphamide, as a commercial chemical product or manufacturing chemical intermediate or an off-specification commercial chemical product or a manufacturing chemical intermediate, becomes a waste, it must be managed according to Federal and/or State hazardous waste regulations. Also defined as a hazardous waste is any residue, contaminated soil, water, or other debris resulting from the cleanup of a spill, into water or on dry land, of this waste. Generators of small quantities of this waste may qualify for partial exclusion from hazardous waste regulations (40 CFR 261.5).
[40 CFR 261.33 (7/1/2001)]**PEER REVIEWED**

FDA Requirements:

Manufacturers, packers, and distributors of drug and drug products for human use are responsible for complying with the labeling, certification, and usage requirements as prescribed by the Federal Food, Drug, and Cosmetic Act, as amended (secs 201-902, 52 Stat. 1040 et seq., as amended; 21 U.S.C. 321-392).
[21 CFR 200-299, 300-499, 820, and 860 (4/1/2001)]**PEER REVIEWED**

Chemical/Physical Properties:

Molecular Formula:

C7-H15-Cl2-N2-O2-P
[The Merck Index. 10th ed. Rahway, New Jersey: Merck Co., Inc., 1983. 394]**PEER REVIEWED**

Molecular Weight:

261.10
[Budavari, S. (ed.). The Merck Index - Encyclopedia of Chemicals, Drugs and Biologicals. Rahway, NJ: Merck and Co., Inc., 1989. 429]**PEER REVIEWED**

Color/Form:

LIQUEFIES ON LOSS OF ITS WATER OF CRYSTALLIZATION
[Osol, A. (ed.). Remington's Pharmaceutical Sciences. 16th ed. Easton, Pennsylvania: Mack Publishing Co., 1980. 1087]**PEER REVIEWED**

Crystalline solid
[Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 13th ed. New York, NY: John Wiley & Sons, Inc. 1997. 327]**PEER REVIEWED**

Odor:

Odorless
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

Taste:

Slightly bitter
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

Melting Point:

49.5-53 deg C
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

Octanol/Water Partition Coefficient:

log Kow = 0.63
[Hansch, C., Leo, A., D. Hoekman. Exploring QSAR - Hydrophobic, Electronic, and Steric Constants. Washington, DC: American Chemical Society., 1995. 35]**PEER REVIEWED**

Solubilities:

1 in 25 parts water
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

1 in 1 parts alcohol
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

Slightly soluble in benzene, carbon tetrachloride; very slightly soluble in ether and acetone
[Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 12th ed. New York, NY: Van Nostrand Rheinhold Co., 1993 341]**PEER REVIEWED**

Soluble in chloroform, dioxane and glycols and insoluble in carbon tetrachloride and carbon disulfide.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 136]**PEER REVIEWED**

In water, 40,000 ppm @ 20 deg C
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 (1975) 136]**PEER REVIEWED**

Spectral Properties:

Intense mass spectral peaks: 69 m/z, 147 m/z, 175 m/z, 211 m/z, 260 m/z
[Pfleger, K., H. Maurer and A. Weber. Mass Spectral and GC Data of Drugs, Poisons and their Metabolites. Parts I and II. Mass Spectra Indexes. Weinheim, FederalRepublic of Germany. 1985. 436]**PEER REVIEWED**

Other Chemical/Physical Properties:

Fine, white, crystalline powder; odorless or almost odorless; slightly bitter taste /Monohydrate/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 166 (1981)]**PEER REVIEWED**

MP: 41-45 deg C; MW: 279.10. Solubility: 40 g/l in water; slightly sol in alcohol, benzene, ethylene glycol, dioxane, carbon tetrachloride; sparingly sol in ether and acetone /Monohydrate/
[Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals. Whitehouse Station, NJ: Merck and Co., Inc., 2001. 479]**PEER REVIEWED**

Darkens on exposure to light. Hydrolysis occurs at temperatures above 30 deg C, with removal of chlorine atoms.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 (1975) 136]**PEER REVIEWED**

Sensitive to oxidation, moisture, and light.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

Chemical Safety & Handling:

Hazards Summary:

The major hazards encountered in the use and handling of cyclophosphamide stem from its toxicologic properties. Exposure to this odorless, white, crystalline powder may occur from its manufacture, formulation, or distribution for use as an antineoplastic drug. Effects from exposure may include fever, chills, shortness of breath, dizziness, fatigue, headache, nausea, hemorrhagic colitis, hepatitis, leukopenia, and pneumonitis or interstitial pulmonary fibrosis. Cyclophosphamide has been indicated as a human carcinogen (Group 1) by the International Agency for Research on Cancer (IARC). Exposure should be controlled by mechanical ventilation with high-efficiency particulate arrestors (HEPA) or charcoal filters to minimize the amount of the substance in exhausted air. In activities or situations where over-exposure may occur, wear protective clothing and a carefully fitted respirator. Potentially exposed skin should be thoroughly washed with soap and water. Contaminated clothing should be removed and discarded or left at the work site for cleaning before reuse. Smoking, eating, and drinking should be prohibited in cyclophosphamide work areas. Cyclophosphamide should be stored and transported in securely sealed glass bottles or ampoules, which are in turn placed inside strong screw-cap or snap-top containers. Also, the material should be stored cool (below 30 deg C), dry, and shielded from light. This substance is a good candidate for disposal by rotary kiln, or fluidized bed forms of incineration.
**PEER REVIEWED**

Skin, Eye and Respiratory Irritations:

A powerful skin irritant.
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 973]**PEER REVIEWED**

Hazardous Reactivities & Incompatibilities:

/It was/ reported that immersion of a needle with an aluminum component in cyclophosphamide 20 mg/ml resulted in a slight darkening of the aluminum & gas production after a few days at 24 deg C with protection from light.
[Trissel, L.A. Handbook on Injectable Drugs. 9th ed. Bethesda, MD. American Society of Health-System Pharmacists' Product Development. 1996. 306]**PEER REVIEWED**

Hazardous Decomposition:

When heated to decomposition it emits highly toxic fumes of /phosphorus oxides, nitrogen oxides, & hydrogen chloride/.
[Lewis, R.J. Sax's Dangerous Properties of Industrial Materials. 9th ed. Volumes 1-3. New York, NY: Van Nostrand Reinhold, 1996. 973]**PEER REVIEWED**

The rate constant for decomp of cyclophosphamide when constituted with benzyl alcohol-preserved bacteriostatic water for injection is significantly higher than with sterile water for injection. It was suggested that benzyl alcohol may catalyze somewhat the decomp of cyclophosphamide the rate of decomp is independent of pH over the range of 2-10.
[Trissel, L.A. Handbook on Injectable Drugs. 9th ed. Bethesda, MD. American Society of Health-System Pharmacists' Product Development. 1996. 300]**PEER REVIEWED**

Protective Equipment & Clothing:

PRECAUTIONS FOR "CARCINOGENS": ... Dispensers of liq detergent /should be available./ ... Safety pipettes should be used for all pipetting. ... In animal laboratory, personnel should ... wear protective suits (preferably disposable, one piece & close fitting at ankles & wrists), gloves, hair covering & overshoes. ... In chemical laboratory, gloves & gowns should always be worn ... however, gloves should not be assumed to provide full protection. Carefully fitted masks or respirators may be necessary when working with particulates or gases, & disposable plastic aprons might provide addnl protection. ... gowns ... /should be/ of distinctive color, this is a reminder that they are not to be worn outside the laboratory. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 8]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Protective apparel: Disposable closed-front gown or coveralls, disposable utility gloves over disposable latex gloves, NIOSH-approved air-purifying half-mask respirator equipped with a high efficiency filter, and eye protection should be worn. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Class 100 clean-air work stations, both horizontal and vertical airflow (with no containment characteristics), are inappropriate engineering controls for handling hazardous drugs because they provide no personnel protection and permit environmental contamination. Although there are no engineering controls designed specifically for the safe handling of hazardous chemicals as sterile products, Class II contained vertical-flow biological safety cabinets (biohazard cabinets) have been adopted for this use. Biohazard cabinetry is, however, designed for the handling of infectious agents, not hazardous chemicals. ... Based on design, ease of use, and cost considerations, Class II contained-vertical-flow biohazard cabinetry is currently recommended for use in preparing sterile doses of hazardous drugs. Class II cabinetry design and performance specifications are defined in NSF Standard 49. Biological safety cabinets selected for use with hazardous drugs should meet NSF Standard 49 specifications to ensure the maximum protection from these engineering controls. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Workers should wear powder free, disposable surgical latex gloves of good quality when preparing hazardous drugs. Selection criteria for gloves should include thickness (especially at the fingertips where stress is the greatest), fit, length, and tactile sensation. ... The practice of double gloving is supported by research that indicates that many glove materials vary in drug permeability even within lots; therefore, double gloving is recommended. ... In general, surgical latex gloves fit better, have appropriate elasticity for double gloving and maintaining the integrity of the glove-gown interface, and have sufficient tactile sensation (even during double gloving) for stringent aseptic procedures. ... Powdered gloves should be avoided. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Workers who are not protected by the containment environment of a biohazard cabinet should use respiratory protection when handling hazardous drugs. Respiratory protection should be an adjunct to and not a substitute for engineering controls. Surgical masks of all types provide no respiratory protection against powdered or liquid aerosols of hazardous drugs. In situations where workers may be exposed to potential eye contact with hazardous drugs, an appropriate plastic face shield or splash goggles should be worn. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ During compounding of hazardous drugs (eg, crushing, dissolving, and preparing an ointment), workers should wear low permeability gowns and double gloves. Compounding should take place in a protective area such as a disposable glove box. If compounding must be done in the open, an area away from drafts and traffic must be selected, and the worker should use appropriate respiratory protection. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 757]**PEER REVIEWED**

Preventive Measures:

PRECAUTIONS FOR "CARCINOGENS": Smoking, drinking, eating, storage of food or of food & beverage containers or utensils, & the application of cosmetics should be prohibited in any laboratory. All personnel should remove gloves, if worn, after completion of procedures in which carcinogens have been used. They should ... wash ... hands, preferably using dispensers of liq detergent, & rinse ... thoroughly. Consideration should be given to appropriate methods for cleaning the skin, depending on nature of the contaminant. No standard procedure can be recommended, but the use of organic solvents should be avoided. Safety pipettes should be used for all pipetting. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 8]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": In animal laboratory, personnel should remove their outdoor clothes & wear protective suits (preferably disposable, one piece & close fitting at ankles & wrists), gloves, hair covering & overshoes. ... clothing should be changed daily but ... discarded immediately if obvious contamination occurs ... /also,/ workers should shower immediately. In chemical laboratory, gloves & gowns should always be worn ... however, gloves should not be assumed to provide full protection. Carefully fitted masks or respirators may be necessary when working with particulates or gases, & disposable plastic aprons might provide addnl protection. If gowns are of distinctive color, this is a reminder that they should not be worn outside of lab. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 8]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": ... Operations connected with synth & purification ... should be carried out under well ventilated hood. Analytical procedures ... should be carried out with care & vapors evolved during ... procedures should be removed. ... Expert advice should be obtained before existing fume cupboards are used ... & when new fume cupboards are installed. It is desirable that there be means for decreasing the rate of air extraction, so that carcinogenic powders can be handled without ... powder being blown around the hood. Glove boxes should be kept under negative air pressure. Air changes should be adequate, so that concn of vapors of volatile carcinogens will not occur. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 8]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": Vertical laminar flow biological safety cabinets may be used for containment of in vitro procedures ... provided that the exhaust air flow is sufficient to provide an inward air flow at the face opening of the cabinet, & contaminated air plenums that are under positive pressure are leak tight. Horizontal laminar flow hoods or safety cabinets, where filtered air is blown across the working area towards the operator, should never be used ... Each cabinet or fume cupboard to be used ... should be tested before work is begun (eg, with fume bomb) & label fixed to it, giving date of test & avg air flow measured. This test should be repeated periodically & after any structural changes. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 9]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": Principles that apply to chem or biochem lab also apply to microbiological & cell culture labs ... Special consideration should be given to route of admin. ... Safest method of administering volatile carcinogen is by injection of a soln. Admin by topical application, gavage, or intratracheal instillation should be performed under hood. If chem will be exhaled, animals should be kept under hood during this period. Inhalation exposure requires special equipment. ... unless specifically required, routes of admin other than in the diet should be used. Mixing of carcinogen in diet should be carried out in sealed mixers under fume hood, from which the exhaust is fitted with an efficient particulate filter. Techniques for cleaning mixer & hood should be devised before expt begun. When mixing diets, special protective clothing &, possibly, respirators may be required. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 9]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": When ... admin in diet or applied to skin, animals should be kept in cages with solid bottoms & sides & fitted with a filter top. When volatile carcinogens are given, filter tops should not be used. Cages which have been used to house animals that received carcinogens should be decontaminated. Cage cleaning facilities should be installed in area in which carcinogens are being used, to avoid moving of ... contaminated /cages/. It is difficult to ensure that cages are decontaminated, & monitoring methods are necessary. Situations may exist in which the use of disposable cages should be recommended, depending on type & amt of carcinogen & efficiency with which it can be removed. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 10]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": To eliminate risk that ... contamination in lab could build up during conduct of expt, periodic checks should be carried out on lab atmospheres, surfaces, such as walls, floors & benches, & ... interior of fume hoods & airducts. As well as regular monitoring, check must be carried out after cleaning up of spillage. Sensitive methods are required when testing lab atmospheres. ... Methods ... should ... where possible, be simple & sensitive. ... /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 10]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": Rooms in which obvious contamination has occurred, such as spillage, should be decontaminated by lab personnel engaged in expt. Design of expt should ... avoid contamination of permanent equipment. ... Procedures should ensure that maintenance workers are not exposed to carcinogens. ... Particular care should be taken to avoid contamination of drains or ventilation ducts. In cleaning labs, procedures should be used which do not produce aerosols or dispersal of dust, ie, wet mop or vacuum cleaner equipped with high efficiency particulate filter on exhaust, which are avail commercially, should be used. Sweeping, brushing & use of dry dusters or mops should be prohibited. Grossly contaminated cleaning materials should not be reused ... If gowns or towels are contaminated, they should not be sent to laundry, but ... decontaminated or burnt, to avoid any hazard to laundry personnel. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 10]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": Doors leading into areas where carcinogens are used ... should be marked distinctively with appropriate labels. Access ... limited to persons involved in expt. ... A prominently displayed notice should give the name of the Scientific Investigator or other person who can advise in an emergency & who can inform others (such as firemen) on the handling of carcinogenic substances. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 11]**PEER REVIEWED**

SRP: Contaminated protective clothing should be segregated in such a manner so that there is no direct personal contact by personnel who handle, dispose, or clean the clothing. Quality assurance to ascertain the completeness of the cleaning procedures should be implemented before the decontaminated protective clothing is returned for reuse by the workers. Contaminated clothing should not be taken home at end of shift, but should remain at employee's place of work for cleaning.
**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Accidental contamination of the health-care environment, resulting in exposure of personnel, patients, visitors, and family members to hazardous substances, is prevented by maintaining the physical integrity and security of packages of hazardous drugs. 1. Access to all areas where hazardous drugs are stored is limited to specified authorized staff. 2. A method should be present for identifying to personnel those drugs that require special precautions (eg, cytotoxics). One way to accomplish this is to apply appropriate warning labels to all hazardous drug containers, shelves, and bins where the drug products are stored. ... 3. A method of identifying, for patients and family members, those drugs that require special precautions in the home should be in place. This may be accomplished in the health-care setting, by providing specific labeling for discharge medications, along with written instructions. 4. Methods for identifying shipping cartons of hazardous drugs should be required from manufacturers and distributors of these drugs. 5. Written procedures for handling damaged packages of hazardous drugs should be maintained. Personnel involved in shipping and receiving hazardous drugs should be trained in these procedures, including the proper use of protective garments and equipment. Damaged shipping cartons of hazardous drugs should be received and opened in an isolated area (eg, in a laboratory fume hood, if available, not in a vertical laminar airflow biological safety cabinet used for preparing sterile products). /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 753]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Facilities (eg, shelves, carts, counters, and trays) for storing hazardous drugs are designed to prevent breakage and to limit contamination in the event of leakage. Bins, shelves with barriers at the front, or other design features that reduce the chance of drug containers falling to the floor should be used. Hazardous drugs requiring refrigeration should be stored separately from nonhazardous drugs in individual bins designed to prevent breakage and to contain leakage. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Until the reproductive risks (or lack thereof) associated with handling hazardous drugs within a safety program have been substantiated, staff who are pregnant or breast-feeding should be allowed to avoid contact with these drugs. Policies should be in effect that provide these individuals with alternative tasks or responsibilities if they so desire. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The pharmacy should provide access to information on toxicity, treatment of acute exposure (if available), chemical inactivators, solubility and stability of hazardous drugs (including investigational agents) used in the workplace. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Appropriate engineering controls should be in place to protect the drug product from microbial contamination and to protect personnel and the environment from the potential hazards of the product. These engineering controls should be maintained according to applicable regulations and standards. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Biological safety cabinets should be cleaned and disinfected regularly to ensure a proper environment for preparation of sterile products. For routine cleanups of surfaces between decontaminations, water should be used (for injection or irrigation) with or without a small amount of cleaner. If the contamination is soluble only in alcohol, then 70% isopropyl or ethyl alcohol may be used in addition to the cleaner. In general, alcohol is not a good cleaner, only a disinfectant, and its use in a biohazard cabinet should be limited. The biohazard cabinet should be disinfected with 70% alcohol before any aseptic manipulation is begun. The excessive use of alcohol should be avoided in biohazard cabinets where air is recirculated ... because alcohol vapors may build up in the cabinet. A lint-free, plastic-backed disposable liner may be used in the biological safety cabinet to facilitate spill cleanup. ... If used, the liner should be changed frequently ... /or/ whenever it is overtly contaminated. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 755]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The biological safety cabinets should be decontaminated on a regular basis (ideally at least weekly) and whenever there is a spill or the biological safety cabinet is moved or serviced, including for certification. ... Currently, no single reagent will deactivate all known hazardous drugs; therefore, decontamination of a biological safety cabinet used for such drugs is limited to removal of contamination from a nondisposable surface (the cabinet) to a disposable surface (eg, gauze or towels) by use of a good cleaning agent that removes chemicals from stainless steel. The cleaning agent selected should have a pH approximating that of soap and be appropriate for stainless steel. Cleaners containing chemicals such as quaternary ammonium compounds should be used with caution, because they may be hazardous to humans and their vapors may build up in any biological safety cabinet where air is recirculated. Similar caution should be used with any pressurized aerosol cleaner; spraying a pressurized aerosol into a biological safety cabinet may disrupt the protective containment airflow, damage the high efficiency particulate air filter, and cause an accumulation of the propellant within a biological safety cabinet where air is recirculated, resulting in a fire and explosion hazard. During decontamination, the operator should wear a disposable closed front gown, disposable latex gloves covered by disposable utility gloves, safety glasses or goggles, a hair covering, and a disposable respirator, because the glass shield of the biological safety cabinet occasionally must be lifted. The blower must be left on, and only heavy toweling or gauze should be used in the biological safety cabinet to prevent it from being "sucked" up the plenum and into the high efficiency particulate air filter. Decontamination should be done from top to bottom (areas of lesser contamination to greater) by applying the cleaner, scrubbing, and rinsing thoroughly with distilled or deionized water. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 755]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The high efficiency particulate air filters /or other exhaust scrubbing system/ of the biohazard cabinet must be replaced whenever they restrict required airflow velocity or if they are overtly contaminated (eg, by a breach in technique that causes hazardous drug to be introduced onto the clean side of the supply high efficiency particulate air filter). Personnel and environmental protection must be maintained during replacement of a contaminated high efficiency particulate air filter. Because replacement of a high efficiency particulate air filter generally requires breaking the integrity of the containment aspect of the cabinet, this procedure may release contamination from the filter into the pharmacy or intravenous preparation area if carried out in an inappropriate manner. Before replacement of a high efficiency particulate air filter contaminated with hazardous drugs, the biological safety cabinet service agent should be consulted for a mutually acceptable procedure for replacing and subsequently disposing of a contaminated high efficiency particulate air filter. One procedure would include moving the biological safety cabinet to a secluded area or using plastic barriers to segregate the contaminated area. Protective clothing and equipment must be used by the servicer. The biological safety cabinet should be decontaminated before filter replacement. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ During removal of gloves, ... avoid touching the inside of the glove or the skin with the contaminated glove fingers. ... The worker should wear a protective disposable gown made of lint free, low-permeability fabric with a solid front, long sleeves, and tight-fitting elastic or knit cuffs when preparing hazardous drugs. Washable garments are immediately penetrated by liquids and therefore provide little, if any protection. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ When double gloving, one glove should be placed under the gown cuff and one over. The glove-gown interface should be such that no skin on the arm or wrist is exposed. Gloves and gowns should not be worn outside the immediate preparation area. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Eyewash fountains should be available in areas where hazardous drugs are routinely handled. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Although noninjectable dosage forms of hazardous drugs contain varying proportions of drug to nondrug (nonhazardous) components, there is potential for personnel exposure and environmental contamination with the hazardous components. Procedures should be developed to avoid the release of aerosolized powder or liquid into the environment during manipulation of these drugs. Drugs designated as hazardous should be labeled or otherwise identified as such to prevent their improper handling. Tablet and capsule forms of these drugs should not be placed in automated counting machines, which subject them to stress and may introduce powdered contaminants into the work area. During routine handling of hazardous drugs and contaminated equipment, workers should wear one pair of gloves of good quality and thickness. The counting and pouring of hazardous drugs should be done carefully, and clean equipment dedicated for use with these drugs should be used. ... When hazardous drug tablets in unit-of-use packaging are being crushed, the package should be placed in a small sealable plastic bag and crushed with a spoon or pestle; caution should be used not to break the plastic bag. Disposal of unused or unusable oral or topical dosage forms of hazardous drugs should be performed in the same manner as for hazardous injectable dosage forms and waste. ... Hazardous drug work areas should have a sink (preferably with an eyewash fountain) and appropriate first aid equipment to treat accidental skin or eye contact according to the protocol. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 757]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ A distinctive warning label with an appropriate CAUTION statement should be attached to all hazardous drug materials, consistent with state laws and regulations. This would include, for example, syringes, IV containers, containers of unit-dose tablets and liquids, prescription vials and bottles, waste containers, and patient specimens that contain hazardous drugs. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 757]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Supplies of disposable gloves and gowns, safety glasses, disposable plastic-backed absorbent liners, gauze pads, hazardous waste disposal bags, hazardous drug warning labels, and puncture-resistant containers for disposal of needles and ampuls should be conveniently located for all areas where hazardous drugs are handled. Assembling a "hazardous drug preparation and administration kit" is one way to furnish nursing and medical personnel with the materials needed to reduce the risk of preparing and administering a hazardous drug. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 758]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Prospective temporary and permanent employees who may be required to work with hazardous drugs should be so notified and should receive adequate information about the policies and procedures pertaining to their use. This notification should be documented during the interview process and retained as part of the employment record for all employees. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ All personnel involved with the transportation, preparation, administration, and disposal of cytotoxic and hazardous substances should continually be updated on new or revised information on safe handling of cytotoxic and hazardous substances. Policies and procedures should be updated accordingly. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 754]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The work area should be designed to provide easy access to those items necessary to prepare, label, and transport final products; contain all related waste; and avoid inadvertent contamination of the work area. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Each health-care setting should have an established first aid protocol for treating cases of direct contact with hazardous drugs, many of which are irritating or caustic and can cause tissue destruction. Medical care providers in each setting should be contacted for input into this protocol. The protocol should include immediate treatment measures and should specify the type and location of medical follow-up and work-injury reporting. Copies of the protocol, highlighting emergency measures, should be posted wherever hazardous drugs are routinely handled. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 757]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Only individuals trained to administer hazardous drugs should be allowed to perform this function. Training programs should contain information on the therapeutic and adverse effects of these drugs and the potential, long term health risk to personnel handling these drugs. Each individual's knowledge and technique should be evaluated before administration of these drugs. This should be done by written examination and direct observation of the individual's performance. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 757]**PEER REVIEWED**

Stability/Shelf Life:

AQ SOLN KEEPS FOR A FEW HR @ ROOM TEMP, BUT HYDROLYSIS OCCURS ABOVE 30 DEG C, REMOVES CHLORINE ATOMS; DARKENS ON EXPOSURE TO LIGHT /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 136 (1975)]**PEER REVIEWED**

SENSITIVE TO OXIDATION, MOISTURE ... /MONOHYDRATE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 166 (1981)]**PEER REVIEWED**

Constitute solns should be used within 24 hr if stored at room temp or within 6 days if stored under refrigeration. When constituted with sterile water for injection or paraben-preserved bacteriostatic water for injection to a concn of 21 mg/ml, <1.5% cyclophosphamide decomposition will occur within 8 hr at 24-27 deg C & within 6 days at 5 deg C.
[Trissel, L.A. Handbook on Injectable Drugs. 9th ed. Bethesda, MD. American Society of Health-System Pharmacists' Product Development. 1996. 300]**PEER REVIEWED**

Shipment Methods and Regulations:

PRECAUTIONS FOR "CARCINOGENS": Procurement ... of unduly large amt ... should be avoided. To avoid spilling, carcinogens should be transported in securely sealed glass bottles or ampoules, which should themselves be placed inside strong screw-cap or snap-top container that will not open when dropped & will resist attack from the carcinogen. Both bottle & the outside container should be appropriately labelled. ... National post offices, railway companies, road haulage companies & airlines have regulations governing transport of hazardous materials. These authorities should be consulted before ... material is shipped. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 13]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": When no regulations exist, the following procedure must be adopted. The carcinogen should be enclosed in a securely sealed, watertight container (primary container), which should be enclosed in a second, unbreakable, leakproof container that will withstand chem attack from the carcinogen (secondary container). The space between primary & secondary container should be filled with absorbent material, which would withstand chem attack from the carcinogen & is sufficient to absorb the entire contents of the primary container in the event of breakage or leakage. Each secondary container should then be enclosed in a strong outer box. The space between the secondary container & the outer box should be filled with an appropriate quantity of shock-absorbent material. Sender should use fastest & most secure form of transport & notify recipient of its departure. If parcel is not received when expected, carrier should be informed so that immediate effort can be made to find it. Traffic schedules should be consulted to avoid ... arrival on weekend or holiday ... /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 13]**PEER REVIEWED**

Storage Conditions:

Cyclophosphamide should be preserved in tight containers, at a temperature between 2 & 32 deg C.
[American Medical Association, Department of Drugs. Drug Evaluations. 6th ed. Chicago, Ill: American Medical Association, 1986. 263]**PEER REVIEWED**

Protect from light.
[Reynolds, J.E.F., Prasad, A.B. (eds.) Martindale-The Extra Pharmacopoeia. 28th ed. London: The Pharmaceutical Press, 1982. 199]**PEER REVIEWED**

PRECAUTIONS FOR "CARCINOGENS": Storage site should be as close as practicable to lab in which carcinogens are to be used, so that only small quantities required for ... expt need to be carried. Carcinogens should be kept in only one section of cupboard, an explosion proof refrigerator or freezer (depending on chemicophysical properties ...) that bears appropriate label. An inventory ... should be kept, showing quantity of carcinogen & date it was acquired ... Facilities for dispensing ... should be contiguous to storage area. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 13]**PEER REVIEWED**

Cleanup Methods:

PRECAUTIONS FOR "CARCINOGENS": A high efficiency particulate arrestor (HEPA) or charcoal filters can be used to minimize amt of carcinogen in exhausted air ventilated safety cabinets, lab hoods, glove boxes or animal rooms ... Filter housing that is designed so that used filters can be transferred into plastic bag without contaminating maintenance staff is available commercially. Filters should be placed in plastic bags immediately after removal ... The plastic bag should be sealed immediately ... The sealed bag should be labelled properly ... Waste liquids ... should be placed or collected in proper containers for disposal. The lid should be secured & the bottles properly labelled. Once filled, bottles should be placed in plastic bag, so that outer surface ... is not contaminated ... The plastic bag should also be sealed & labelled. ... Broken glassware ... should be decontaminated by solvent extraction, by chemical destruction, or in specially designed incinerators. /Chemical Carcinogens/
[Montesano, R., H. Bartsch, E.Boyland, G. Della Porta, L. Fishbein, R. A. Griesemer, A.B. Swan, L. Tomatis, and W. Davis (eds.). Handling Chemical Carcinogens in the Laboratory:Problems of Safety. IARC Scientific Publications No. 33. Lyon, France: International Agency for Research on Cancer, 1979. 15]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Spill kits containing all materials needed to clean up spills of hazardous drugs should be assembled or purchased. These kits should be readily available in all areas where hazardous drugs are routinely handled. If hazardous drugs are being prepared or administered in a nonroutine area (home setting or unusual patient-care area), a spill kit should be obtained by the drug handler. The kit should include two pairs of disposable gloves (one outer pair of utility gloves and one inner latex pair); low-permeability, disposable protective garments (coveralls or gown and shoe covers); safety glasses or splash goggles; respirator; absorbent, plastic-backed sheets or spill pads; disposable toweling; at least 2 sealable thick plastic hazardous waste disposal bags (prelabeled with an appropriate warning label); a disposable scoop for collecting glass fragments; and a puncture-resistant container for glass fragments. All individuals who routinely handle hazardous drugs must be trained in proper spill management and cleanup procedures. Spills and breakages must be cleaned up immediately according to the following procedures. If the spill is not located in a confined space, the spill area should be identified and other people should be prevented from approaching and spreading the contamination. Wearing protective apparel from the spill kit, workers should remove any broken glass fragments and place them in the puncture-resistant container. Liquids should be absorbed with a spill pad; powder should be removed with damp disposable gauze pads or soft toweling. The hazardous material should be completely removed and the area rinsed with water and then cleaned with detergent. The spill cleanup should proceed progressively from areas of lesser to greater contamination. The detergent should be thoroughly rinsed and removed. All contaminated materials should be placed in the disposal bags provided and sealed and transported to a designated containment receptacle. Spills occurring in the biohazard cabinet should be cleaned up immediately; a spill kit should be used if the volume exceeds 150 ml or the contents of one drug vial or ampule. If there is broken glass, utility gloves should be worn to remove it and place it in the puncture-resistant container located in the biohazard cabinet. The biological safety cabinet, including the drain spillage trough, should be thoroughly cleaned. If the spill is not easily and thoroughly contained, the biological safety cabinet should be decontaminated after cleanup. If the spill contaminates the high efficiency particulate air filter, use of the biological safety cabinet should be suspended until the cabinet has been decontaminated and the high efficiency particulate air filter replaced. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 758]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ If hazardous drugs are routinely prepared or administered in carpeted areas, special equipment is necessary to remove the spill. Absorbent powder should be substituted for pads or sheets and left in place on the spill for the time recommended by the manufacturer. The powder should then be picked up with a small vacuum unit reserved for hazardous drug cleanup. The carpet should then be cleaned according to usual procedures. The vacuum bag should be removed and discarded or cleaned, and the exterior of the vacuum cleaner should be washed with detergent and rinsed before being covered and stored. The contaminated powder should be discarded into a sealable plastic bag and segregated with other contaminated waste materials. Alternatively, inexpensive wet or dry vacuum units may be purchased for this express use and used with appropriate cleaners. All such units are contaminated, once used, and must be cleaned, stored, and ultimately discarded /properly/ ... The circumstances and handling of spills should be documented. Health-care personnel exposed during spill management should also complete an incident report or exposure form. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 759]**PEER REVIEWED**

Disposal Methods:

Generators of waste (equal to or greater than 100 kg/mo) containing this contaminant, EPA hazardous waste number U058, must conform with USEPA regulations in storage, transportation, treatment and disposal of waste.
[40 CFR 240-280, 300-306, 702-799 (7/1/92)]**PEER REVIEWED**

A potential candidate for rotary kiln incineration at a temperature range of 820 to 1,600 deg C and residence times of seconds for liquids and gases, and hours for solids. A potential candidate for fluidized bed incineration at a temperature range of 450 to 980 deg C and residence times of seconds for liquids and gases, and longer for solids.
[USEPA; Engineering Handbook for Hazardous Waste Incineration p.3-12 (1981) EPA 68-03-3025]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ All contaminated disposables should be contained in sealable bags for transfer to larger waste containers. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 755]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ All bottles must be discarded as contaminated waste after decontamination of the biohazard cabinet. All protective apparel (gown, gloves, goggles, and respirator) should be discarded as contaminated waste. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The contaminated filters must be removed, bagged in thick plastic and prepared for disposal in a hazardous waste dump site or incinerator licensed by the Environmental Protection Agency (EPA). /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ The gown should be removed and placed in a sealable container before removal of the inner gloves. The inner gloves should be removed last and placed in the container with the gown. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 756]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Hazardous drug waste should be placed in specially marked (specifically labeled CAUTION: HAZARDOUS CHEMICAL WASTE) thick plastic bags or leakproof containers. These receptacles should be kept in all areas where the drugs are commonly used. All and only hazardous drug waste should be placed in them. Receptacles used for glass fragments, needles, and syringes should be puncture resistant. Hazardous drug waste should not be mixed with any other waste. Waste containers should be handled with uncontaminated gloves. ... Gloves, gowns, drug vials, etc, should be sealed in specially labeled (CAUTION: HAZARDOUS CHEMICAL WASTE) thick plastic bags or leakproof containers. ... All hazardous waste collected from drug preparation and patient-care areas should be held in a secure place in labeled, leakproof drums or cartons (as required by state or local regulation or disposal contractor) until disposal. This waste should be disposed of as hazardous or toxic waste in an EPA-permitted state-licensed hazardous waste incinerator. Transport to an offsite incinerator should be done by a contractor licensed to handle and transport hazardous waste. ... If access to an appropriately licensed incinerator is not available, transport to and burial in an EPA-licensed hazardous waste dump site is an acceptable alternative. While there are concerns that destruction of carcinogens by incineration may be incomplete, newer technologies and stringent licensing criteria have improved this disposal method. ... Chemical deactivation of hazardous drugs should be undertaken only by individuals who are thoroughly familiar with the chemicals and the procedures required to complete such a task. The IARC recently published a monograph describing methods for chemical destruction of some cytotoxic (antineoplastic) drugs in the laboratory setting. The chemicals and equipment described, however, are not generally found in the clinical setting, and many of the deactivating chemicals are toxic and hazardous. Most procedures require the use of a chemical fume hood. The procedures are generally difficult, and the deactivation is not always complete. Serious consideration should be given to the negative aspects of chemical deactivation before one commits to such a course of action. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 758]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ Regulatory agencies such as the EPA and state solid and hazardous waste agencies and local air and water quality control boards must be consulted regarding the classification and appropriate disposal of drugs that are defined as hazardous or toxic chemicals. EPA categorizes several of the antineoplastic agents as toxic wastes, while many states are more stringent and include as carcinogens certain cytotoxic drugs and hormonal preparations. EPA also allows exemptions from toxic waste regulations for small quantity generators, whereas certain states do not. It is critical to research these regulations when disposal procedures are being established. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 759]**PEER REVIEWED**

/PRECAUTIONS FOR ANTINEOPLASTIC AGENTS:/ If the biological safety cabinets is equipped with a drainpipe and valve, it may be used to collect rinse water. The collection vessel used must fit well around the drain valve and not allow splashing. Gauze may be used around the connection to prevent aerosol from escaping. The collection vessel must have a tight fitting cover, and all rinse water (gauze, if used) must be disposed of as contaminated waste. /Antineoplastic agents/
[McEvoy, G.K. (ed.). American Hospital Formulary Service - Drug Information 95. Bethesda, MD: American Society of Hospital Pharmacists, Inc., 1995 (Plus Supplements 1995). 755]**PEER REVIEWED**

Occupational Exposure Standards:

Manufacturing/Use Information:

Major Uses:

Therap Cat: Antineoplastic
[Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals. Whitehouse Station, NJ: Merck and Co., Inc., 2001. 479]**PEER REVIEWED**

Immunosupressive
[SRI International. 2000 Directory of Chemical Producers -- United States. SRI Consulting, Menlo Park: CA 2000 35]**PEER REVIEWED**

Antineoplastic for treatment of leukemia, etc; tested for use in chemical shearing of sheep and as an insect chemosterilant.
[Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 13th ed. New York, NY: John Wiley & Sons, Inc. 1997. 327]**PEER REVIEWED**

MEDICATION
**PEER REVIEWED**

MEDICATION (VET)
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Methods of Manufacturing:

Cyclophosphamide can be prepared by treating N,N-bis(B-chloroethyl)-phosphamide dichloride with propanolamine in the presence of trimethylamine and dioxane.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 167]**PEER REVIEWED**

Prepn: H. Arnold et al., Naturwiss 45, 64 (1957); eidem, Nature 181, 931 (1958); H. Arnold, F. Bourseaux, Angew Chem. 70, 539 (1958).
[Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals. Whitehouse Station, NJ: Merck and Co., Inc., 2001. 479]**PEER REVIEWED**

Formulations/Preparations:

CYCLOPHOSPHAMIDE IS SUPPLIED AS 25 & 50 MG TABLETS & AS A POWDER (100 TO 2000 MG) IN STERILE VIALS.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1217]**PEER REVIEWED**

Grade: USP, measured as containing 95.0 - 105.0% active ingredient calculated as the monohydrate, 5.7 - 6.8% max. water content, 0.002% max. heavy metals, and producing an aqueous solution (1 in 100) at pH 3.9 - 7.1.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

Available as 25 and 50 mg tablets ... and in vials for injection in amounts of 100, 200 or 500 mg measured as containing 90.0 - 110.0% of the stated amount of anhydrous cyclophosphamide.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

Consumption Patterns:

Total US sales are 600 kg/year (1975)
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 137]**PEER REVIEWED**

U. S. Production:

Not produced in the US.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

U. S. Imports:

No data were available on the quantities imported.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

Laboratory Methods:

Clinical Laboratory Methods:

SAMPLE MATRIX: BLOOD AND URINE. ASSAY PROCEDURE: GAS CHROMATOGRAPHY WITH NITROGEN PHOSPHORUS DETECTION; WHITING B ET AL, BR J CLIN PHARMACOL 6: 373 (1978). THIN-LAYER CHROMATOGRAPHY WITH SCINTILLATION SPECTROMETRY; WAGNER T ET AL; CANCER RES 37: 2592 (1977).
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 168 (1981)]**PEER REVIEWED**

Analytic Laboratory Methods:

SAMPLE MATRIX: IN FORMULATIONS. ASSAY PROCEDURES: HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY WITH ULTRA-VIOLET DETECTION; KENSLER TT ET AL; J PHARM SCI 68: 172 (1979). GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION; US PHARMACOPEIAL CONVENTION, INC. THE US PHARMACOPEIA, 15TH ED, ROCKVILLE, MD, PAGES 189-190. /FROM TABLE/
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 168 (1981)]**PEER REVIEWED**

Method 3640A Gel Permeation Chromatography (GPC) Cleanup Procedure. Gel permeation chromatography with high performance liquid chromatography. No detection limit reported.
[USEPA/Office of Solid Waste (OSW); Test Methods for Evaluating Solid Waste, Physical/Chemical Methods SW846 Methods (1986)]**PEER REVIEWED**

Estimation of nitrogen, phosphorus, or chloride content; colorimetric analysis, based on the intensity of a cobalt thiocyanate-cyclophosphamide complex or by use of 4-(4'-nitrobenzyl)pyridine after hydrolysis; titrimetric analysis, after precipitation of the digested material by quinoline and citric-molybdic acid solution; and infrared spectrometry (the method with the most specificity). Also gas-liquid chromatography and mass spectrometry.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V9 138]**PEER REVIEWED**

Special References:

Special Reports:

U.S. Department of Health & Human Services/National Toxicology Program; 9th Report on Carcinogens. National Institute of Environmental Health Sciences, Research Triangle Park, NC. (2000)

Anderson D et al; Mutat Res 330 (1-2): 115-81 (1995). Cyclophosphamide: Review of its Mutagenicity for an Assessment of Potential Germ Cell Risks.

Synonyms and Identifiers:

Related HSDB Records:

177 [ACROLEIN] (Metabolite)

Synonyms:

B 518
**PEER REVIEWED**

ASTA B 518
**PEER REVIEWED**

1-BIS(2-CHLOROETHYL)AMINO-1-OXO-2-AZA-5-OXAPHOSPHORIDIN
**PEER REVIEWED**

2-(BIS(2-CHLOROETHYL)AMINO)TETRAHYDRO-2H-1,3,2-OXAZOPHOSPHORINE 2-OXIDE
**PEER REVIEWED**

BIS(2-CHLOROETHYL)PHOSPHAMIDE CYCLIC PROPANOLAMIDE ESTER
**PEER REVIEWED**

BIS(2-CHLOROETHYL)PHOSPHORAMIDE CYCLIC PROPANOLAMIDE ESTER
**PEER REVIEWED**

N,N-BIS(BETA-CHLOROETHYL)-N',O-PROPYLENEPHOSPHORIC ACID ESTER DIAMIDE
**PEER REVIEWED**

N,N-BIS(2-CHLOROETHYL)-N',O-PROPYLENEPHOSPHORIC ACID ESTER DIAMIDE
**PEER REVIEWED**

N,N-BIS(2-CHLOROETHYL)TETRAHYDRO-2H-1,3,2-OXAZAPHOSPHORIN-2-AMINE 2-OXIDE
**PEER REVIEWED**

N,N-BIS(BETA-CHLOROETHYL)N',O-TRIMETHYLENEPHOSPHORIC ACID ESTER DIAMIDE
**PEER REVIEWED**

CLAFEN
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CLAPHENE
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CYCLOPHOSPHAMID
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CYCLOPHOSPHAN
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CYCLOPHOSPHANE
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CYTOPHOSPHAN
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CYTOPHOSPHANE
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CYTOXAN
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ENDOXAN
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GENOXAL
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NSC 26271
**PEER REVIEWED**

2H-1,3,2-OXAZAPHOSPHORIN-2-AMINE, N,N-BIS(2-CHLOROETHYL)TETRAHYDRO-, 2-OXIDE
**PEER REVIEWED**

2H-1,3,2-OXAZAPHOSPHORINE, 2-(BIS(2-CHLOROETHYL)AMINO)TETRAHYDRO-, 2-OXIDE
**PEER REVIEWED**

PROCYTOX
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SENDOXAN
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Associated Chemicals:

Cyclophosphamide monohydrate;6055-19-2

Formulations/Preparations:

CYCLOPHOSPHAMIDE IS SUPPLIED AS 25 & 50 MG TABLETS & AS A POWDER (100 TO 2000 MG) IN STERILE VIALS.
[Gilman, A.G., T.W. Rall, A.S. Nies and P. Taylor (eds.). Goodman and Gilman's The Pharmacological Basis of Therapeutics. 8th ed. New York, NY. Pergamon Press, 1990. 1217]**PEER REVIEWED**

Grade: USP, measured as containing 95.0 - 105.0% active ingredient calculated as the monohydrate, 5.7 - 6.8% max. water content, 0.002% max. heavy metals, and producing an aqueous solution (1 in 100) at pH 3.9 - 7.1.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

Available as 25 and 50 mg tablets ... and in vials for injection in amounts of 100, 200 or 500 mg measured as containing 90.0 - 110.0% of the stated amount of anhydrous cyclophosphamide.
[IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Man. Geneva: World Health Organization, International Agency for Research on Cancer,1972-PRESENT. (Multivolume work).,p. V26 (1981) 166]**PEER REVIEWED**

EPA Hazardous Waste Number:

U058; A toxic waste when a discarded commercial chemical product or manufacturing chemical intermediate or an off-specification commercial chemical product or manufacturing chemical intermediate.

RTECS Number:

NIOSH/RP5950000

Administrative Information:

Hazardous Substances Databank Number: 3047

Last Revision Date: 20020829
Last Review Date: Reviewed by SRP on 5/11/2002

Great Lake Chemical Corporation and the Pathfinders Camp